| IconNMR Automation Run Status: | |
| Day Experiments: | 00:00 |
| Busy Until: | Wed 13:09 |
| Night Experiments: | 00:00 |
| Holder | Status | Name | ExpNo | Experiment | User | Time | Title |
| 3 | Completed | 250910-iconnmr | 1 | N sst.1H.lsh 1H Lineshape: CHCl3 in d6-Acetone | iconnmr | 00:01:13 | Supervisor Thomas 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height ( < 6 Hz) Linewidth at 0.11% of signal height ( < 12 Hz) Halfwidth ( < 0.6 Hz) |
| 4 | Completed | 250910-iconnmr | 2 | N sst.1H.sen 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 | iconnmr | 00:01:02 | Supervisor Thomas 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found (> 650:1) |
| 5 | Completed | 250910-iconnmr | 3 | N sst.13C.sen 13C Sensitivity 10% Ethylbenzene in CDCl3 | iconnmr | 00:05:04 | Supervisor Thomas 13C Sensitivity 10% Ethylbenzene in CDCl3 Specification result of sinocal: Best sino value found (> 250:1) |
| 6 | Completed | 250910-iconnmr | 4 | N sst.19F.sen-new 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found (> 250:1) | iconnmr | 00:00:10 | Supervisor Thomas Supervisor Thomas Supervisor Thomas 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found (> 250:1) sst.19F.sen-new CDCl3 {E:\Tesla} iconnmr 42 sst.19F.sen-new CDCl3 {E:\Tesla} iconnmr 25 |
| 7 | Completed | 250910-iconnmr | 5 | N sst.31P.sen 31P Sensitivity 0.0485 M triphenylphosphate in d6-acetone | iconnmr | 00:00:12 | Supervisor Thomas 31P Sensitivity 0.0485 M triphenylphosphate in d6-acetone Specification result of sinocal: Best sino value found (> 200:1) |
| Holder | Time | Name | ExpNo | Experiment | User | Load | Atma | Spin | Lock | Shim | Acq | Proc | Title | Remarks |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 4 | 12:37:33 | 250910-iconnmr | 2 | sst.1H.sen | iconnmr | + | + | + | + | + | + | + | Supervisor Thomas 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found (> 650:1) | Automation was stopped by user |
| 7 | 12:30:09 | 250910-iconnmr | 5 | sst.31P.sen | iconnmr | + | + | + | + | + | + | + | Supervisor Thomas 31P Sensitivity 0.0485 M triphenylphosphate in d6-acetone Specification result of sinocal: Best sino value found (> 200:1) | |
| 6 | 12:24:55 | 250910-iconnmr | 4 | sst.19F.sen-new | iconnmr | + | + | + | - | + | + | + | Supervisor Thomas Supervisor Thomas Supervisor Thomas 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found (> 250:1) sst.19F.sen-new CDCl3 {E:\Tesla} iconnmr 42 sst.19F.sen-new CDCl3 {E:\Tesla} iconnmr 25 | |
| 5 | 12:10:44 | 250910-iconnmr | 3 | sst.13C.sen | iconnmr | + | + | + | - | + | + | + | Supervisor Thomas 13C Sensitivity 10% Ethylbenzene in CDCl3 Specification result of sinocal: Best sino value found (> 250:1) | |
| 4 | 12:02:02 | 250910-iconnmr | 2 | sst.1H.sen | iconnmr | + | + | + | + | + | x | - | Supervisor Thomas 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found (> 650:1) | log_err: In experiment: 250910-iconnmr 2 1 E:/Tesla/data/iconnmr/nmr (Parameter Set = 'sst.1H.sen') Exception in drucontr-TRX1: DAM: Error during attempt to notify file change for /root/.topspin-BladeEpu/local_acqu/250910-iconnmr/2/fid: CORBA exception when trying to write remote file "/root/.topspin-BladeEpu/local_acqu/250910-iconnmr/2/fid": TIMEOUT / IDL:omg.org/CORBA/TIMEOUT:1.0 ->Experiment aborted by AccumCtrlServer! , Acquisition Failed |
| 3 | 11:52:57 | 250910-iconnmr | 1 | sst.1H.lsh | iconnmr | + | + | + | + | + | + | + | Supervisor Thomas 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height ( < 6 Hz) Linewidth at 0.11% of signal height ( < 12 Hz) Halfwidth ( < 0.6 Hz) | humpcal: Hump: at 0.11%: between 4819.8 and 4812.5 Hz = 7.3 Hz at 0.55%: between 4817.5 and 4814.4 Hz = 3.1 Hz at 50%: Half width at 4815.8 Hz = 0.31 Hz |