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IconNMR Automation Run Status:
Day Experiments: 00:17
Busy Until: Wed 12:43
Night Experiments: 00:00

Setup List
Holder Status Name ExpNo Experiment User Time Title
31 Completed 250402-iconnmr 6 N sst.1H.lsh 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) iconnmr 00:01:46 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz)
32 Completed 250402-phy 2 N 13C.day 13C experiment; 140 scans, 10 minutes nmrcomm 00:10:26 NMR-2025-10, Q-2025-1 ID-25032
33 Completed 250402-z5489717 1 N 1H 1H experiment z5489717 00:01:00 DSM-R226-H2O DCM ext. COSY CDCl3
33 Running 250402-z5489717 2 N 1H.cosy z5489717 00:10:09 DSM-R226-H2O DCM ext. COSY CDCl3
34 Submitted 250402-z5489717 3 N 1H 1H experiment z5489717 00:01:00 DSM-R228-heat overnight-direct TFT CDCl3
34 Submitted 250402-z5489717 4 N 19F 19F z5489717 00:01:58 DSM-R228-heat overnight-direct TFT CDCl3
35 Submitted 250402-z5489717 5 N 1H 1H experiment z5489717 00:01:00 DSM-R228-heat overnight-vac. TFT CDCl3
35 Submitted 250402-z5489717 6 N 19F 19F z5489717 00:01:58 DSM-R228-heat overnight-vac. TFT CDCl3
36 Submitted 250402-z3541685 1 N 1H 1H experiment z3541685 00:01:00 MWB_04_045a
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
33 12:16:10 250402-z5489717 2 1H.cosy z5489717 - - - - - - - DSM-R226-H2O DCM ext. COSY CDCl3
33 12:07:40 250402-z5489717 1 1H z5489717 + + + + + + + DSM-R226-H2O DCM ext. COSY CDCl3
32 11:51:21 250402-phy 2 13C.day nmrcomm + + + + + + + NMR-2025-10, Q-2025-1 ID-25032 ADC reported overflow
31 11:41:18 250402-iconnmr 6 sst.1H.lsh iconnmr + x + + + + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) ATM Failed, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/6/pdata/1/250402-iconnmr_6_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/6/pdata/1/250402-iconnmr_6_1.pdf Check for printing system problems
30 11:34:31 250402-phy 1 31P{1H}.pg nmrcomm + + + + + + + NMR-2025-10, Q-2025-1 ID-25032
29 11:21:15 250402-z5550254 1 1H z5550254 + + + + + + + AY-075.crude
29 10:59:41 250402-z5550254 1 1H z5550254 + + + + + x - AY-075.crude Acquisition Failed
28 10:51:07 250402-iconnmr 5 sst.31P.sen iconnmr + + + + + + + 31P Sensitivity 0.0485 M triphenylphosphate (TPP) in d6-acetone Specification result of sinocal: Best sino value found ( > 150:1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/5/pdata/1/250402-iconnmr_5_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/5/pdata/1/250402-iconnmr_5_1.pdf Check for printing system problems
27 10:39:58 250402-iconnmr 4 sst.19F.qnp.sen iconnmr + + + + + + + 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found ( > 250 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/4/pdata/1/250402-iconnmr_4_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/4/pdata/1/250402-iconnmr_4_1.pdf Check for printing system problems
26 10:18:20 250402-iconnmr 3 sst.13C.sen iconnmr + x + + + + + 13C Sensitivity 10% Ethylbenzene (EB) in CDCl3 Specification result of sinocal: Best sino value found ( > 200 :1) ATM Failed, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/3/pdata/1/250402-iconnmr_3_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/3/pdata/1/250402-iconnmr_3_1.pdf Check for printing system problems
25 10:08:35 250402-iconnmr 2 sst.1H.sen iconnmr + + + + + + + 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found ( > 300 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/2/pdata/1/250402-iconnmr_2_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/2/pdata/1/250402-iconnmr_2_1.pdf Check for printing system problems
24 09:57:59 250402-iconnmr 1 sst.1H.lsh iconnmr + + + + + + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/1/pdata/1/250402-iconnmr_1_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250402-iconnmr/1/pdata/1/250402-iconnmr_1_1.pdf Check for printing system problems
2 09:01:25 250402-z5363218 1 1H z5363218 + + + + + + + CDO-4 Automation was stopped by user
1 08:20:23 250402-isj 1 19F{1H} isj + + + + + + + IJ-026 set 2 after hplc
43 01:09:39 250401-rdr 2 1H rdr + x + + + + + 2-018 rt B ATM Failed
42 01:03:11 250401-rdr 1 1H rdr + + + + + + + 2-018 rt A
41 00:52:13 250401-z5485590 1 1H z5485590 + + + + + + + MM339-010425-0620pm
40 22:44:14 250401-ccc 3 13C.night ccc - x + - - + + GC8093-13C; C5 6-quinoline isopropyl amination; F8-23; CDCl3; 400MHz ATM Failed
40 22:36:44 250401-ccc 2 1H ccc + + + + + + + GC8093; C5 6-quinoline isopropyl amination; F8-23; CDCl3; 400MHz
39 21:32:52 250401-law 4 13C.night law - x + - - + + WJ-D1-19 ATM Failed, ADC reported overflow
39 21:26:36 250401-law 3 1H law + x + + + + + WJ-D1-19 ATM Failed
38 21:18:33 250401-law 2 1H law + + + + + + + LW-167-A1-P1-F2+17-19
37 21:11:02 250401-law 1 1H law + + + + + + + LW-167-A1-P1-F3-16
36 21:07:40 250401-jsm 5 11B jsm - + + - - + + JM308 ethynylbenzene BMIDA check for step 1 to see if any left before adding indole, Zn(OTf)2 approx 20h blue LED irradiation
36 20:56:34 250401-jsm 4 1H jsm + + + + + + + JM308 ethynylbenzene BMIDA check for step 1 to see if any left before adding indole, Zn(OTf)2 approx 20h blue LED irradiation
35 20:47:47 250401-jsm 3 1H jsm + + + + + + + JM305mm
34 20:36:55 250401-jsm 2 1H jsm + + + + + + + JM305ll
33 20:27:15 250401-jsm 1 1H jsm + + + + + + + JM305kk
32 20:16:33 250401-jnn 1 1H jnn + + + + + + + JAN-212.1
31 19:11:04 250401-z5550254 12 13C.night z5550254 - + + - - + + AY-2PF
31 19:04:35 250401-z5550254 11 19F{1H} z5550254 - + + - - + + AY-2PF
31 18:57:48 250401-z5550254 10 19F z5550254 - + + - - + + AY-2PF
31 18:42:14 250401-z5550254 9 1H z5550254 + + + + + + + AY-2PF
30 17:36:42 250401-z5550254 8 13C.night z5550254 - + + - - + + AY-074.4 ADC reported overflow
30 17:29:25 250401-z5550254 7 19F{1H} z5550254 - + + - - + + AY-074.4
30 17:24:13 250401-z5550254 6 19F z5550254 - x + - - + + AY-074.4 ATM Failed
30 17:10:00 250401-z5550254 5 1H z5550254 + + + + + + + AY-074.4
29 17:04:02 250401-z5676313 2 11B z5676313 - + + - - + + AB-19-zs1
29 16:57:06 250401-z5676313 1 1H z5676313 + + + + + + + AB-19-zs1
27 16:47:06 250401-zhz 3 1H zhz + + + + + + + ZZ-104 CDCl3 insoluble
28 16:30:53 250401-z5438782 3 1H z5438782 + + + + + + + bapo 6h
27 16:19:41 250401-zhz 2 1H zhz + + + + + + + ZZ-104 worked up
26 16:11:26 250401-zhz 1 1H zhz + + + + + + + ZZ-101 crude
25 16:06:46 250401-z5489717 4 19F z5489717 - + + - - + + DSM-R228-2day-crude-direct-TFT CDCl3
25 16:00:00 250401-z5489717 3 1H z5489717 + + + + + + + DSM-R228-2day-crude-direct-TFT CDCl3
24 15:54:20 250401-z5489717 2 19F z5489717 - + + - - + + DSM-R228-2day-crude-dried-TFT CDCl3
24 15:47:29 250401-z5489717 1 1H z5489717 + + + + + + + DSM-R228-2day-crude-dried-TFT CDCl3
23 15:39:44 250401-z5547474 2 1H z5547474 + + + + + + + P(LA-co-DEGEEA)-CTA 54k crude
22 15:32:19 250401-z5547474 1 1H z5547474 + + + + + + + P(LA-co-DEGEEA)-CTA 32k crude
21 15:23:11 250401-kee 1 1H kee + + + + + + + DMSO-BisXan
20 15:12:40 250401-z5438782 2 1H z5438782 + + + + + + + bapo 4h
51 15:05:05 250401-z5550254 4 1H z5550254 + + + + + + + AY-074.4
50 14:57:13 250401-z5550254 3 1H z5550254 + x + + + + + AY-074.3 ATM Failed
49 14:48:50 250401-z5550254 2 1H z5550254 + + + + + + + AY-074.2
48 14:41:28 250401-z5550254 1 1H z5550254 + x + + + + + AY-074.1 ATM Failed
47 14:31:48 250401-dgu 3 1H.es dgu + + + + + + + 10 mM dihydroxyacetone
46 14:19:57 250401-dgu 2 1H.es dgu + + + + + + + 10 mM glyceraldehyde
45 14:10:19 250401-dgu 1 1H.es dgu + x + + + + + 10 vol% glycerol ATM Failed
19 14:00:47 250401-thh 2 1H thh + x + + + + + B79-4-37 ATM Failed
18 13:49:24 250401-thh 1 1H thh + + + + + + + B79-4-36
17 13:42:05 250401-z5564533 7 1H z5564533 + + + + + + + CM-069-3
16 13:32:34 250401-yux 5 1H yux + + + + + + + saved pba113-phea56 pr
15 13:20:16 250401-yux 4 1H yux + + + + + + + 0331 pba133-phea66 random 17.5h cr
41 12:32:50 250401-djg 1 1H djg + x + + + + + DJG-B-152 2,5-dimethylterephthalic acid ATM Failed
40 12:11:12 250401-z3545554 1 1H z3545554 + + + + + + +
14 12:01:34 250401-suj 1 1H suj + + + + + + + ss-25-04 o.n. crude a/w
13 11:44:51 250401-z5382436 5 1H z5382436 + + + + + + + T7
12 11:35:35 250401-z5382436 4 1H z5382436 + + + + + + + T6
11 11:26:16 250401-z5382436 3 1H z5382436 + x + + + + + T5 ATM Failed
10 11:14:44 250401-z5382436 2 1H z5382436 + + + + + + + T4
9 11:05:59 250401-z5382436 1 1H z5382436 + x + + + + + AH02,140 T1 ATM Failed
8 10:59:40 250401-ccc 1 1H ccc + x + + + + + GC8095; 6-methyl C5 borylation; crude; CDCl3; 400MHz ATM Failed
7 10:27:50 250401-z5564533 6 19F{1H} z5564533 - + + - - + + CM-070-2
7 10:23:43 250401-z5564533 5 19F z5564533 - + + - - + + CM-070-2
7 10:12:13 250401-z5564533 4 1H z5564533 + + + + + + + CM-070-2
6 10:08:42 250401-z5564533 3 19F{1H} z5564533 - x + - - + + CM-070-1 ATM Failed
6 10:03:51 250401-z5564533 2 19F z5564533 - + + - - + + CM-070-1
6 09:53:32 250401-z5564533 1 1H z5564533 + x + + + + + CM-070-1 ATM Failed
5 09:48:53 250401-yux 3 1H yux + + + x - - - 0207 pba113-phea56 pr Lock failed after multiple attempts
4 09:38:44 250401-yux 2 1H yux + + + + + + + 0331 pba133-phea66 random 16h cr
3 09:30:25 250401-yux 1 1H yux + + + + + + + 0331 pba133-phea66 random 0h
2 09:11:59 250401-z5438782 1 1H z5438782 + + + + + + + elp
18 00:58:32 250331-yab 3 15N yab - + + - - + + TROPLN+_NOH_PURE
18 23:02:09 250331-yab 2 13C.night yab + x + + + + + TROPLN+_NOH_PURE ATM Failed
1 22:52:21 250331-z3545554 1 1H z3545554 + + + + + + +
47 22:45:20 250331-z5676313 3 1H z5676313 + + + + + + + ss-25-04 crude 2hr after workup
46 22:41:55 250331-z5676313 2 11B z5676313 - + + - - + + HBpin
46 22:34:01 250331-z5676313 1 1H z5676313 + + + + + + + HBpin
45 22:25:26 250331-jlt 5 1H jlt + x + + + + + JT-P5JS-03-prod-D2Os ATM Failed
44 22:21:31 250331-jlt 4 19F{1H} jlt - x + - - + + JT-P5J5-02d-flask ATM Failed
44 22:12:09 250331-jlt 3 1H jlt + + + + + + + JT-P5J5-02d-flask
43 22:06:45 250331-jlt 2 19F{1H} jlt - x + - - + + JT-P5J5-02d-fl4 ATM Failed
43 21:56:54 250331-jlt 1 1H jlt + + + + + + + JT-P5J5-02d-fl4
42 21:49:40 250331-z5543281 1 1H z5543281 + + + + + + + TSDA7 after base wash
41 21:42:25 250331-ild 3 1H ild + + + + + + + ID12053; condensation cr; DMSO
40 21:33:58 250331-z5363829 1 1H.es z5363829 + + + + x + + PET D2O Maleic Acid Shim failed
39 21:22:14 250331-nnt 5 13C.dept135 nnt - + + - - + + PGV-001-2
39 21:08:46 250331-nnt 4 1H13C.hmbc nnt - + + - - + + PGV-001-2
39 20:49:50 250331-nnt 3 1H13C.hsqc.aded nnt - + + - - + + PGV-001-2
39 19:44:56 250331-nnt 2 13C.night nnt - + + - - + + PGV-001-2
39 19:38:19 250331-nnt 1 1H nnt + + + + + + + PGV-001-2
38 19:18:29 250331-z5564533 9 1H13C.hsqc.aded z5564533 - + + - - + + CM-065-1-3
38 19:07:29 250331-z5564533 8 1H.cosy z5564533 - + + - - + + CM-065-1-3
38 19:04:00 250331-z5564533 7 1H z5564533 - + + - - + + CM-065-1-3
38 18:59:55 250331-z5564533 5 19F z5564533 - + + - - + + CM-065-1-3
38 18:52:55 250331-z5564533 3 19F{1H} z5564533 - + + - - + + CM-065-1-3
38 17:44:24 250331-z5564533 2 13C.night z5564533 + + + + + + + CM-065-1-3
37 17:24:58 250331-z5564533 10 1H13C.hsqc.aded z5564533 - + + - - + + CM-065-1-2
37 17:13:33 250331-z5564533 9 1H.cosy z5564533 - + + - - + + CM-065-1-2
37 17:10:41 250331-z5564533 6 1H z5564533 - + + - - + + CM-065-1-2
37 17:05:35 250331-z5564533 4 19F{1H} z5564533 - + + - - + + CM-065-1-2
37 17:01:00 250331-z5564533 3 19F z5564533 - + + - - + + CM-065-1-2
37 15:51:19 250331-z5564533 1 13C.night z5564533 + + + + + + + CM-065-1-2
36 15:44:55 250331-cke 7 1H cke + + + + + + + CKL-23B-10 bluebox half 2 TFA Vial 10
35 15:38:37 250331-cke 6 1H cke + + + + + + + CKL-23B-5 bluebox half 2 TFA Vial 5
34 15:32:53 250331-cke 5 1H cke + x + + + + + CKL-23B-4 bluebox half 2 TFA Vial 4 ATM Failed
33 15:26:19 250331-cke 4 1H cke + + + + + + + CKL-23B-3 bluebox half 2 TFA Vial 3
32 15:19:25 250331-cke 3 1H cke + x + + + + + CKL-23B-2 bluebox half 2 TFA Vial 2 ATM Failed
31 15:11:51 250331-cke 2 1H cke + + + + + + + CKL-23B-1 bluebox half 2 TFA Vial 1
30 15:04:07 250331-cke 1 1H cke + + + + + + + CKL-23A-4 bluebox half 1 TFA Vial 4
29 14:55:31 250331-djg 3 1H djg + + + + + + + DJG-S-015b Isopyrocoll malononitrile for TR-EPR post hexane trit
28 14:46:13 250331-isj 1 19F{1H} isj + + + + + + + IJ-026 set 1 after HPLC
27 14:38:45 250331-yfo 3 1H yfo + x + + + + + df30 1545 m ATM Failed
26 14:31:12 250331-yfo 2 1H yfo + + + + + + + df30 1645 m
25 14:23:26 250331-yfo 1 1H yfo + + + + + + + df30 1445 m
24 14:15:00 250331-suj 3 1H suj + + + + + + + ss-25-03 f red
23 14:08:38 250331-suj 2 1H suj + + + + + + + ss-25-03 f orange 2
22 14:00:33 250331-suj 1 1H suj + + + + + + + ss-25-03 f orange 1
21 13:52:28 250331-zhz 2 1H zhz + + + + x + + ZZ-101 DCE overnight reflux + BF3 Shim failed
20 13:43:53 250331-zhz 1 1H zhz + + + + + + + ZZ-080 pyrrole to CCl3COCl
19 13:23:10 250331-rdr 2 1H rdr + + + + + + + 2-018 r.t
18 13:12:55 250331-rdr 1 1H rdr + + + + + + + 2-018 0C old
17 13:04:17 250331-phy 1 1H nmrcomm + + + + + + + CDCl3 screening
16 12:02:12 250331-yab 1 1H yab + + + + + + + TROPLN+_NOH_MEOH
15 11:54:14 250331-ild 2 1H ild + + + + + + + ID12053; glyoxylate amide condensation cr; CDCl3
14 11:46:56 250331-ild 1 1H ild + + + + + + + ID12051; oxidative Heck cr; CDCl3
13 11:39:47 250331-djg 2 1H djg + + + + + + + DJG-S-015b ipc malononitrile purity check for TR-EPR
12 11:13:57 250331-amn 1 1H amn + + + + + + + AMM - H-010 - NiTMP in tol-d8 - dissolved Ni(acac)2 in MeOH and spiked plug with Et3N
11 10:51:44 250331-djg 1 1H djg + + + + + + + DJG-S-015a dtipc purity check for TR-EPR
10 09:50:38 250331-jnn 3 19F{1H} jnn - + + - - + + JAN-211.1
10 09:40:19 250331-jnn 2 19F jnn - + + - - + + JAN-211.1
10 09:29:33 250331-jnn 1 1H jnn + + + + + + + JAN-211.1
10 09:27:02 250331-jnn 1 1H jnn x - - - - - - JAN-211.1 Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 10
10 09:25:04 250331-jnn 1 1H jnn x - - - - - - JAN-213 Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 10
8 09:05:22 250331-z5489717 2 19F z5489717 - + + - - + + DSM-R228-overnight-direct-crude TFT CDCl3
8 08:54:31 250331-z5489717 1 1H z5489717 + + + + + + + DSM-R228-overnight-direct-crude TFT CDCl3
7 19:18:07 250330-thh 6 1H thh + x + + + + + B80-5-2 ATM Failed
6 19:09:39 250330-thh 5 1H thh + + + + + + + B80-5-1
5 18:59:36 250330-thh 4 1H thh + + + + + + + benz
4 17:55:31 250330-z5550254 16 13C.night z5550254 - x + - - + + AY-073.2 new ATM Failed
4 17:49:22 250330-z5550254 15 19F{1H} z5550254 - + + - - + + AY-073.2 new
4 17:43:28 250330-z5550254 14 19F z5550254 - + + - - + + AY-073.2 new
4 17:28:51 250330-z5550254 13 1H z5550254 + + + + + + + AY-073.2 new
3 16:22:56 250330-z5550254 12 13C.night z5550254 - + + - - + + AY-073.2 ADC reported overflow
3 16:17:34 250330-z5550254 11 19F{1H} z5550254 - x + - - + + AY-073.2 ATM Failed
3 16:11:24 250330-z5550254 10 19F z5550254 - + + - - + + AY-073.2
3 15:57:30 250330-z5550254 9 1H z5550254 + x + + + + + AY-073.2 ATM Failed
2 15:47:38 250330-thh 3 1H thh + + + + + + + TB-04-14
1 15:35:41 250330-thh 2 13C.day thh - x + - - + + TB-04 ATM Failed
1 15:28:15 250330-thh 1 1H thh + + + + + + + TB-04
60 14:59:26 250330-z5426952 1 1H z5426952 + + + + + + + RI-Boc-Br
59 14:34:26 250330-z5550254 8 1H z5550254 + + + + + + + AY-073.3
58 14:21:13 250330-z5550254 7 1H z5550254 + + + + + + + AY-073.2
57 14:06:41 250330-z5550254 6 1H z5550254 + + + + + + + AY-073.1
56 12:01:42 250330-z5550254 5 13C.night z5550254 - + + - - + + AY-070
56 11:48:18 250330-z5550254 4 1H z5550254 + + + + + + + AY-070
55 11:36:59 250330-z5438782 1 1H z5438782 + + + + + + + elp 50/50 re 2h
54 09:43:05 250330-z5550254 3 19F{1H} z5550254 - + + - - + + AY-065.crude
54 09:37:39 250330-z5550254 2 19F z5550254 - + + - - + + AY-065.crude
54 09:27:06 250330-z5550254 1 1H z5550254 + + + + + + + AY-065.crude
53 20:45:16 250329-dem 4 1H dem + + + + + + + DM-MS-02-82A
52 19:33:34 250329-dem 3 1H dem + + + + + + + DM-MS-03-80B
51 18:21:37 250329-dem 2 1H dem + + + + + + + DM-MS-03-80A
50 17:09:47 250329-dem 1 1H dem + + + + + + + DM-MS-02-68F-Dep
49 02:28:59 250328-z3544630 5 1H z3544630 + x + + + + + DE-FBTZ-CO2-DMSO ATM Failed
48 02:21:40 250328-z3544630 4 1H z3544630 + x + + + + + TE-DBB-CO2-CDCl3 ATM Failed
47 02:14:45 250328-z3544630 3 1H z3544630 + + + + + + + DE-DBB-CO2-CDCl3
46 02:07:32 250328-z3544630 2 1H z3544630 + + + + + + + TE-FBTZ-CO2-CDCl3
45 01:57:36 250328-z3544630 1 1H z3544630 + + + + + + + DE-FBTZ-CO2-CDCl3
44 01:47:41 250328-mda 4 1H mda + + + + + + + VKK-05
43 01:40:44 250328-mda 3 1H mda + + + + + + + VKK-04
42 01:31:46 250328-mda 2 1H mda + x + + + + + Re_CinCTA-CD ATM Failed
41 01:23:25 250328-mda 1 1H mda + + + + + + + Re_Cin CTA-DM
40 01:18:23 250328-z5550254 5 19F{1H} z5550254 - x + - - + + AY-073.2 ATM Failed
40 01:13:09 250328-z5550254 4 19F z5550254 - x + - - + + AY-073.2 ATM Failed
40 00:58:23 250328-z5550254 3 1H z5550254 + + + + + + + AY-073.2
39 00:45:39 250328-z5550254 2 1H z5550254 + x + + + + + AY-070.2 ATM Failed
38 00:31:43 250328-z5550254 1 1H z5550254 + + + + + + + AY-070.1
37 22:24:50 250328-ccc 2 13C.night ccc - + + - - + + GC8023; C5 aminopyrimidine isopropyl amination; C2F11-16; CDCl3; 400MHz
37 22:15:58 250328-ccc 1 1H ccc + + + + + + + GC8023; C5 aminopyrimidine isopropyl amination; C2F11-16; CDCl3; 400MHz
36 22:08:05 250328-jcy 12 1H jcy + + + + + + + VP-03-03-100-T6h
35 22:00:38 250328-jcy 11 1H jcy + + + + + + + VP-03-03-75-T6h
34 21:53:21 250328-jcy 10 1H jcy + + + + + + + VP-03-02-100-T6h
33 21:46:18 250328-jcy 9 1H jcy + x + + + + + VP-03-02-75-T6h ATM Failed
32 21:36:26 250328-jcy 8 1H jcy + + + + + + + VP-03-01-100-T6h
31 21:28:38 250328-jcy 7 1H jcy + + + + + + + VP-03-01-75-T6h
30 21:20:39 250328-jcy 6 1H jcy + x + + + + + VP-03-03-100-T0 ATM Failed
29 21:13:23 250328-jcy 5 1H jcy + + + + + + + VP-03-03-75-T0
28 21:06:13 250328-jcy 4 1H jcy + + + + + + + VP-03-02-100-T0
27 20:58:19 250328-jcy 3 1H jcy + + + + + + + VP-03-02-75-T0
26 20:50:48 250328-jcy 2 1H jcy + + + + + + + VP-03-01-100-T0
25 20:43:46 250328-jcy 1 1H jcy + x + + + + + VP-03-01-75-T0 ATM Failed
24 20:33:35 250328-z3541685 2 1H z3541685 + + + + + + + MWB_04_043d
23 20:27:00 250328-z3541685 1 1H z3541685 + + + + + + + MWB_04_043c
22 19:23:16 250328-jlt 14 13C.night jlt - x + - - + + JT-P5JS-03-col ATM Failed, ADC reported overflow
22 19:17:46 250328-jlt 13 19F{1H} jlt - + + - - + + JT-P5JS-03-col
22 19:06:49 250328-jlt 12 1H.cosy jlt - + + - - + + JT-P5JS-03-col
22 18:57:12 250328-jlt 11 1H jlt + + + + + + + JT-P5JS-03-col
20 18:43:44 250328-z5493478 7 1H13C.hmbc z5493478 - + + - - + + SIC045 full characterization DMSO Weber
20 18:24:13 250328-z5493478 6 1H13C.hsqc.aded z5493478 - + + - - + x SIC045 full characterization DMSO Weber
20 17:49:10 250328-z5493478 5 1H.noesy z5493478 - + + - - + + SIC045 full characterization DMSO Weber
20 17:37:53 250328-z5493478 4 1H.cosy z5493478 - + + - - + + SIC045 full characterization DMSO Weber
20 17:29:49 250328-z5493478 3 19F z5493478 - + + - - + + SIC045 full characterization DMSO Weber
20 15:22:30 250328-z5493478 2 13C.night z5493478 - + + - - + + SIC045 full characterization DMSO Weber ADC reported overflow
20 15:15:12 250328-z5493478 1 1H z5493478 + + + + + + + SIC045 full characterization DMSO Weber
19 14:01:57 250328-rdr 2 1H rdr + + + + + + + tosyl phenyl hydrazine resubmit
18 13:52:37 250328-rdr 1 1H rdr + x + + + + + 2-018 NMe r.t ATM Failed
17 13:42:21 250328-sub 4 1H sub + x + + + + + SB-SFD-2 CF5 CDCl3 ATM Failed
16 13:33:55 250328-sub 3 1H sub + + + + + + + SB148 DF4 after distillation CDCl3
15 13:25:15 250328-sub 2 1H sub + + + + + + + SB148 DF3 after distillation CDCl3
14 13:16:29 250328-sub 1 1H sub + + + + + + + SB148 DF2 after distillation CDCl3
13 13:09:24 250328-yab 3 1H yab + + + + + + + TRN+NOH_IISPOT
12 13:02:40 250328-yab 1 1H yab + + + + + + + TRN+NOH_ISPOT
11 12:55:23 250328-ogc 1 1H ogc + x + + + + + OG8035, K11 Boc pyrazole crude, DMSO ATM Failed
10 12:50:46 250328-jlt 10 19F{1H} jlt - + + - - + + 2499-011-impure-check
10 12:41:24 250328-jlt 9 1H jlt + x + + + + + 2499-011-impure-check ATM Failed
9 12:36:54 250328-jlt 8 19F{1H} jlt - + + - - + + X-3092-fum-19F{1H}
9 12:30:08 250328-jlt 7 1H jlt + + + + + + + X-3092-fum-19F{1H}
8 12:25:46 250328-jlt 6 19F{1H} jlt - + + - - + + JT-P5JR-05E-fb-D2Os-19F{1H}
8 12:16:46 250328-jlt 5 1H jlt + + + + + + + JT-P5JR-05E-fb-D2Os-19F{1H}
7 12:12:38 250328-jlt 4 19F{1H} jlt - + + - - + + JT-P5JR-05B-fum-D2Os-19F{1H}
7 12:03:58 250328-jlt 3 1H jlt + + + + + + + JT-P5JR-05B-fum-D2Os-19F{1H}
6 11:58:58 250328-jlt 2 19F{1H} jlt - + + - - + + JT-P5J5-05C-fum-D2Os-19F{1H}
6 11:49:57 250328-jlt 1 1H jlt + + + + + + + JT-P5J5-05C-fum-D2Os-19F{1H}
5 11:41:52 250328-z5489717 1 1H z5489717 + + + + + + + DSM-R226-H20 DCM ext. CDCl3
4 11:29:55 250328-gab 2 13C.day gab - x + - - + + gab-4-84 ATM Failed
4 11:22:53 250328-gab 1 1H gab + + + + + + + gab-4-84
20 10:48:55 250328-z3545554 3 1H z3545554 + + + + + + +
3 10:42:28 250328-z3545554 2 1H z3545554 + + + + + + +
1 10:32:44 250328-z3545554 1 1H z3545554 + + + + + + +
45 05:46:27 250327-z5676313 8 11B z5676313 - + + - - + + AB-15-m3
45 05:38:26 250327-z5676313 7 1H z5676313 + + + + + + + AB-15-m3
1 05:32:01 250327-z3545554 1 1H z3545554 + x + + + + + chiral-step 1 ATM Failed
52 05:25:45 250327-rdr 4 1H rdr + + + + + x - Tosyl phenyl hydrazine? Acquisition Failed
51 05:16:58 250327-rdr 3 1H rdr + + + + + + + Sakurai 2?
50 05:07:21 250327-rdr 2 1H rdr + + + + + + + Sakurai 1?
49 04:58:14 250327-z3544630 1 1H z3544630 + + + + + + + PET+H2O2-PC 6h 300+50 mM MA D2O 300
48 03:53:36 250327-jlt 6 13C.night jlt - + + - - + + JT-P5H1-04-col
48 03:42:34 250327-jlt 5 1H.cosy jlt - + + - - + + JT-P5H1-04-col
48 03:28:45 250327-jlt 4 1H13C.hmbc jlt - + + - - + + JT-P5H1-04-col
48 03:09:05 250327-jlt 3 1H13C.hsqc.aded jlt - + + - - + + JT-P5H1-04-col
48 03:00:23 250327-jlt 2 19F{1H} jlt - + + - - + + JT-P5H1-04-col
48 02:47:32 250327-jlt 1 1H jlt + + + + + + + JT-P5H1-04-col
47 02:40:13 250327-thh 13 1H thh + x + + + + + TB-03--36 ATM Failed
46 02:26:56 250327-thh 12 13C.day thh - + + - - + + TB-03--35
46 02:19:27 250327-thh 11 1H thh + + + + + + + TB-03--35
45 02:16:39 250327-z5676313 8 11B z5676313 - + + - - + + AB-15-m3
45 02:10:22 250327-z5676313 7 1H z5676313 + + + + + x - AB-15-m3 Acquisition Failed, JDX Copy failed
44 02:06:18 250327-z5676313 6 11B z5676313 - + + - - + + AB-15-m2
44 01:57:53 250327-z5676313 5 1H z5676313 + + + + + + + AB-15-m2
43 01:55:31 250327-z5676313 4 11B z5676313 - x + - - + + AB-15-m1 ATM Failed
43 01:48:54 250327-z5676313 3 1H z5676313 + + + + + + + AB-15-m1
42 01:45:43 250327-z5676313 2 11B z5676313 - + + - - + + AB-15-r
42 01:39:05 250327-z5676313 1 1H z5676313 + + + + + + + AB-15-r
41 01:28:51 250327-sub 5 1H sub + x + + + + + SB-SFD-2 CF4 DPND-7 dimer with Ph(acy)2 spacer CDCl3 ATM Failed
40 01:18:39 250327-sub 4 1H sub + + + + + + + SB-SFD-2 CF3 DPND-7 dimer with Ph(acy)2 spacer CDCl3
39 01:09:45 250327-sub 3 1H sub + x + + + + + SB-SFD-2 CF2 DPND-7 dimer with Ph(acy)2 spacer CDCl3 ATM Failed
38 00:58:20 250327-sub 2 1H sub + + + + + + + SB-SFD-2 CF1 DPND-7 dimer with Ph(acy)2 spacer CDCl3
37 23:53:50 250327-yab 3 13C.night yab - x + - - + + TROPLN+_NH_CRY ATM Failed, ADC reported overflow
37 23:47:22 250327-yab 2 1H yab + + + + + + + TROPLN+_NH_CRY
36 23:38:56 250327-jnn 3 19F{1H} jnn - x + - - + + JAN-209.1 ATM Failed
36 23:29:45 250327-jnn 2 19F jnn - + + - - + + JAN-209.1
36 23:18:15 250327-jnn 1 1H jnn + + + + + + + JAN-209.1
35 22:13:33 250327-z5550254 5 13C.night z5550254 - + + - - + + AY-P2F
35 21:57:45 250327-z5550254 4 1H z5550254 + + + + + + + AY-P2F
34 20:53:04 250327-z5550254 3 13C.night z5550254 - + + - - + + AY-070
34 20:37:02 250327-z5550254 2 1H z5550254 + + + + + + + AY-070
33 16:18:33 250327-z5550254 1 1H z5550254 + + + + + + + AY-021 Automation was stopped by user
32 16:10:05 250327-mda 2 1H mda + + + + + + + CRL-DM
31 16:02:07 250327-mda 1 1H mda + x + + + + + CRL-CD ATM Failed
30 15:55:26 250327-yab 1 1H yab + x + + + + + TROPLN+_NH_III ATM Failed
29 15:47:49 250327-ccc 1 1H ccc + + + + + + + GC8027; 6-methyl C5 iodination; F8-12 re-nmr; CDCl3; 400MHz
28 15:35:35 250327-zhz 1 1H zhz + + + + + + + ZZ-101 crude
27 15:18:07 250327-thh 10 13C.day thh - + + - - + + TA-62
27 15:10:06 250327-thh 9 1H thh + + + + + + + TA-62
26 15:00:15 250327-nap 2 1H nap + + + + + + + 110m
25 14:49:08 250327-nap 1 1H nap + + + + + + + 110l
24 14:40:49 250327-z5540930 1 1H z5540930 + + + + + + + P1 530 boc r pure
23 14:30:28 250327-amn 1 1H amn + + + + + + + AMM-H009-First plug fraction washed with hexane with 1% pyr-d5
22 14:22:32 250327-z5319902 1 1H z5319902 + + + + + + + AA-021
21 14:16:13 250327-z3541685 4 1H z3541685 + + + + + + + MWB_04_043b
20 14:08:11 250327-z3541685 3 1H z3541685 + + + + + + + MWB_04_043a
19 13:48:18 250327-thh 8 13C.day thh + x + + + + + B79-2 ATM Failed
18 13:41:00 250327-suj 1 1H suj + + + + + + + ss-25-03 large scale o.n. a/workup
17 13:30:54 250327-thh 7 1H thh + + + + + + + B80-5-3
16 13:24:16 250327-thh 6 1H thh + + + + + + + B80-5-2
15 13:17:28 250327-thh 5 1H thh + + + + + + + B80-5-1
14 13:10:50 250327-thh 4 1H thh + + + + + + + B79-E3
13 13:04:54 250327-thh 3 1H thh + x + + + + + B79-E2 ATM Failed
12 12:56:53 250327-thh 2 1H thh + + + + + + + B79-E1
11 12:33:52 250327-rdr 1 1H rdr + x + + + + + 2-018 4CN 30C ATM Failed
10 12:27:44 250327-z3541685 2 1H z3541685 + + + + + + + MWB_04_036d
9 12:21:42 250327-z3541685 1 1H z3541685 + + + + + + + MWB_04_036c
8 12:12:23 250327-z5628481 1 1H z5628481 + + + + + + + methyl prop. reac col f1 1H
7 12:05:43 250327-z5438782 2 1H z5438782 + + + + + + + elp
6 11:58:11 250327-thh 1 1H thh + x + + + + + B79-2 ATM Failed
5 11:46:31 250327-z5489717 7 1H.cosy z5489717 - + + - - + + DSM-R224-2day-crude-vac. CDCl3
5 11:41:54 250327-z5489717 6 19F z5489717 - x + - - + + DSM-R224-2day-crude-vac. CDCl3 ATM Failed
5 11:33:44 250327-z5489717 5 1H z5489717 + + + + + + + DSM-R224-2day-crude-vac. CDCl3
4 10:15:55 250327-z5438782 1 1H z5438782 + + + + + + + pelp after purifying 3
3 10:09:49 250327-z5489717 4 19F z5489717 - + + - - + + DSM-R223-2-day crude-direct CDCl3
3 10:02:16 250327-z5489717 3 1H z5489717 + + + + + + + DSM-R223-2-day crude-direct CDCl3
2 09:57:13 250327-z5489717 2 19F z5489717 - + + - - + + DSM-R224-overnight-crude-direct TFT shift ref. CDCl3
2 09:50:28 250327-z5489717 1 1H z5489717 + + + + + + + DSM-R224-overnight-crude-direct TFT shift ref. CDCl3
1 09:27:07 250327-sub 1 1H sub + + + + + + + SB 148 crude CDCl3
56 01:34:38 250326-jsm 5 1H jsm x - - - - - - JM308 (BMIDA ethynylbenzene + BQ + indole + Zn(OTf)2 blue light rxn) Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 56
55 01:21:46 250326-z5543307 8 13C.day z5543307 - + + - - + + RAK-02-070 (Lowest spot-Unk)
55 01:15:26 250326-z5543307 7 1H z5543307 + + + + + + + RAK-02-070 (Lowest spot-Unk)
54 00:10:39 250326-z5543307 6 13C.night z5543307 - + + - - + + RAK-02-070 (Frac-2)
54 00:04:21 250326-z5543307 5 1H z5543307 + + + + + + + RAK-02-070 (Frac-2)
53 23:51:23 250326-z5543307 4 13C.day z5543307 - + + - - + + RAK-02-070 (Frac-1)
53 23:45:26 250326-z5543307 3 1H z5543307 + x + + + + + RAK-02-070 (Frac-1) ATM Failed
52 23:32:34 250326-z5543307 2 13C.day z5543307 - + + - - + + RAK-02-070 (Pure F.)
52 23:24:16 250326-z5543307 1 1H z5543307 + + + + + + + RAK-02-070 (Pure F.)
51 23:10:18 250326-sub 6 1H sub + + + + + + + SB145-E+TEA protecting CHO of indole-2-CHO CDCl3
50 22:56:59 250326-sub 5 1H sub + x + + + + + SB148 crude Protecting CHO of Furan-3-aldehyde CDCl3 ATM Failed
49 22:49:26 250326-sub 4 1H sub + + + + + + + Furan-3-carbaldehyde CDCl3
48 22:35:46 250326-sag 1 1H sag + + + + + + + GSN-JW-pyrrolidne cr
47 22:27:56 250326-ccc 4 1H ccc + + + + + + + GC8089; methene reduction; crude; CDCl3; 400MHz
46 22:18:09 250326-z5455435 4 1H z5455435 + + + + + + + C83 Amine After Purification
45 20:08:56 250326-ccc 3 13C.night ccc - + + - - + + GC8085-13C; dihalide C6 methylsulfonamidephenyl suzuki; F5-9; CDCl3; 400MHz ADC reported overflow
45 19:58:16 250326-ccc 2 1H ccc + + + + + + + GC8085; dihalide C6 methylsulfonamidephenyl suzuki; F5-9; CDCl3; 400MHz
44 19:50:42 250326-ccc 5 1H ccc + + + + + + + GC8091; C6 6-quinoline/5-Br 4-pyr suzuki; crude; CDCl3; 400MHz
43 19:41:26 250326-jsm 4 1H jsm + + + + + + + JM305z
42 19:32:00 250326-jsm 3 1H jsm + + + + + + + JM305y
41 19:24:17 250326-ogc 4 1H ogc + + + + + + + OG8031, K12 gem KSAc sub scale up F6-10, CDCl3
40 19:11:54 250326-jlt 1 1H jlt + + + + + + + JT-P5J5-05A-b-fb-D2Os
39 19:01:07 250326-ccc 1 1H ccc + + + + + + + GC8085; dihalide C6 methylsulfonamidephenyl suzuki; F4; CDCl3; 400MHz
38 18:51:38 250326-jnn 9 19F{1H} jnn - + + - - + + JAN-209.1
38 18:42:41 250326-jnn 8 19F jnn - + + - - + + JAN-209.1
38 18:31:00 250326-jnn 7 1H jnn + + + + + + + JAN-209.1
37 18:21:26 250326-jnn 6 19F{1H} jnn - + + - - + + JAN-207.1
37 18:12:52 250326-jnn 5 19F jnn - x + - - + + JAN-207.1 ATM Failed
37 18:00:31 250326-jnn 4 1H jnn + + + + + + + JAN-207.1
36 17:50:46 250326-ogc 3 1H ogc + + + + + + + OG8025, K12 gem cycl 10 mg F6-10, CDCl3
35 17:37:07 250326-zhz 3 1H13C.hmbc zhz - + + - - + + ZZ-101-1
35 17:18:56 250326-zhz 2 1H13C.hsqc.aded zhz - x + - - + + ZZ-101-1 ATM Failed
35 17:08:30 250326-zhz 1 1H zhz + + + + + + + ZZ-101-1
34 17:00:18 250326-z5455435 3 1H z5455435 + + + + + + + C83 Amine after Hexane Slurry
33 16:49:24 250326-z5455435 2 1H z5455435 + + + + + + + C83 Amine after Hexane Slurry
32 16:42:28 250326-z5289573 2 1H z5289573 + + + + + + + JL146 3h
31 16:35:11 250326-z5289573 1 1H z5289573 + + + + + + + JL146 0h
30 16:25:46 250326-tat 2 1H tat + + + + + + + X5-1
29 16:16:31 250326-tat 1 1H tat + + + + + + + X4-1
28 16:08:37 250326-z5451239 1 1H z5451239 + + + + + + + thiourea 2 carbon-nh2
27 15:59:44 250326-ogc 2 1H ogc + + + + + + + OG8031, K12 gem KSAc sub 200 mg crude, CDCl3
26 15:48:53 250326-ogc 1 1H ogc + + + + + + + OG8029, CAALS ester reduction crude, CDCl3
25 15:41:01 250326-z5550254 1 1H z5550254 + + + + + + + AY-011
24 15:33:41 250326-yfo 2 1H yfo + + + + + + + df30 1345
23 15:25:43 250326-yfo 1 1H yfo + + + + + + + df30 1245
22 15:17:47 250326-z5492576 1 1H z5492576 + + + + + + + ZA-02-34-cdcl3
21 15:10:49 250326-z5426952 2 1H z5426952 + + + + + + + RI-D-88 F2R
20 15:03:45 250326-z5426952 1 1H z5426952 + x + + + + + RI-D-88 F1R ATM Failed
19 14:52:23 250326-sub 3 1H sub + + + + + + + SB145-E residue acetone
18 14:42:30 250326-sub 2 1H sub + + + + + + + SB145-E filtrate after evaporating tol CDCl3
17 14:35:03 250326-sub 1 1H sub + + + + + + + SB100-H DPND-7 Br CDCl3
16 14:28:04 250326-z5226398 1 1H z5226398 + + + + + + + yulin sample with curcumin
15 14:24:38 250326-z5489717 4 19F z5489717 - x + - - + + DSM-R222-overnight-direct CDCl3 ATM Failed
15 14:17:28 250326-z5489717 3 1H z5489717 + + + + + + + DSM-R222-overnight-direct CDCl3
14 14:12:32 250326-z5489717 2 19F z5489717 - + + - - + + DSM-R221-overnight-EtOAc ext. CDCl3
14 14:06:06 250326-z5489717 1 1H z5489717 + + + + + + + DSM-R221-overnight-EtOAc ext. CDCl3
13 13:51:14 250326-z5363218 10 1H13C.hmbc z5363218 - + + - - + + CDO-3.2
13 13:31:47 250326-z5363218 9 1H13C.hsqc.aded z5363218 - + + - - + + CDO-3.2
13 13:18:46 250326-z5363218 8 13C.day z5363218 - + + - - + + CDO-3.2
13 13:12:06 250326-z5363218 7 1H z5363218 + + + + + + + CDO-3.2
12 12:58:08 250326-z5363218 6 1H13C.hmbc z5363218 - + + - - + + CDO-3.1
12 12:39:19 250326-z5363218 5 1H13C.hsqc.aded z5363218 - + + - - + + CDO-3.1
12 12:25:59 250326-z5363218 4 13C.day z5363218 - + + - - + + CDO-3.1 ADC reported overflow
12 12:18:40 250326-z5363218 3 1H z5363218 + + + + + + + CDO-3.1
11 12:09:20 250326-iconnmr 5 sst.31P.sen iconnmr + + + + + + + 31P Sensitivity 0.0485 M triphenylphosphate (TPP) in d6-acetone Specification result of sinocal: Best sino value found ( > 150:1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/5/pdata/1/250326-iconnmr_5_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/5/pdata/1/250326-iconnmr_5_1.pdf Check for printing system problems
10 11:56:43 250326-iconnmr 4 sst.19F.qnp.sen iconnmr + + + + + + + 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found ( > 250 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/4/pdata/1/250326-iconnmr_4_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/4/pdata/1/250326-iconnmr_4_1.pdf Check for printing system problems
9 11:30:42 250326-iconnmr 3 sst.13C.sen iconnmr + x + + + + + 13C Sensitivity 10% Ethylbenzene (EB) in CDCl3 Specification result of sinocal: Best sino value found ( > 200 :1) ATM Failed, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/3/pdata/1/250326-iconnmr_3_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/3/pdata/1/250326-iconnmr_3_1.pdf Check for printing system problems
8 11:20:09 250326-iconnmr 2 sst.1H.sen iconnmr + x + + + + + 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found ( > 300 :1) ATM Failed, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/2/pdata/1/250326-iconnmr_2_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/2/pdata/1/250326-iconnmr_2_1.pdf Check for printing system problems
7 11:10:52 250326-iconnmr 1 sst.1H.lsh iconnmr + + + + + + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/1/pdata/1/250326-iconnmr_1_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250326-iconnmr/1/pdata/1/250326-iconnmr_1_1.pdf Check for printing system problems
6 11:02:24 250326-jnn 3 19F{1H} jnn - x + - - + + JAN-209.1 ATM Failed
6 10:52:50 250326-jnn 2 19F jnn - + + - - + + JAN-209.1
6 10:41:46 250326-jnn 1 1H jnn + + + + + + + JAN-209.1
5 09:52:10 250326-z5358936 1 1H z5358936 + + + + + + + Adipate crude Automation was stopped by user
4 09:41:58 250326-z5512706 2 1H z5512706 + + + + + + + AK38
3 09:31:08 250326-z5512706 1 1H z5512706 + + + + + + + AK37
2 09:15:10 250326-z5363218 2 1H z5363218 + + + + + + + CDO-3-C2
1 09:06:19 250326-z5363218 1 1H z5363218 + + + + + + + CDO-3-C1
47 04:53:31 250326-jsm 2 13C.day jsm - x + - - + + suj-03 CF3 purified ATM Failed
47 04:43:18 250326-jsm 1 1H jsm + + + + + + + suj-03 CF3 purified
1 01:57:47 250325-z3545554 1 1H z3545554 + + + + + + +
46 01:48:37 250326-z5455435 1 1H z5455435 + + + + + + + C83 Amine
45 01:35:42 250325-yab 4 13C.day yab - + + - - + + TAT_II-SPOT
45 01:28:43 250325-yab 3 1H yab + + + + + + + TAT_II-SPOT
44 01:18:36 250325-sub 4 1H sub + + + + + + + SB145-E aliquot 2 protection of aldehyde on imidazole-2-CHO D2O
43 01:07:57 250325-sub 3 1H sub + + + + + + + SB145-E aliquot 2 protection of aldehyde on imidazole-2-CHO CDCl3
42 00:59:08 250325-sub 2 1H sub + x + + + + + 2-formyl indole CDCl3 ATM Failed
41 00:33:39 250325-jsm 3 13C.day jsm - + + - - + + JM307 (BMIDA ethynylbenzene) ADC reported overflow
41 00:31:07 250325-jsm 2 11B jsm - x + - - + + JM307 (BMIDA ethynylbenzene) ATM Failed
41 00:24:24 250325-jsm 1 1H jsm + + + + + + + JM307 (BMIDA ethynylbenzene)
40 00:11:31 250325-thh 2 13C.day thh - + + - - + + TB-200 ADC reported overflow
40 00:04:19 250325-thh 1 1H thh + + + + + + + TB-200
39 23:50:08 250325-z5676313 5 13C.day z5676313 - + + - - + + AB-18-crude
39 23:44:58 250325-z5676313 4 11B z5676313 - + + - - + + AB-18-crude
39 23:29:56 250325-z5676313 3 1H z5676313 + + + + x + + AB-18-crude Shim failed
38 23:26:40 250325-z5676313 2 11B z5676313 - + + - - + + AB-16
38 23:18:45 250325-z5676313 1 1H z5676313 + + + + + + + AB-16
37 23:05:32 250325-yab 2 13C.day yab - x + - - + + TAT_I-SPOT ATM Failed
37 22:58:43 250325-yab 1 1H yab + + + + + + + TAT_I-SPOT
36 22:51:20 250325-ccc 3 1H ccc + + + + + + + GC8087; pyrimidine methine mannich; crude; CDCl3; 400MHz
35 22:42:47 250325-ccc 2 1H ccc + + + + + + + GC8085; dihalide C6 methylsulfonamidephenyl suzuki; crude; CDCl3; 400MHz
34 21:30:37 250325-dem 3 1H dem + + + + + + + DM-MS-02-76E
33 20:18:17 250325-dem 2 1H dem + + + + + + + DM-MS-02-76D
32 19:07:34 250325-dem 1 1H dem + + + + + + + DM-MS-02-76A
31 18:58:26 250325-zhz 1 1H zhz + + + + + + + ZZ-101 normal workup
30 18:48:35 250325-jnn 3 19F{1H} jnn - + + - - + + JAN-207.1
30 18:35:26 250325-jnn 2 19F jnn - + + - - + + JAN-207.1
30 18:24:25 250325-jnn 1 1H jnn + + + + + + + JAN-207.1
29 17:15:57 250325-z5550254 4 13C.night z5550254 + + + + + + + AY-033 ADC reported overflow
28 17:06:27 250325-z5426952 4 1H z5426952 + + + + + + + RI-90 crude
27 16:56:36 250325-z5426952 3 1H z5426952 + + + + + + + RI-89 crude
26 16:49:47 250325-z5426952 2 1H z5426952 + + + + + + + RI-D-88 Fl
25 16:42:47 250325-z5426952 1 1H z5426952 + + + + + + + RI-D-88 F'
24 16:29:03 250325-nnt 2 13C.day nnt - + + - - + + ADC reported overflow
24 16:22:10 250325-nnt 1 1H nnt + + + + + + +
23 16:16:11 250325-z5550254 3 19F{1H} z5550254 - + + - - + + AY-065
23 16:09:38 250325-z5550254 2 19F z5550254 - + + - - + + AY-065
23 15:59:24 250325-z5550254 1 1H z5550254 + + + + + + + AY-065
22 15:52:47 250325-z5455435 1 1H z5455435 + x + + + + + C83 Phthalimide N-alkylation ATM Failed
21 15:42:15 250325-sub 1 1H sub + + + + + + + SB144-E aliquot 1 CDCl3
20 15:37:37 250325-z5564533 4 19F{1H} z5564533 - + + - - + + CM-065-2
20 15:30:01 250325-z5564533 2 19F z5564533 + + + + + + + CM-065-2
19 15:25:31 250325-z5564533 3 19F{1H} z5564533 - + + - - + + CM-065-1
19 15:16:09 250325-z5564533 1 19F z5564533 + + + + + + + CM-065-1
18 15:06:31 250325-z3541685 3 1H z3541685 + + + + + + + MWB_04_042b red fraction
17 14:59:06 250325-z3541685 2 1H z3541685 + + + + + + + MWB_04_042a green fraction
16 14:51:16 250325-z3541685 1 1H z3541685 + + + + + + + MWB_04_037a NODIPS-Acet
15 14:43:49 250325-z5492576 1 1H z5492576 + + + + + + + ZA-Nitroso_New-CDCl3
14 14:39:29 250325-z5489717 8 19F z5489717 - + + - - + + DSM-R221-direct-filt.
14 14:32:39 250325-z5489717 7 1H z5489717 + + + + + + + DSM-R221-direct-filt.
13 14:28:31 250325-z5489717 6 19F z5489717 - + + - - + + DSM-R220-3h-direct
13 14:22:04 250325-z5489717 5 1H z5489717 + + + + + + + DSM-R220-3h-direct
12 14:14:54 250325-z5489717 4 1H z5489717 + + + + + + + DSM-NitroSM purity check
11 14:04:57 250325-vkk 1 1H vkk + + + + + + + VKK-III-03
10 13:57:28 250325-ccc 1 1H ccc + + + + + + + GC8049; pyrimidine carboxaldehyde; check; CDCl3; 400MHz
9 13:05:49 250325-amn 2 1H amn + + + + + + + AMM - H-008 - NiTMP after HighVac in tol-d8
8 11:52:24 250325-z5165127 3 1H z5165127 + x + + + + + Ph - CDCl3 ATM Failed
7 11:46:03 250325-z5165127 2 1H z5165127 + + + + + + + 4-Me - CDCl3
6 11:37:41 250325-z5165127 1 1H z5165127 + + + + + + + Pyridine - CDCl3
5 11:10:03 250325-z5489717 3 19F z5489717 - + + - - + + DSM-R220-heat 10min crude-direct CDCl3
5 11:02:33 250325-z5489717 2 1H z5489717 + + + + + + + DSM-R220-heat 10min crude-direct CDCl3
4 10:56:16 250325-z5489717 1 1H z5489717 + + + + + + + DSM-Chalcone purity check CDCl3
3 10:35:50 250325-ild 2 1H ild + + + + + + + ID12043; boc deprot QA2; CDCl3
2 10:27:35 250325-ild 1 1H ild + + + + + + + ID12041; hydrolysis scale up/; DMSO
1 09:08:49 250325-z5438782 1 1H z5438782 + + + + + + + bzlp after purifying
22 08:25:42 250325-z5628481 2 1H13C.hsqc.aded z5628481 - x + - - + + me-03 HSQC ATM Failed
22 08:16:18 250325-z5628481 1 1H z5628481 + + + + + + + me-03 1H
42 22:15:30 250324-rdr 4 1H rdr + + + + + + + 2-018 4nitro bottom spot ADC reported overflow
41 21:07:06 250324-rdr 3 1H rdr + x + + + + + 2-018 4Nitro recolumn ATM Failed
40 21:00:07 250324-z3545554 2 1H z3545554 + + + + + + +
21 20:47:50 250324-jlt 2 1H jlt + + + + + + + JT-P5J5-05B-b-fb-D2Os
20 20:35:17 250324-jlt 1 1H jlt + + + + + + + JT-P5J5-05A-b-fb-D2Os
19 20:27:24 250324-ccc 2 1H ccc + + + + + + + GC8083; C5 aminopyrimidine isopropyl amination; crude; CDCl3; 400MHz
18 18:20:25 250324-ccc 3 13C.night ccc - + + - - + + GC8081-13C; dihalide C6 4-cyanophenyl suzuki; F7-13; CDCl3; 400MHz
18 18:13:32 250324-ccc 1 1H ccc + + + + + + + GC8081; dihalide C6 4-cyanophenyl suzuki; F7-13; CDCl3; 400MHz
17 18:01:35 250324-nap 1 1H nap + + + + + + + 111b
16 17:54:46 250324-z5289573 1 1H z5289573 + + + + + + + JL140
15 17:47:04 250324-yfo 5 1H yfo + + + + + + + df26 m
14 17:39:36 250324-yfo 4 1H yfo + + + + + + + df28 m
13 17:32:00 250324-yfo 3 1H yfo + + + + + + + df30 11 15 m
12 17:24:41 250324-yfo 2 1H yfo + + + + + + + df30 11 45 m
11 17:16:35 250324-yfo 1 1H yfo + + + + + + + df21 m
9 17:08:49 250324-djg 2 1H djg + + + + + + + DJG-B-148 LiAlH4 red - crude EtAc off plug
8 16:59:28 250324-djg 1 1H djg + + + + + + + DJG-B-148 LiAlH4 red - crude DCM off plug
7 16:52:50 250324-z5426952 5 1H z5426952 + + + + + + + RI-88 F5
6 16:46:00 250324-z5426952 4 1H z5426952 + + + + + + + RI-88 F4
5 16:38:49 250324-z5426952 3 1H z5426952 + + + + + + + RI-88 F3
4 16:31:42 250324-z5426952 2 1H z5426952 + + + + + + + RI-88 F2
3 16:25:02 250324-z5426952 1 1H z5426952 + + + + + + + RI-88 F1
2 16:10:19 250324-mda 2 1H mda + + + + + + + Cina-DM
1 15:59:05 250324-mda 1 1H mda + + + + + + + Cina-CD
28 15:19:54 250324-z5532358 2 11B z5532358 - + + - - + + white powder from chloroform rinse
28 15:12:19 250324-z5532358 1 1H z5532358 + + + + + + + white powder from chloroform rinse
27 15:06:09 250324-kee 2 1H kee + + + + + + + Dioxane chain extension 8h
26 14:58:59 250324-kee 1 1H kee + + + + + + + BA chain extension 8h
25 14:52:23 250324-rdr 2 1H rdr + + + + + + + 2-018 4Bpin hexane washed orange
24 14:43:15 250324-rdr 1 1H rdr + + + + + + + 2-018 4Bpin hexane washed purple
23 13:57:59 250324-lit 2 1H lit + + + + + + + Jenny-polymer2, CDCl3
22 13:49:26 250324-lit 1 1H lit + + + + + + + Jenny-polymer1, CDCl3
21 13:41:29 250324-z5564533 1 1H z5564533 + + + + + + + CM-064-1
20 13:30:19 250324-sub 3 1H sub + + + + + + + SB144-D CF3 Imidazole-CHO Buli CDCl3
19 13:19:24 250324-sub 2 1H sub + + + + + + + SB144-D CF2 Imidazole-CHO Buli CDCl3
18 13:07:06 250324-sub 1 1H sub + + + + + + + SB144-D CF1 Imidazole-CHO Buli CDCl3
3 12:57:42 250324-amn 1 1H amn + + + + + + + AMM - H007 - H2TMP after Recryst in CDCl3 - 1% pyr-d5
2 12:51:35 250324-z3544630 2 1H z3544630 + + + + + + + TE-FBTZ-CO2-2-CDCl3
1 12:42:46 250324-z3544630 1 1H z3544630 + + + + + + + TE-BTZ-CO2-2-CDCl3
17 12:27:31 250324-z5550254 1 1H z5550254 + + + + + + + AY-021.crude
16 11:49:53 250324-z5628481 2 19F{1H} z5628481 - x + - - + + dichloro meo-02 sn2 test 19F ATM Failed
16 11:43:29 250324-z5628481 1 1H z5628481 + + + + + + + dichloro meo-02 sn2 test 1H
15 11:22:57 250324-z5363218 4 1H.cosy z5363218 - + + - - + + CDO-3.2
15 11:16:15 250324-z5363218 3 1H z5363218 + x + + + + + CDO-3.2 ATM Failed
14 11:04:51 250324-z5363218 2 1H.cosy z5363218 - + + - - + + CDO-3.1
14 10:53:51 250324-z5363218 1 1H z5363218 + + + + + + + CDO-3.1
13 10:20:03 250324-vkk 3 1H vkk + + + + + + + VKK-III-02 without RAFT
12 10:13:09 250324-vkk 2 1H vkk + + + + + + + VKK-III-01 with RAFT
11 10:06:59 250324-vkk 1 1H vkk + x + + + + + VKK-III-pure PHB ATM Failed
10 09:53:23 250324-z3545554 1 1H z3545554 + + + + + + +
50 22:49:49 250323-z3545554 1 1H z3545554 x - - - - - - Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 50
37 22:42:37 250323-yab 1 1H yab + + + + + + + T3_Bn_crude
36 22:41:59 250322-jsm 8 11B jsm x - - - - - - Nhan compound 4Cl Ph alkenyl Bpin check to see if it decomposed Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 36
34 22:41:05 250322-jsm 11 13C.day jsm x - - - - - - JM311 test 1 (Fac-Ir(ppy)3 cat + 4-Cl Ph alkenyl Bpin + diphenylacetylene approx 18h) Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 34
28 21:36:31 250323-z3544630 7 13C.night z3544630 - + + - - + + TE-FBTZ-CO2 + CDCl3
28 21:29:12 250323-z3544630 5 1H z3544630 + + + + + + + TE-FBTZ-CO2 + CDCl3
27 20:25:32 250323-z3544630 6 13C.night z3544630 - x + - - + + TE-BTZ-CO2 + CDCl3 ATM Failed
27 20:19:15 250323-z3544630 4 1H z3544630 + + + + + + + TE-BTZ-CO2 + CDCl3
26 20:13:01 250323-z3544630 3 1H z3544630 + + + + + + + FBTZ Mono + CDCl3
25 20:06:37 250323-z3544630 2 1H z3544630 + + + + + + + BTZ Mono + CDCl3
24 19:59:20 250323-z3544630 1 1H z3544630 + + + + + + + TE Mono + CDCl3
28 18:42:50 250323-z3544630 7 13C.night z3544630 - x + - - x - TE-FBTZ-CO2 + CDCl3 ATM Failed, Acquisition Failed, Automation was stopped by user
28 18:32:26 250323-z3544630 5 1H z3544630 + x + + x x - TE-FBTZ-CO2 + CDCl3 ATM Failed, Shim failed, Acquisition Failed
27 18:29:50 250323-z3544630 6 13C.night z3544630 - x + - - x - TE-BTZ-CO2 + CDCl3 ATM Failed, Acquisition Failed
27 18:19:21 250323-z3544630 4 1H z3544630 + x + + x x - TE-BTZ-CO2 + CDCl3 ATM Failed, Shim failed, Acquisition Failed
26 18:08:51 250323-z3544630 3 1H z3544630 + x + + x x - FBTZ Mono + CDCl3 ATM Failed, Shim failed, Acquisition Failed
25 17:58:27 250323-z3544630 2 1H z3544630 + x + + x x - BTZ Mono + CDCl3 ATM Failed, Shim failed, Acquisition Failed
24 17:46:22 250323-z3544630 1 1H z3544630 + x + + x x - TE Mono + CDCl3 ATM Failed, Shim failed, Acquisition Failed
50 16:18:07 250323-z3545554 2 13C.day z3545554 + x + + x x - ATM Failed, Shim failed, Acquisition Failed
37 14:03:33 250323-yab 1 1H yab + x + + x x - T3_Bn_crude ATM Failed, Shim failed, Acquisition Failed
34 02:23:10 250322-jsm 11 13C.day jsm + x + + x x - JM311 test 1 (Fac-Ir(ppy)3 cat + 4-Cl Ph alkenyl Bpin + diphenylacetylene approx 18h) ATM Failed, Shim failed, Acquisition Failed
36 02:19:57 250322-jsm 10 13C.day jsm - x + - - x - Nhan compound 4Cl Ph alkenyl Bpin check to see if it decomposed ATM Failed, Acquisition Failed
36 02:09:27 250322-jsm 9 11B jsm + x + + x x - Nhan compound 4Cl Ph alkenyl Bpin check to see if it decomposed ATM Failed, Shim failed, RGA Failed, Acquisition Failed
36 21:57:13 250322-jsm 8 11B jsm - x + - - x - Nhan compound 4Cl Ph alkenyl Bpin check to see if it decomposed ATM Failed, RGA Failed, Acquisition Failed
36 21:48:13 250322-jsm 7 1H jsm + + + + + + + Nhan compound 4Cl Ph alkenyl Bpin check to see if it decomposed
35 21:34:59 250322-jsm 6 13C.day jsm - + + - - + + JM311 test 2 (Fac-Ir(ppy)3 cat + 4-Cl Ph alkenyl Bpin + p-tolualdehyde approx 18h) ADC reported overflow
35 21:28:13 250322-jsm 5 11B jsm - + + - - + + JM311 test 2 (Fac-Ir(ppy)3 cat + 4-Cl Ph alkenyl Bpin + p-tolualdehyde approx 18h)
35 21:19:31 250322-jsm 4 1H jsm + + + + + + + JM311 test 2 (Fac-Ir(ppy)3 cat + 4-Cl Ph alkenyl Bpin + p-tolualdehyde approx 18h)
34 21:06:21 250322-jsm 3 13C.day jsm - x + - - + + JM311 test 1 (Fac-Ir(ppy)3 cat + 4-Cl Ph alkenyl Bpin + diphenylacetylene approx 18h) ATM Failed
34 20:59:46 250322-jsm 2 11B jsm - + + - - + + JM311 test 1 (Fac-Ir(ppy)3 cat + 4-Cl Ph alkenyl Bpin + diphenylacetylene approx 18h)
34 20:50:38 250322-jsm 1 1H jsm + + + + + + + JM311 test 1 (Fac-Ir(ppy)3 cat + 4-Cl Ph alkenyl Bpin + diphenylacetylene approx 18h)
32 16:27:52 250322-thh 10 1H thh + x + + + + + B80-4-09 ATM Failed
31 16:18:54 250322-thh 9 1H thh + + + + + + + B80-4-10
30 16:11:00 250322-thh 8 1H thh + + + + + + + B80-4-11
29 16:02:43 250322-thh 7 1H thh + + + + + + + B80-4-12
28 15:52:27 250322-thh 6 1H thh + + + + + + + B80-4-13
27 15:43:00 250322-thh 5 1H thh + + + + + + + B80-4-14
26 15:32:59 250322-thh 4 1H thh + + + + + + + B80-4-15
25 15:25:18 250322-thh 3 1H thh + + + + + + + B80-4-16
24 15:20:28 250322-thh 2 1H thh - x + - - + + B80-4-17 ATM Failed
24 15:13:08 250322-thh 1 1H thh + + + + + + + B80-4-17
23 14:53:38 250322-z5537965 1 1H z5537965 + + + + + + + LH_200mg_Post deprotection_19.3.25
22 10:02:11 250321-z3544630 6 13C.night z3544630 - + + - - + + pp-i2-12
22 09:43:21 250321-z3544630 5 1H z3544630 + + + + + + + pp-i2-12
21 08:39:37 250321-jlt 15 13C.night jlt - x + - - + + JT-P5J5-05B-b-fb ATM Failed, ADC reported overflow
21 08:33:47 250321-jlt 14 19F{1H} jlt - + + - - + + JT-P5J5-05B-b-fb
21 08:24:03 250321-jlt 13 1H jlt + + + + + + + JT-P5J5-05B-b-fb
20 07:18:59 250321-jlt 12 13C.night jlt - + + - - + + JT-P5J5-05A-b-fb
20 07:12:51 250321-jlt 11 19F{1H} jlt - + + - - + + JT-P5J5-05A-b-fb
20 07:04:28 250321-jlt 10 1H jlt + x + + + + + JT-P5J5-05A-b-fb ATM Failed
19 05:59:40 250321-jlt 9 13C.night jlt - + + - - + + JT-P5JR-04E-col-2ndspot
19 05:55:44 250321-jlt 8 19F{1H} jlt - x + - - + + JT-P5JR-04E-col-2ndspot ATM Failed
19 05:44:39 250321-jlt 7 1H.cosy jlt - + + - - + + JT-P5JR-04E-col-2ndspot
19 05:33:40 250321-jlt 6 1H jlt + + + + + + + JT-P5JR-04E-col-2ndspot
18 04:23:59 250321-jlt 5 13C.night jlt - + + - - + + JT-P5JR-04D-col ADC reported overflow
18 04:18:21 250321-jlt 4 19F{1H} jlt - + + - - + + JT-P5JR-04D-col
18 04:06:54 250321-jlt 3 1H.cosy jlt - + + - - + + JT-P5JR-04D-col
18 03:57:48 250321-jlt 2 1H jlt + x + + + + + JT-P5JR-04D-col ATM Failed
17 03:48:04 250321-jlt 1 1H jlt + + + + + + + JT-P5J5-01g-BP
16 02:44:15 250321-z3544630 4 13C.night z3544630 - x + - - + + pp-i2-9 ATM Failed
16 02:31:20 250321-z3544630 3 1H z3544630 + + + + + + + pp-i2-9 ADC reported overflow
15 01:25:39 250321-z3544630 2 13C.night z3544630 - + + - - + + pp-i2-6h ADC reported overflow
15 01:09:44 250321-z3544630 1 1H z3544630 + + + + + + + pp-i2-6h
11 00:57:24 250321-sub 4 1H sub + + + + + + + SB147 org layer afetr EtOAc wash CDCl3
10 00:46:25 250321-zhz 4 1H zhz + + + + + + + ZZ-102 crude
9 00:36:05 250321-amn 1 1H amn + + + + + + + AMM - H007 in tol-d8 - Main fraction after plug - 32 scans - changed colour during transit (could decompose before NMR is run successfully)
8 00:26:18 250321-jnn 7 19F{1H} jnn - + + - - + + JAN-208.1
8 00:15:38 250321-jnn 6 19F jnn - + + - - + + JAN-208.1
8 00:01:12 250321-jnn 5 1H13C.hmbc jnn - + + - - + + JAN-208.1
8 23:42:24 250321-jnn 4 1H13C.hsqc.aded jnn - + + - - + + JAN-208.1
8 23:31:22 250321-jnn 3 1H.cosy jnn - + + - - + + JAN-208.1
8 21:24:41 250321-jnn 2 13C.night jnn - + + - - + + JAN-208.1
8 21:08:45 250321-jnn 1 1H jnn + + + + + + + JAN-208.1
7 20:03:21 250321-z5676313 3 13C.night z5676313 - x + - - + + AB-11-a ATM Failed
7 19:57:20 250321-z5676313 2 11B z5676313 - + + - - + + AB-11-a
7 19:47:57 250321-z5676313 1 1H z5676313 + + + + + + + AB-11-a
6 18:44:01 250321-z5550254 14 13C.night z5550254 - x + - - + + AY-071.1 ATM Failed, ADC reported overflow
6 18:30:00 250321-z5550254 13 1H z5550254 + + + + + + + AY-071.1
5 18:20:36 250321-z5550254 12 19F{1H} z5550254 - + + - - + + AY-072.3
5 18:11:23 250321-z5550254 11 19F z5550254 - + + - - + + AY-072.3
5 17:58:09 250321-z5550254 10 1H z5550254 + x + + + + + AY-072.3 ATM Failed
4 17:47:48 250321-z5550254 9 19F{1H} z5550254 - x + - - + + AY-072.2 ATM Failed
4 17:39:40 250321-z5550254 8 19F z5550254 - x + - - + + AY-072.2 ATM Failed
4 17:26:09 250321-z5550254 7 1H z5550254 + + + + + + + AY-072.2
3 17:16:34 250321-z5550254 6 19F{1H} z5550254 - + + - - + + AY-072.1
3 17:08:27 250321-z5550254 5 19F z5550254 - x + - - + + AY-072.1 ATM Failed
3 16:53:53 250321-z5550254 4 1H z5550254 + + + + + + + AY-072.1
2 16:41:28 250321-ild 1 1H ild + + + + + + + ID12039; nitrile hydrolysis cr; DMSO
1 16:25:37 250321-z5489717 1 1H z5489717 + + + + + + + DSM-R219-crude-driect CDCl3
55 15:54:29 250321-ccc 2 1H ccc + + + + + + + GC8071; aminopyrimidine isopropylamine SNAr; F35-45; CDCl3; 400MHz
54 15:43:41 250321-ccc 1 1H ccc + + + + + + + GC8081; dihalide C6 cyanophenyl suzuki; crude; CDCl3; 400MHz
53 15:25:07 250321-z5537965 1 1H z5537965 + + + + + + + LH_300mg_post deprotection_18.3.25
52 15:14:11 250321-zhz 3 1H zhz + + + + + + + ZZ-099 overtime base-soluble very fluorescent
51 15:03:40 250321-zhz 2 1H zhz + + + + + + + ZZ-101 F7-10
50 14:52:43 250321-zhz 1 1H zhz + + + + + + + ZZ-101 repeat
49 14:38:43 250321-nap 1 1H nap + x + + + + + 112e-standard ATM Failed
48 14:27:54 250321-z5438782 2 1H z5438782 + + + + + + + 470nm 5k elp 24h
47 14:20:50 250321-suj 1 1H suj + + + + + + + ss-25-03 crude o.n. a/workup repeat rxn
46 14:12:59 250321-rdr 2 1H rdr + + + + + + + 2-018 4Bpin orange
45 14:05:27 250321-rdr 1 1H rdr + + + + + + + 2-018 4Bpin Purple
44 13:56:47 250321-thh 7 1H thh + + + + + + + B80-4-08
43 13:47:36 250321-thh 6 1H thh + + + + + + + B80-4-07
42 13:37:28 250321-thh 5 1H thh + + + + + + + B80-4-06
41 13:28:24 250321-thh 4 1H thh + + + + + + + B80-4-05
40 13:18:06 250321-thh 3 1H thh + + + + + + + B80-4-04
39 13:09:13 250321-thh 2 1H thh + + + + + + + B80-4-02
38 13:01:02 250321-thh 1 1H thh + + + + + + + B80-4-01
37 12:53:12 250321-sub 3 1H sub + + + + + + + SB147 org layer after EtOAc wash protecting aldehyde on imidazole CDCl3
36 12:43:46 250321-sub 2 1H sub + + + + + + + SB-SFD-1B green spot DPND-7 dimer with Ph spacer CDCl3
35 12:34:58 250321-sub 1 1H sub + + + + + + + SB-SFD-1B CF4 (rest portions of CF2) DPND-7 dimer with Ph spacer CDCl3
34 11:55:42 250321-z5363218 2 1H z5363218 + + + + + + + CDO3.2
33 11:47:19 250321-z5363218 1 1H z5363218 + + + + + + + CDO-3.1
32 11:40:41 250321-z5426952 1 1H z5426952 + + + + x + + RI-85 F2 Shim failed
31 11:31:59 250321-z5167506 2 1H z5167506 + + + + + + + PDMAPAA PBuA PGlu6 T20 CDCl3
30 11:20:41 250321-z5167506 1 1H z5167506 + + + + + + + PDMAPAA PBuA PGlu6 T0 CDCl3
27 10:18:57 250321-z5628481 2 19F{1H} z5628481 - + + - - + + dichloro sn2 test 19F
27 10:12:01 250321-z5628481 1 1H z5628481 + + + + + + + dichloro sn2 test 1H
29 10:01:03 250321-z5438782 1 1H z5438782 + + + + + + + bzlp after drying
28 09:53:43 250321-z5605300 2 1H z5605300 + + + + + + + PTS-pyrrole-purtiycheck
27 09:47:15 250321-z5550254 3 19F{1H} z5550254 - + + - - + + AY-072.1
27 09:41:09 250321-z5550254 2 19F z5550254 - + + - - + + AY-072.1
27 09:25:37 250321-z5550254 1 1H z5550254 + + + + + + + AY-072.1
26 00:44:32 250320-z5676313 4 13C.day z5676313 - + + - - + + AB-10-crude2
26 00:41:19 250320-z5676313 3 11B z5676313 - + + - - + + AB-10-crude2
26 00:33:23 250320-z5676313 2 1H z5676313 + + + + + + + AB-10-crude2
25 00:11:00 250320-nap 6 13C.day nap - + + - - + + 112e-column ADC reported overflow
25 00:03:25 250320-nap 5 1H nap + + + + + + + 112e-column
24 23:54:16 250320-mda 2 1H mda + + + + + + + Crosslinker DM
23 23:44:16 250320-mda 1 1H mda + + + + + + + Crosslinker
22 23:36:39 250320-z5537965 2 1H z5537965 + + + + + + + LH_200mg_19.3.25_post poly
21 23:28:05 250320-z5489717 3 1H z5489717 + + + + + + + DSM-R214-ppt. (N,O)? CDCl3
20 22:22:54 250320-jlt 4 13C.night jlt - + + - - + + JT-2M2MPA-step2-filt-D2Os
20 22:13:00 250320-jlt 3 1H jlt + + + + + + + JT-2M2MPA-step2-filt-D2Os
19 22:07:08 250320-jlt 2 19F{1H} jlt - + + - - + + JT-WJ-suzuki
19 21:57:01 250320-jlt 1 1H jlt + x + + + + + JT-WJ-suzuki ATM Failed
18 19:50:08 250320-ccc 2 13C.night ccc - + + - - + + GC8079-13C; dihalide C6 5-indole suzuki; F10-30; DMSO; 400MHz
18 19:42:42 250320-ccc 1 1H ccc + + + + + + + GC8079; dihalide C6 5-indole suzuki; F10-30; DMSO; 400MHz
17 19:33:05 250320-lit 2 1H lit + + + + + + + 25Batch-GTHQCy5-5M HCL-5h, D2O
16 19:22:42 250320-lit 1 1H lit + + + + + + + 30Batch-GTHQCy5-5M HCL-20h, D2O
15 19:10:00 250320-nap 4 13C.day nap - + + - - + + 111b-2
15 19:00:45 250320-nap 3 1H nap + + + + + + + 111b-2
14 18:47:33 250320-nap 2 13C.day nap - + + - - + + 111b-1
14 18:40:07 250320-nap 1 1H nap + + + + + + + 111b-1
13 18:36:41 250320-thh 6 1H thh - + + - - + + imine
13 18:27:00 250320-thh 5 1H thh + + + + + + + imine
12 18:14:03 250320-thh 4 13C.day thh - + + - - + + B80-2-10
12 18:07:05 250320-thh 3 1H thh + + + + + + + B80-2-10
11 17:53:52 250320-thh 2 13C.day thh - + + - - + + B80-2--09
11 17:47:31 250320-thh 1 1H thh + x + + + + + B80-2--09 ATM Failed
10 17:34:44 250320-zhz 1 1H zhz + + + + x + + ZZ-101 F1-2 Shim failed
9 17:28:21 250320-z5550254 7 19F{1H} z5550254 - + + - - + + AY-072.2
9 17:21:29 250320-z5550254 5 19F z5550254 - + + - - + + AY-072.2
9 17:06:27 250320-z5550254 4 1H z5550254 + x + + + + + AY-072.2 ATM Failed
8 17:00:01 250320-z5550254 6 19F{1H} z5550254 - + + - - + + AY-072.1
8 16:53:24 250320-z5550254 5 19F z5550254 - + + - - + + AY-072.1
8 16:38:07 250320-z5550254 3 1H z5550254 + + + + + + + AY-072.1
7 16:28:07 250320-z5550254 2 1H z5550254 + + + + + + + AY-071.1
6 16:17:12 250320-z5550254 1 1H z5550254 + + + + + + + AY-036.1
5 15:47:53 250320-iconnmr 3 bbfo.1H.qnmr iconnmr + + + + + + + AQA 20 10.00 mg in stock 675.58 mg (maleic acid 26.88 mg in 2629.48 mg D2O) 1H D2O
4 15:21:16 250320-iconnmr 2 bbfo.1H.qnmr iconnmr + + + + + + + AQA 20 5.70 mg in stock 669.84 mg (maleic acid 26.88 mg in 2629.48 mg D2O) 1H D2O
3 14:55:59 250320-iconnmr 1 bbfo.1H.qnmr iconnmr + + + + + + + AQA 20 D2O no IS 6.08 mg 670.30 mg
2 14:32:45 250320-z5537965 1 1H z5537965 + + + + + + + LH_200mg_19.3.25
1 14:11:39 250320-z5371131 3 1H z5371131 + + + + + + + AM5.01 more conc. 2
46 13:41:28 250320-kee 1 1H kee + + + + + + + elp-pure2
45 12:55:12 250320-yab 3 1H yab + + + + + + + TROPL_N+_NH_NaOAc
44 12:41:28 250320-yab 2 13C.day yab - + + - - + + 1E3_M+_TR ADC reported overflow
44 12:34:34 250320-yab 1 1H yab + + + + + + + 1E3_M+_TR
43 12:27:44 250320-z5371131 2 1H z5371131 + + + + + + + 5.01 column more conc.
42 12:21:10 250320-z5371131 1 1H z5371131 + + + + + + + 1.06-4 D2O exchange
41 12:14:21 250320-z3541685 1 1H z3541685 + + + + + + + MWB_04_039a
40 12:05:45 250320-sub 1 1H sub + + + + + + + SB100-G DPND-7 mono Br CDCl3
39 11:54:14 250320-z5438782 3 1H z5438782 + + + + + + + re 530 nm 72h
38 11:42:16 250320-z5438782 2 1H z5438782 + + + + + + + re 530nm 60h
37 11:31:45 250320-z5438782 1 1H z5438782 + + + + + + + bzlp
36 11:24:59 250320-suj 1 1H suj + + + + + + + ss-25-02 crude o.n. workup fresh grignard reagent
35 11:11:46 250320-dem 2 13C.day dem - + + - - + + DM-MS-02-68F_New
35 10:55:28 250320-dem 1 1H dem + + + + + + + DM-MS-02-68F_New
34 10:47:00 250320-z5167506 2 1H z5167506 + + + + + + + Glu6 T20 CDCl3
33 10:38:38 250320-z5167506 1 1H z5167506 + + + + + + + Glu6 T0 CDCl3
32 10:30:59 250320-z5363218 1 1H z5363218 + + + + + + + CDO-3-C
31 10:23:30 250320-z5489717 2 1H z5489717 + + + + + + + DSM-R217-overnight-crude-direct CDCl3
30 10:15:54 250320-z5489717 1 1H z5489717 + + + + + + + DSM-R216-overnight-crude-direct CDCl3
29 10:09:10 250320-z5358936 4 1H z5358936 + x + + + + + Fraction 8-11 ATM Failed
28 10:01:12 250320-z5358936 3 1H z5358936 + + + + + + + Fraction 6,7
27 09:53:39 250320-z5358936 2 1H z5358936 + + + + + + + Fraction 4,5
26 09:41:39 250320-z5358936 1 1H z5358936 + + + + + + + Fraction 3
25 09:26:22 250320-z5676313 1 13C.day z5676313 + x + + + + + AB-10-crude ATM Failed
24 09:18:44 250320-z5426952 2 1H z5426952 + + + + + + + RI-D-83
23 09:10:20 250320-z5426952 3 1H z5426952 + + + + + + + RI-D-82 Crude
22 09:03:56 250320-z5426952 1 1H z5426952 + + + + + + + RI-D-OH4-F2
21 08:52:08 250319-z3545554 2 1H z3545554 + + + + + + +
20 08:42:07 250319-z3545554 1 1H z3545554 + + + + + + +
13 08:34:03 250319-z5255867 2 1H z5255867 + + + + + + + JL-032 RS1
12 08:27:11 250319-z5255867 1 1H z5255867 + + + + + + + JL-031 RS3
11 08:18:49 250319-zhz 1 1H zhz + x + + + + + ZZ-101 F3-4 ATM Failed
10 08:11:45 250319-mda 2 1H mda + + + + + + + PEG 2K
9 08:04:17 250319-mda 1 1H mda + + + + + + + Repurified Poly CTA
8 07:59:43 250319-z5676313 2 11B z5676313 - x + - - + + AB-10-crude ATM Failed
8 07:49:56 250319-z5676313 1 1H z5676313 + + + + + + + AB-10-crude
7 07:41:13 250319-z5485590 3 1H z5485590 + + + + + + + T20-poly1
6 07:34:17 250319-z5485590 2 1H z5485590 + + + + + + + PEG-old
5 07:26:52 250319-z5485590 1 1H z5485590 + + + + + + + PEG-new
4 06:22:41 250319-law 4 13C.night law - + + - - + + LW-162-A2
4 06:14:45 250319-law 3 1H law + + + + + + + LW-162-A2
3 05:09:42 250319-law 2 13C.night law - + + - - + + JT-K1-03? ADC reported overflow
3 05:03:26 250319-law 1 1H law + + + + + + + JT-K1-03?
2 04:57:11 250319-jlt 2 19F{1H} jlt - + + - - + + JT-4F-MET-Step2
2 04:50:30 250319-jlt 1 1H jlt + x + + + + + JT-4F-MET-Step2 ATM Failed
1 03:45:57 250319-ogc 2 13C.night ogc - + + - - + + OG4107, K12 acid carbon, DMSO ADC reported overflow
1 03:38:05 250319-ogc 1 1H ogc + + + + + + + OG4107, K12 acid carbon, DMSO
60 02:10:12 250319-z5550254 10 13C.night z5550254 - + + - - + + AY-072.crude ADC reported overflow
60 02:01:48 250319-z5550254 9 19F{1H} z5550254 - x + - - + + AY-072.crude ATM Failed
60 01:52:31 250319-z5550254 8 19F z5550254 - + + - - + + AY-072.crude
60 01:38:28 250319-z5550254 7 1H z5550254 + + + + + + + AY-072.crude
59 01:30:42 250319-z3544630 4 1H z3544630 + x + + + + + 100 mM GOA 300 uL + 50 mM MA D2O 300 uL ATM Failed
58 01:21:10 250319-z3544630 3 1H z3544630 + + + + + + + 100 mM GCA 300 uL + 50 mM MA D2O 300 uL
57 01:12:13 250319-z3544630 2 1H z3544630 + + + + + + + Mo0.08-0h 300 uL + 50 mM MA D2O 300 uL
56 01:02:42 250319-z3544630 1 1H z3544630 + + + + + + + PET PS 300 uL + 50 mM MA D2O 300 uL
55 22:55:41 250319-ccc 2 13C.night ccc - + + - - + + GC8075-13C; dihalide C6 6-quinoline suzuki; F7-17; CDCl3; 400MHz
55 22:45:06 250319-ccc 1 1H ccc + + + + + + + GC8075; dihalide C6 6-quinoline suzuki; F7-17; CDCl3; 400MHz
54 22:37:40 250319-z5489717 5 1H z5489717 + + + + + + + DSM-R215-vac. CDCl3
53 22:29:34 250319-z5489717 4 1H z5489717 + + + + + + + DSM-R214-ext-N,O? CDCl3
52 22:22:09 250319-z5489717 3 1H z5489717 + + + + + + + DSM-Benzamide CDCl3
51 22:13:58 250319-z5492576 5 1H z5492576 + + + + + + + ZA-02-06-Mesitylene-CDCl3
50 22:07:10 250319-z5492576 4 1H z5492576 + + + + x + + ZA-02-06-mcn-CDCl3 Shim failed
49 21:56:15 250319-z5492576 3 1H z5492576 + x + + + + + ZA-02-06-meoh-CDCl3 ATM Failed
48 21:49:14 250319-z5492576 2 1H z5492576 + + + + + + + ZA-02-06-dmf-CDCl3
47 21:39:52 250319-z5492576 1 1H z5492576 + + + + + + + ZA-02-06-HFIP-CDCl3
46 21:29:27 250319-z5382436 9 1H z5382436 + + + + + + + AH02,157
45 21:19:40 250319-z5382436 8 1H z5382436 + + + + + + + AH(37, 38)
44 21:09:58 250319-z5382436 7 1H z5382436 + + + + + + + AH(36-4)
43 20:57:53 250319-z5382436 6 1H z5382436 + + + + + + + AH(36-2)
42 20:48:31 250319-z5382436 5 1H z5382436 + + + + + + + AH(36)
41 20:37:50 250319-z5382436 4 1H z5382436 + + + + + + + AH02,160
40 20:27:03 250319-z5382436 3 1H z5382436 + + + + + + + AH02,156
39 20:16:34 250319-z5382436 2 1H z5382436 + + + + + + + AH02,154
38 20:06:34 250319-z5382436 1 1H z5382436 + + + + + + + AH02,153
37 19:31:48 250319-z5628481 3 1H.noesy z5628481 - + + - - + + Me-03d ullman coupling k2co3 noesy
37 19:28:30 250319-z5628481 2 19F{1H} z5628481 - x + - - + + Me-03d ullman coupling k2co3 19F ATM Failed
37 19:20:54 250319-z5628481 1 1H z5628481 + + + + + + + Me-03d ullman coupling k2co3 1H
36 19:17:27 250319-nnt 7 1H.es nnt - + + - - + + after coupling (water phase)
36 19:05:36 250319-nnt 6 13C.day nnt - x + - - + + after coupling (water phase) ATM Failed, ADC reported overflow
36 18:56:22 250319-nnt 5 1H nnt + + + + + + + after coupling (water phase)
35 18:43:17 250319-nnt 4 13C.day nnt - + + - - + + after coupling (organic phase)
35 18:36:03 250319-nnt 3 1H nnt + + + + + + + after coupling (organic phase)
34 18:32:30 250319-nnt 3 1H.es nnt - + + - - + x eosin Y
34 18:19:19 250319-nnt 2 13C.day nnt - x + - - + + eosin Y ATM Failed
34 18:10:49 250319-nnt 1 1H nnt + + + + + + + eosin Y
33 18:02:58 250319-z5426952 1 1H z5426952 + + + + + + + RI-D-0083 OH
32 17:54:38 250319-z5537965 2 1H z5537965 + + + + + + + LH_300mg_18.3.25_post polymerization
31 17:47:27 250319-suj 2 1H suj + + + + + + + bromobenzene
30 17:38:40 250319-suj 1 1H suj + + + + + + + ss-25-03 crude o.n. after workup
29 17:31:54 250319-kee 1 1H kee + + + + + + + Purified PELP
28 17:25:12 250319-rdr 1 1H rdr + + + + + + + 2-018 4Bpin column purple
27 17:14:02 250319-yux 1 1H yux + x + + + + + rithik pba133phea66 pr ATM Failed
26 17:04:41 250319-jnn 9 19F{1H} jnn - + + - - + + JAN-188.1
26 16:55:14 250319-jnn 8 19F jnn - + + - - + + JAN-188.1
26 16:41:25 250319-jnn 7 1H jnn + + + + + + + JAN-188.1
25 16:35:13 250319-z5550254 6 19F{1H} z5550254 - + + - - + + AY-072
25 16:29:53 250319-z5550254 5 19F z5550254 - + + - - + + AY-072
25 16:19:47 250319-z5550254 4 1H z5550254 + + + + + + + AY-072
24 16:13:13 250319-amn 1 1H amn + x + + + + + AMM - H006 - H2TMP in CDCl3 After semi-column (main collection) ATM Failed
23 16:04:18 250319-jnn 6 19F{1H} jnn - + + - - + + JAN-203.1
23 15:54:41 250319-jnn 5 19F jnn - + + - - + + JAN-203.1
23 15:39:56 250319-jnn 4 1H jnn + x + + + + + JAN-203.1 ATM Failed
22 15:30:18 250319-jnn 3 19F{1H} jnn - + + - - + + JAN-206 Crude
22 15:21:13 250319-jnn 2 19F jnn - + + - - + + JAN-206 Crude
22 15:06:53 250319-jnn 1 1H jnn + + + + + + + JAN-206 Crude
21 14:59:51 250319-z5426952 2 1H z5426952 + x + + + + + RI-D-83 Crude ATM Failed
20 14:51:23 250319-z5426952 1 1H z5426952 + + + + + + + RI-OH-4 F2
19 14:41:46 250319-z5564533 2 1H z5564533 + + + + + + + CM-061-2
18 14:31:23 250319-z5564533 1 1H z5564533 + + + + + + + CM-061-1
17 14:24:39 250319-z5547474 1 1H z5547474 + + + + + + + P(LA-co-DEGEEA)-CTA 15k pure
16 14:10:37 250319-z5550254 3 1H z5550254 + + + + + + + AY-053.1
15 13:56:04 250319-z5550254 2 1H z5550254 + + + + + + + AY-070.1
14 13:41:06 250319-z5550254 1 1H z5550254 + + + + + + + AY-069.1
13 13:32:38 250319-z5167506 4 1H z5167506 + + + + + + + 8 T20 CDCl3
12 13:24:11 250319-z5167506 3 1H z5167506 + + + + + + + 8 T0 CDCl3
11 13:15:07 250319-z5167506 2 1H z5167506 + + + + + + + 10 T20 CDCl3
10 13:07:20 250319-z5167506 1 1H z5167506 + x + + + + + 10 T0 CDCl3 ATM Failed
9 13:00:12 250319-iconnmr 5 sst.31P.sen iconnmr + + + + + + + 31P Sensitivity 0.0485 M triphenylphosphate (TPP) in d6-acetone Specification result of sinocal: Best sino value found ( > 150:1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/5/pdata/1/250319-iconnmr_5_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/5/pdata/1/250319-iconnmr_5_1.pdf Check for printing system problems
8 12:51:19 250319-iconnmr 4 sst.19F.qnp.sen iconnmr + x + + + + + 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found ( > 250 :1) ATM Failed, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/4/pdata/1/250319-iconnmr_4_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/4/pdata/1/250319-iconnmr_4_1.pdf Check for printing system problems
7 12:26:38 250319-iconnmr 3 sst.13C.sen iconnmr + + + + + + + 13C Sensitivity 10% Ethylbenzene (EB) in CDCl3 Specification result of sinocal: Best sino value found ( > 200 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/3/pdata/1/250319-iconnmr_3_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/3/pdata/1/250319-iconnmr_3_1.pdf Check for printing system problems
6 12:15:51 250319-iconnmr 2 sst.1H.sen iconnmr + + + + + + + 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found ( > 300 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/2/pdata/1/250319-iconnmr_2_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/2/pdata/1/250319-iconnmr_2_1.pdf Check for printing system problems
5 12:06:29 250319-iconnmr 1 sst.1H.lsh iconnmr + + + + + + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/1/pdata/1/250319-iconnmr_1_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250319-iconnmr/1/pdata/1/250319-iconnmr_1_1.pdf Check for printing system problems
4 12:01:18 250319-z5489717 2 19F z5489717 - + + - - + + DSM-R214-60C-overnight-crude-vac-TFT CDCl3
4 11:55:26 250319-z5489717 1 1H z5489717 + x + + + + + DSM-R214-60C-overnight-crude-vac-TFT CDCl3 ATM Failed
3 11:49:10 250319-ehw 1 1H ehw + x + + + + + EW0071_pro ATM Failed
2 11:30:19 250319-z5371131 5 1H13C.hsqc.aded z5371131 - + + - - + + AM1.06-4
2 11:27:36 250319-z5371131 4 1H z5371131 - + + - - + + AM1.06-4
2 11:17:31 250319-z5371131 3 13C.dept90 z5371131 - + + - - + + AM1.06-4
2 11:05:43 250319-z5371131 2 13C.dept135 z5371131 - + + - - + + AM1.06-4
2 10:50:46 250319-z5371131 1 13C.day z5371131 + x + + + + + AM1.06-4 ATM Failed, ADC reported overflow
1 10:41:43 250319-z5537965 1 1H z5537965 + + + + + + + LH_200_(1)_19.3.25
43 08:42:51 250319-isj 4 19F{1H} isj - + + - - + + IJ-026 r cat set 2 after first attempt of heating Automation was stopped by user
43 08:35:32 250319-isj 3 1H isj + + + + + + + IJ-026 r cat set 2 after first attempt of heating
42 08:31:50 250319-isj 2 19F{1H} isj - x + - - + + IJ-026 r cat set 1 after first attempt of heating ATM Failed
42 08:22:26 250319-isj 1 1H isj + + + + + + + IJ-026 r cat set 1 after first attempt of heating
40 20:03:11 250318-z3545554 1 1H z3545554 + + + + + + +
37 19:55:06 250318-z5540930 2 1H z5540930 + + + + + + + PEGLA S2r
36 19:46:50 250318-z5540930 1 1H z5540930 + + + + + + + CatLA S2r
35 19:39:20 250318-z5371131 2 1H z5371131 + + + + + + + AM5.01 column
34 19:32:30 250318-z5371131 1 1H z5371131 + + + + + + + AM1.06-4 precipitate
33 19:28:04 250318-z5489717 2 19F z5489717 - + + - - + + DSM-R213-1hour-crude-direct CDCl3
33 19:21:39 250318-z5489717 1 1H z5489717 + + + + + + + DSM-R213-1hour-crude-direct CDCl3
31 19:12:33 250318-kee 1 1H kee + + + + + + + pelp-pure
30 19:00:53 250318-z3543503 8 19F.polymer z3543503 - + + - - + + EB11r1 poly s2
30 18:53:58 250318-z3543503 7 1H z3543503 + x + + + + + EB11r1 poly s2 ATM Failed
29 18:40:20 250318-z3543503 6 19F.polymer z3543503 - + + - - + + EB11r1 poly s2 t=0
29 18:31:30 250318-z3543503 5 1H z3543503 + + + + + + + EB11r1 poly s2 t=0
28 18:28:02 250318-jpe 10 31P{1H}.pg jpe - x + - - + + m8-m-washed cdcle ATM Failed
28 17:22:18 250318-jpe 9 13C.night jpe - + + - - + + m8-m-washed cdcle ADC reported overflow
28 17:14:01 250318-jpe 8 1H.es jpe + + + + + + + m8-m-washed cdcle
27 17:09:04 250318-jpe 7 31P{1H}.pg jpe - + + - - + + u6-m-washed cdcle
27 16:05:05 250318-jpe 6 13C.night jpe - x + - - + + u6-m-washed cdcle ATM Failed
27 15:57:52 250318-jpe 5 1H.es jpe + + + + + + + u6-m-washed cdcle
26 15:53:17 250318-jlt 5 19F{1H} jlt - + + - - + + JT-P5JR-05A-col-fb
26 15:44:27 250318-jlt 4 1H jlt + x + + + + + JT-P5JR-05A-col-fb ATM Failed
25 15:39:56 250318-jlt 3 19F{1H} jlt - + + - - + + JT-P5J5-05C-col-fb
25 15:29:42 250318-jlt 2 1H jlt + + + + + + + JT-P5J5-05C-col-fb
24 15:21:58 250318-jlt 1 1H jlt + x + + + + + JT-2M2MPA-step1-ppt ATM Failed
23 15:11:59 250318-jsm 3 1H jsm + + + + + + + JM305m (had to add some DMSO-d6 too cause wasn't dissolving use that in future for the NMR)
22 15:01:54 250318-jsm 2 1H jsm + + + + + + + JM305l (had to add some DMSO-d6 too cause wasn't dissolving use that in future for the NMR)
21 14:52:10 250318-jsm 1 1H jsm + + + + + + + JM305k (had to add some DMSO-d6 too cause wasn't dissolving use that in future for the NMR)
20 14:47:27 250318-z5628481 5 19F{1H} z5628481 - + + - - + + Me-03d crude reac mix na2co3 19F
20 14:40:09 250318-z5628481 4 1H z5628481 + + + + + + + Me-03d crude reac mix na2co3 1H
19 14:35:21 250318-isj 8 19F{1H} isj - + + - - + + IJ-026 r cat set 2 (pure?) before heating in deut acn
19 14:31:05 250318-isj 7 19F isj - + + - - + + IJ-026 r cat set 2 (pure?) before heating in deut acn
19 14:21:32 250318-isj 6 1H isj + x + + + + + IJ-026 r cat set 2 (pure?) before heating in deut acn ATM Failed
18 14:16:44 250318-isj 5 19F{1H} isj - + + - - + + IJ-026 r cat set 1 (not a mixture) before heating in deut acn
18 14:11:38 250318-isj 4 19F isj - + + - - + + IJ-026 r cat set 1 (not a mixture) before heating in deut acn
18 14:05:53 250318-isj 3 1H isj + x + + + + + IJ-026 r cat set 1 (not a mixture) before heating in deut acn ATM Failed
17 13:52:52 250318-yab 4 13C.day yab - + + - - + + YA_TROPL_N+_RC_PURE
17 13:45:24 250318-yab 3 1H yab + + + + + + + YA_TROPL_N+_RC_PURE
16 13:31:34 250318-yab 2 13C.day yab - + + - - + + YA_1E3_P+_TR_RC_PURE
16 13:23:22 250318-yab 1 1H yab + + + + + + + YA_1E3_P+_TR_RC_PURE
15 13:05:49 250318-z5628481 3 19F{1H} z5628481 + + + + + + + 3-fluorophenol 19F
14 12:34:36 250318-z5628481 2 19F{1H} z5628481 + x + + + + + me-03d pybop reac mix 19F nmr 3hr ATM Failed
13 12:26:57 250318-z5361776 1 1H z5361776 + + + + + + + JP-001 iPr diarylquinocyclopropene + 1% py-d5
12 12:19:03 250318-isj 2 1H isj + + + + + + + IJ-026 t cat pure? set 2
11 12:08:26 250318-isj 1 1H isj + + + + + + + IJ-026 r cat not a mixture set 1
10 12:00:59 250318-z5537965 1 1H z5537965 + + + + + + + LH_18.3.25_300_0hr
9 11:52:33 250318-z3544630 8 1H z3544630 + + + + + + + MS-ZIS-6h 300 uL+ 50 mM MA in D2O 300 uL
8 11:44:41 250318-z3544630 7 1H z3544630 + x + + + + + Real PET-6h 300 uL+ 50 mM MA in D2O 300 uL ATM Failed
7 11:36:02 250318-z3544630 6 1H z3544630 + + + + + + + Real PET-0h 300 uL+ 50 mM MA in D2O 300 uL
6 11:27:46 250318-z3544630 5 1H z3544630 + + + + + + + 100 mM AA 300 uL+ 50 mM MA in D2O 300 uL
5 11:19:59 250318-z3544630 4 1H z3544630 + x + + + + + 100 mM FA 300 uL+ 50 mM MA in D2O 300 uL ATM Failed
4 11:10:36 250318-z3544630 3 1H z3544630 + + + + + + + 100 mM EG 300 uL+ 50 mM MA in D2O 300 uL
3 11:02:27 250318-z3544630 2 1H z3544630 + + + + + + + 100 mM TPA 300 uL+ 50 mM MA in D2O 300 uL
2 10:53:59 250318-z3544630 1 1H z3544630 + + + + + + + 1M Naoh 300ul + 50 mM MA in D2O 300 uL
1 10:10:42 250318-z5628481 1 19F{1H} z5628481 + + + + + + + Me-03d ulman coupling reac mix 19 F decoup
31 09:40:53 250318-z3543503 4 19F.polymer z3543503 - + + - - + + EB11r1 poly s1
31 09:34:52 250318-z3543503 3 1H z3543503 + x + + + + + EB11r1 poly s1 ATM Failed
30 09:22:16 250318-z3543503 2 19F.polymer z3543503 - + + - - + + EB11r1 poly s1 t=0
30 09:15:14 250318-z3543503 1 1H z3543503 + + + + + + + EB11r1 poly s1 t=0
29 08:11:03 250318-jpe 4 13C.night jpe - + + - - + + u6-m-dig (only water) ADC reported overflow
29 08:03:55 250318-jpe 3 1H.es jpe + + + + + + + u6-m-dig (only water)
28 06:59:09 250318-jpe 2 13C.night jpe - + + - - + + m8-m-dig (only water)
28 06:50:51 250318-jpe 1 1H.es jpe + + + + + + + m8-m-dig (only water)
27 01:38:58 250317-zhz 3 1H zhz + + + + + + + ZZ-101 MeOH soluble
26 01:28:39 250317-zhz 2 1H zhz + + + + + + + ZZ-101 acetone soluble
25 01:19:33 250317-ccc 1 1H ccc + + + + + + + GC8075; dihalide 6-quinoline suzuki; crude; CDCl3; 400MHz
24 01:05:04 250317-nap 2 13C.day nap - + + - - + + 112-TC ADC reported overflow
24 00:58:05 250317-nap 1 1H nap + + + + + + + 112-TC
23 00:53:48 250317-isj 5 19F{1H} isj - x + - - + + IJ-026 r cat 2nd hplc set pure? ATM Failed
23 00:46:10 250317-isj 4 1H isj + + + + + + + IJ-026 r cat 2nd hplc set pure?
22 22:39:20 250317-jlt 13 13C.night jlt - + + - - + + JT-P5J5-04C-prod-D2Os ADC reported overflow
22 22:19:28 250317-jlt 12 1H13C.hsqc.aded jlt - + + - - + + JT-P5J5-04C-prod-D2Os
22 22:14:07 250317-jlt 11 1H{19F}.ig jlt - + + - - x - JT-P5J5-04C-prod-D2Os Acquisition Failed
22 22:02:26 250317-jlt 10 1H jlt + + + + + + + JT-P5J5-04C-prod-D2Os
21 20:57:24 250317-jlt 9 13C.night jlt - + + - - + + JT-P5JR-04A-prod-D2Os
21 20:39:20 250317-jlt 8 1H13C.hsqc.aded jlt - x + - - + + JT-P5JR-04A-prod-D2Os ATM Failed
21 20:25:45 250317-jlt 7 1H jlt + + + + + + + JT-P5JR-04A-prod-D2Os
20 20:18:36 250317-z5540930 2 1H z5540930 + + + + + + + PEGLA S2
19 20:11:15 250317-z5540930 1 1H z5540930 + + + + + + + CatLA S2
18 20:06:56 250317-jlt 6 19F{1H} jlt - x + - - + + 6-F-Az-step2-recol-t8-11 ATM Failed
18 19:56:16 250317-jlt 5 1H jlt + + + + + + + 6-F-Az-step2-recol-t8-11
17 19:42:39 250317-jsm 14 13C.day jsm - + + - - + + Ph alkyne BMIDA + Benzoquinone + Indole + Zn(OTf)2 crude NMR
17 19:39:29 250317-jsm 13 11B jsm - + + - - + + Ph alkyne BMIDA + Benzoquinone + Indole + Zn(OTf)2 crude NMR
17 19:29:42 250317-jsm 12 1H jsm + + + + + + + Ph alkyne BMIDA + Benzoquinone + Indole + Zn(OTf)2 crude NMR
16 19:26:32 250317-jsm 11 11B jsm - + + - - + + Ph alkyne BMIDA + Benzoquinone 14h crude NMR (should be complete based on the TLC)
16 19:17:05 250317-jsm 10 1H jsm + + + + + + + Ph alkyne BMIDA + Benzoquinone 14h crude NMR (should be complete based on the TLC)
15 19:08:26 250317-jsm 9 1H jsm + + + + + + + JM305j (it's been in the NMR tube overnight as made a mistake when submitting samples)
14 18:58:10 250317-jsm 7 1H jsm + + + + + + + JM305i (it's been in the NMR tube overnight as made a mistake when submitting samples)
13 18:54:48 250317-jsm 6 11B jsm - + + - - + + Ph alkyne BMIDA + Benzoquinone 2h crude NMR check (it's been in the NMR tube overnight as made a mistake when submitting samples)
13 18:44:36 250317-jsm 5 1H jsm + + + + + + + Ph alkyne BMIDA + Benzoquinone 2h crude NMR check (it's been in the NMR tube overnight as made a mistake when submitting samples)
12 18:35:34 250317-zhz 1 1H zhz + + + + + + + ZZ-101 crude
11 18:29:11 250317-vaf 3 1H vaf + + + + + + + 5a-T
10 16:51:56 250317-vaf 2 13C.night vaf - + + - - + + 5a-column ADC reported overflow
10 16:43:06 250317-vaf 1 1H vaf + x + + + + + 5a-column ATM Failed
9 16:26:56 250317-z5628481 3 13C.day z5628481 + + + + + + + Me-02d 13C nmr
8 16:21:56 250317-z5628481 2 19F{1H} z5628481 - + + - - + + Triazole ring closure product 19F
8 16:15:47 250317-z5628481 1 1H z5628481 + + + + + + + Triazole ring closure product 1H
7 16:09:15 250317-z5371131 1 1H z5371131 + + + + + + + AM5.01 check
6 15:00:05 250317-djg 1 13C.night djg + + + + + + + DJG-B-146 5-methylisopyrocoll ADC reported overflow
5 14:47:41 250317-z5493478 2 19F z5493478 - + + - - + + SIC049 Fr.22-30 DMSO Weber
5 14:38:39 250317-z5493478 1 1H z5493478 + + + + + + + SIC049 Fr.22-30 DMSO Weber
4 14:28:29 250317-z5485590 2 1H z5485590 + + + + + + + MKA48-5h-crude
3 14:20:27 250317-z5363218 2 1H z5363218 + x + + + + + CDO-2.3 ATM Failed
2 14:12:49 250317-z5363218 1 1H z5363218 + + + + + + + CDO-2.2
1 13:41:11 250317-isj 3 19F{1H} isj + + + + + + + IJ-026 r cat not a mixture hplc set 1 correct solvent
15 12:46:21 250317-z5564533 2 1H z5564533 + + + + + + + CM-059-2
14 12:38:27 250317-z5564533 1 1H z5564533 + + + + + + + CM-059-1
13 12:28:13 250317-z5438782 5 1H z5438782 + + + + + + + 470nm elp bulk 24h
12 12:20:39 250317-isj 2 19F{1H} isj - + + - - + + IJ-026 r cat not a mixture hplc
12 12:11:38 250317-isj 1 1H isj + + + + + + + IJ-026 r cat not a mixture hplc
11 12:01:38 250317-z5485590 1 1H z5485590 + + + + + + + MKA48-4h-crude
10 11:34:11 250317-jlt 4 19F{1H} jlt - + + - - + + JT-P5JR-04A-prod
10 11:22:53 250317-jlt 3 1H jlt + + + + + + + JT-P5JR-04A-prod
9 11:18:15 250317-jlt 2 19F{1H} jlt - + + - - + + JT-P5J5-04C-col1
9 11:09:14 250317-jlt 1 1H jlt + + + + + + + JT-P5J5-04C-col1
8 10:42:02 250317-z5550254 1 1H z5550254 + + + + + + + AY-069.crude
7 10:35:53 250317-z5165127 3 1H z5165127 + + + + + + + Max - chlorination reagent - REAGENT - CDCl3
6 10:29:43 250317-z5165127 2 1H z5165127 + + + + + + + Max - chlorination product check - PRODUCT - CDCl3
5 10:20:23 250317-z5165127 1 1H z5165127 + + + + + + + CMG115 - pentabenzylCpH crystals from mother liquor (not dried) - CDCl3
4 09:06:44 250317-z5438782 4 1H z5438782 + + + + + + + 470nm bulk elp 10h
3 08:55:25 250317-z5438782 3 1H z5438782 + + + + + + + 470nm bulk elp 8h
2 08:45:21 250317-z5438782 2 1H z5438782 + + + + + + + 470nm bulk elp 6h
1 08:35:56 250317-z5438782 1 1H z5438782 + + + + + + + elp
5 03:42:07 250317-jsm 4 1H jsm x - - - - - - JM305j Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 5
4 03:33:33 250317-jsm 3 1H jsm + + + + + + + JM305i
3 03:24:31 250317-jsm 2 11B jsm - + + - - + + Ph alkyne BMIDA + BQ test 2h NMR crude
3 03:15:27 250317-jsm 1 1H jsm + + + + + + + Ph alkyne BMIDA + BQ test 2h NMR crude
53 14:43:30 250316-z5438782 6 1H z5438782 + + + + + + + 470nm bulk elp 4h
52 12:46:20 250316-z5537965 2 1H z5537965 + x + + + + + C-A-B ATM Failed
51 12:38:40 250316-z5537965 1 1H z5537965 + + + + + + + AC-B Block
50 12:11:09 250316-z5438782 5 1H z5438782 + x + + + + + 470nm bulk elp 2h ATM Failed
49 11:27:07 250316-z5438782 4 1H z5438782 + + + + + + + 470nm bulk elp 1h
48 11:13:11 250316-z5438782 3 1H z5438782 + + + + + + + 470nm bulk elp 30min
47 10:59:40 250316-z5438782 2 1H z5438782 + + + + + + + 470nm bulk elp 15min
46 10:36:34 250316-z5438782 1 1H z5438782 + + + + + + + 530nm elp bisttc 48h
1 23:07:24 250314-jlt 2 19F{1H} jlt - + + - - + + X-2501-t14-20-19F{1H}
1 23:00:17 250314-jlt 1 1H jlt + + + + + + + X-2501-t14-20-19F{1H}
45 22:52:42 250315-mda 2 1H mda + + + + + + + Purified 2MBT
44 22:44:29 250315-jnn 7 19F{1H} jnn - x + - - + + JAN-204.1 ATM Failed
44 22:34:37 250315-jnn 6 19F jnn - + + - - + + JAN-204.1
44 22:20:05 250315-jnn 5 1H13C.hmbc jnn - + + - - + + JAN-204.1
44 22:01:12 250315-jnn 4 1H13C.hsqc.aded jnn - + + - - + + JAN-204.1
44 21:50:11 250315-jnn 3 1H.cosy jnn - + + - - + + JAN-204.1
44 19:43:07 250315-jnn 2 13C.night jnn - + + - - + + JAN-204.1
44 19:28:39 250315-jnn 1 1H jnn + x + + + + + JAN-204.1 ATM Failed
43 19:20:08 250315-mda 1 1H mda + + + + + + + 1 PCTA
42 19:08:55 250314-sub 1 1H sub + x + + + + + SB144-D org layer with BuLi CDCl3 ATM Failed
41 17:28:59 250314-law 6 13C.night law - + + - - + + X-3094-fum-char ADC reported overflow
41 17:23:30 250314-law 5 19F{1H} law - + + - - + + X-3094-fum-char
41 17:15:15 250314-law 4 1H law + + + + + + + X-3094-fum-char
40 15:34:37 250314-law 3 13C.night law - + + - - + + X-3107-fum-char
40 15:29:44 250314-law 2 19F{1H} law - + + - - + + X-3107-fum-char
40 15:22:58 250314-law 1 1H law + + + + + + + X-3107-fum-char
39 14:19:11 250314-jlt 15 13C.night jlt - x + - - + + X-3106-fum-char ATM Failed, ADC reported overflow
39 14:13:17 250314-jlt 14 19F{1H} jlt - + + - - + + X-3106-fum-char
39 14:07:04 250314-jlt 13 1H jlt + + + + + + + X-3106-fum-char
38 13:01:59 250314-jlt 12 13C.night jlt - + + - - + + X-3093-ox-char ADC reported overflow
38 12:56:13 250314-jlt 11 19F{1H} jlt - + + - - + + X-3093-ox-char
38 12:47:56 250314-jlt 10 1H jlt + + + + + + + X-3093-ox-char
37 11:07:58 250314-jlt 9 13C.night jlt - + + - - + + X-1809-char ADC reported overflow
37 11:04:15 250314-jlt 8 19F{1H} jlt - x + - - + + X-1809-char ATM Failed
37 10:57:35 250314-jlt 7 1H jlt + + + + + + + X-1809-char
36 09:52:13 250314-jlt 6 13C.night jlt - + + - - + + JT-P5JR-05B-fb-col ADC reported overflow
36 09:41:12 250314-jlt 5 1H.cosy jlt - + + - - + + JT-P5JR-05B-fb-col
36 09:35:47 250314-jlt 4 19F{1H} jlt - + + - - + + JT-P5JR-05B-fb-col
36 09:26:14 250314-jlt 3 1H jlt + + + + + + + JT-P5JR-05B-fb-col
35 09:16:28 250314-ild 4 1H ild + x + + + + + ID12037; ET suzuki cr; CDCl3 ATM Failed
34 09:08:40 250314-ild 3 1H ild + + + + + + + ID12031; NMethylation cr; CDCl3
33 08:58:56 250314-z3544630 9 1H z3544630 + + + + + + + MS-ZIS-6H
32 08:49:01 250314-z3544630 8 1H z3544630 + + + + + + + MS-ZIS-0H
31 08:39:06 250314-z3544630 7 1H z3544630 + + + + + + + PET-PS-1M
30 07:34:39 250314-z3544630 6 13C.night z3544630 - x + - - + + pp-i2-6h ATM Failed
30 07:16:24 250314-z3544630 5 1H z3544630 + + + + + + + pp-i2-6h
1 06:13:00 250314-jlt 2 19F{1H} jlt - x + - - x - X-2501-t14-20-19F{1H} ATM Failed, Acquisition Failed
1 06:02:16 250314-jlt 1 1H jlt + x + + x x - X-2501-t14-20-19F{1H}
42 05:51:26 250314-sub 1 1H sub + x + + x x - SB144-D org layer with BuLi CDCl3
41 05:48:46 250314-law 6 13C.night law - x + - - x - X-3094-fum-char
41 05:46:13 250314-law 5 19F{1H} law - x + - - x - X-3094-fum-char
41 05:35:43 250314-law 4 1H law + x + + x x - X-3094-fum-char
40 05:33:09 250314-law 3 13C.night law - x + - - x - X-3107-fum-char
40 05:30:08 250314-law 2 19F{1H} law - x + - - x - X-3107-fum-char
40 05:19:43 250314-law 1 1H law + x + + x x - X-3107-fum-char
39 05:16:41 250314-jlt 15 13C.night jlt - x + - - x - X-3106-fum-char
39 05:10:47 250314-jlt 14 19F{1H} jlt - x + - - x - X-3106-fum-char
39 04:59:44 250314-jlt 13 1H jlt + x + + x x - X-3106-fum-char
38 04:57:10 250314-jlt 12 13C.night jlt - x + - - x - X-3093-ox-char
38 04:55:44 250314-jlt 11 19F{1H} jlt - x + - - x - X-3093-ox-char
38 04:45:31 250314-jlt 10 1H jlt + x + + x x - X-3093-ox-char
37 04:44:11 250314-jlt 9 13C.night jlt - x + - - x - X-1809-char
37 04:43:10 250314-jlt 8 19F{1H} jlt - x + - - x - X-1809-char
37 04:32:48 250314-jlt 7 1H jlt + x + + x x - X-1809-char
36 04:30:17 250314-jlt 6 13C.night jlt - x + - - x - JT-P5JR-05B-fb-col
36 04:28:33 250314-jlt 5 1H.cosy jlt - x + - - x - JT-P5JR-05B-fb-col
36 04:25:38 250314-jlt 4 19F{1H} jlt - x + - - x - JT-P5JR-05B-fb-col
36 04:16:22 250314-jlt 3 1H jlt + x + + x x - JT-P5JR-05B-fb-col
35 04:05:49 250314-ild 4 1H ild + x + + x x - ID12037; ET suzuki cr; CDCl3
34 03:54:53 250314-ild 3 1H ild + x + + x x - ID12031; NMethylation cr; CDCl3
33 03:44:43 250314-z3544630 9 1H z3544630 + x + + x x - MS-ZIS-6H
32 03:34:08 250314-z3544630 8 1H z3544630 + x + + x x - MS-ZIS-0H
31 03:23:30 250314-z3544630 7 1H z3544630 + x + + x x - PET-PS-1M
30 03:21:04 250314-z3544630 6 13C.night z3544630 - x + - - x - pp-i2-6h
30 03:09:56 250314-z3544630 5 1H z3544630 - - - - - - - pp-i2-6h
29 02:03:24 250314-z3544630 4 13C.night z3544630 - + + - - + + pp-i2-3h
29 01:51:16 250314-z3544630 3 1H z3544630 + + + + + + + pp-i2-3h
28 00:46:12 250314-z3544630 2 13C.night z3544630 - + + - - + + pp
28 00:31:59 250314-z3544630 1 1H z3544630 + + + + + + + pp
27 00:25:07 250314-z5540930 6 1H z5540930 + + + + + + + CatLA470nm24h
26 00:17:59 250314-z5540930 5 1H z5540930 + + + + + + + PEGLA470 24h
25 00:10:05 250314-z5540930 4 1H z5540930 + + + + + + + BL470nm24h
24 00:02:13 250314-z5540930 3 1H z5540930 + + + + + + + CatLA470T0
23 23:52:32 250314-z5540930 2 1H z5540930 + + + + + + + PEGLA470T0
22 23:46:33 250314-z5540930 1 1H z5540930 + x + + + + + BL470nmT0 ATM Failed
21 23:38:07 250314-z5363218 1 1H z5363218 + + + + + + +
18 21:32:20 250314-ild 2 13C.night ild - x + - - + + ID4049 DMSO ATM Failed
18 21:24:22 250314-ild 1 1H ild + x + + + + + ID4049 DMSO ATM Failed
17 20:20:42 250314-z5550254 9 13C.night z5550254 - x + - - + + AY-067.1 ATM Failed, ADC reported overflow
17 20:06:45 250314-z5550254 8 1H z5550254 + + + + + + + AY-067.1
16 19:01:23 250314-z5550254 7 13C.night z5550254 - + + - - + + AY-066.1 ADC reported overflow
16 18:53:27 250314-z5550254 6 19F{1H} z5550254 - + + - - + + AY-066.1
16 18:47:16 250314-z5550254 5 19F z5550254 - + + - - + + AY-066.1
16 18:31:18 250314-z5550254 4 1H z5550254 + + + + + + + AY-066.1
15 18:20:50 250314-jsm 4 1H jsm + + + + + + + JM305d
14 18:10:55 250314-jsm 3 1H jsm + + + + + + + JM305c
13 18:00:54 250314-jsm 2 1H jsm + + + + + + + JM305b
12 17:49:47 250314-jsm 1 1H jsm + + + + + + + JM305a
11 17:41:28 250314-z5255867 5 1H z5255867 + + + + + + + JL-034 3rd Syn Check 14.03.25
10 16:30:13 250314-z5426952 6 13C.night z5426952 + + + + + + + RI-D-81 F2
9 15:20:08 250314-z5426952 5 13C.night z5426952 + + + + + + + RI-D-81 f1 ADC reported overflow
20 13:40:13 250314-suj 2 1H suj + + + + + + + ss-25-02 crude 15h after workup
19 13:33:02 250314-z5485590 3 1H z5485590 + + + + + + + P3-t0-3
18 13:23:44 250314-z5485590 2 1H z5485590 + + + + + + + P2-t0-2
17 13:15:48 250314-z5485590 1 1H z5485590 + + + + + + + P1-t0-1
16 13:07:38 250314-rdr 1 1H rdr + + + + + + + 2-018 indole 1.1 eq
15 12:59:28 250314-z5489717 3 1H z5489717 + + + + + + + DSM-R209-ext. CDCl3
14 12:52:51 250314-mda 3 1H mda + x + + + + + T0-P3 ATM Failed
13 12:45:57 250314-mda 2 1H mda + x + + + + + T0-P2 ATM Failed
12 12:37:56 250314-mda 1 1H mda + + + + + + + T0-P1
11 12:31:51 250314-z5550254 3 19F{1H} z5550254 - + + - - + + AY-068.crude
11 12:24:05 250314-z5550254 2 19F z5550254 - + + - - + + AY-068.crude
11 12:10:03 250314-z5550254 1 1H z5550254 + + + + + + + AY-068.crude
10 11:53:10 250314-z5426952 4 13C.day z5426952 + + + + + + + RI-D-81 F2 ADC reported overflow
9 11:36:03 250314-z5426952 3 13C.day z5426952 + x + + + + + RI-D-81 F1 ATM Failed, ADC reported overflow
8 11:20:07 250314-z5426952 2 13C.day z5426952 + x + + + + + RI-D-80 F2 ATM Failed
7 11:03:26 250314-z5426952 1 13C.day z5426952 + + + + + + + RI-D-80 F1
6 10:50:10 250314-lit 2 1H lit + + + + + + + GTHQCy5-25Nov2024Batch-DCM+TFA-20h, D2O
5 10:37:39 250314-lit 1 1H lit + x + + + + + GTHQCy5-30Nov2024Batch-DCM+TFA-4h, D2O ATM Failed
4 10:27:34 250314-suj 1 1H suj + + + + + + + ss-25-02 crude o.n. without workup
3 10:15:30 250314-z5564533 2 1H.cosy z5564533 - + + - - + + CM-057-1
3 10:08:20 250314-z5564533 1 1H z5564533 + + + + + + +
2 09:31:24 250314-z5489717 2 1H z5489717 + + + + + + + DSM-R209-daynight-crude-direct CDCl3
1 09:22:31 250314-z5489717 1 1H z5489717 + + + + + + + DSM-N-ethylpiperidine
60 01:20:29 250313-z3545554 1 1H z3545554 + + + + + + +
56 01:12:06 250313-tat 2 1H tat + + + + + + + Tf rxn
55 01:05:23 250313-tat 1 1H tat + + + + + + + SM
54 00:57:12 250313-sub 8 1H sub + + + + + + + SB145-D aq layer_EtOAc extraction CDCl3 ADC reported overflow
53 00:47:36 250313-sub 7 1H sub + + + + + + + SB145-D org layer_EtOAc extraction CDCl3
52 00:39:12 250313-z5489717 1 1H z5489717 + + + + + + + DSM-R209-1day-crude-direct CDCl3
51 00:32:42 250313-z5493478 5 1H z5493478 + + + + + + + Iodobenzene CDCl3 Weber
50 00:27:31 250313-z5493478 4 19F z5493478 - + + - - + + SIC049-crude CDCl3 Weber
50 00:19:23 250313-z5493478 3 1H z5493478 + + + + + + + SIC049-crude CDCl3 Weber
49 00:09:17 250313-sub 6 1H sub + + + + + + + SB-SFD-CF1 Dimer of DPND-7 with 1,4 phenyl spacer CD2Cl2
48 23:04:35 250313-jlt 21 13C.night jlt - + + - - + + LW-139-Fum
48 22:54:55 250313-jlt 20 1H jlt + + + + + + + LW-139-Fum
47 21:50:29 250313-jlt 19 13C.night jlt - + + - - + + LW-137-Fum
47 21:43:54 250313-jlt 18 1H jlt + + + + + + + LW-137-Fum
46 20:39:14 250313-law 4 13C.night law - + + - - + + LW-136-Fum
46 20:32:37 250313-law 3 1H law + + + + + + + LW-136-Fum
45 19:28:05 250313-law 2 13C.night law - + + - - + + LW-135-Fum
45 19:21:07 250313-law 1 1H law + + + + + + + LW-135-Fum
44 19:14:22 250313-z5426952 8 1H z5426952 + + + + + + + RI-OAc F2
43 19:05:34 250313-z5426952 7 1H z5426952 + + + + + + + RI-OAc F1
42 18:58:24 250313-z5426952 6 1H z5426952 + + + + + + + RI-81 F3
41 18:51:27 250313-z5426952 5 1H z5426952 + + + + + + + RI-81 F2
40 18:42:48 250313-z5426952 4 1H z5426952 + x + + + + + RI-81 F1 ATM Failed
39 18:35:46 250313-z5426952 3 1H z5426952 + + + + + + + RI-80 F3
38 18:29:21 250313-z5426952 2 1H z5426952 + + + + + + + RI-80 F2
37 18:20:33 250313-z5426952 1 1H z5426952 + + + + + + + RI-80 F1
36 18:12:28 250313-yab 3 1H yab + + + + + + + TROPL+N+_NH_II
35 17:59:29 250313-yab 2 13C.day yab - + + - - + + 1E3+_P_TR_RECR_III ADC reported overflow
35 17:52:45 250313-yab 1 1H yab + + + + + + + 1E3+_P_TR_RECR_III
34 17:41:19 250313-ild 1 1H ild + + + + + + + ID12035; ET1000 bromination CDCl3; 400 MHz
33 17:02:14 250313-dem 3 1H dem + + + + + + + DM-MS-02-68F
32 16:53:15 250313-z5382436 4 1H z5382436 + x + + + + + Tf ATM Failed
31 16:43:17 250313-z5382436 3 1H z5382436 + + + + + + + T1
30 16:33:22 250313-z5382436 2 1H z5382436 + + + + + + + AH01-74 T0
29 16:23:17 250313-z5382436 1 1H z5382436 + + + + + + + AH02,158
28 16:15:33 250313-mda 4 1H mda + + + + + + + Purified KCDL3-CD
27 16:04:04 250313-mda 3 1H mda + + + + + + + Purified FDBTC-CD
26 15:56:59 250313-mda 2 1H mda + + + + + + + Purified KCDL3 DM
25 15:49:23 250313-mda 1 1H mda + + + + + + + Purified FDBTC-DM
24 15:40:06 250313-sub 5 1H sub + + + + + + + SB145-D aq layer D2O
23 15:32:34 250313-sub 4 1H sub + + + + + + + SB145-D org layer CDCl3
22 15:25:52 250313-sub 3 1H sub + + + + + + + SB-SFD-1 CF3 DPND-7 dimer with 1,4 Ph spacer CDCl3
21 15:13:45 250313-sub 2 1H sub + + + + + + + SB-SFD-1 CF2 DPND-7 dimer with 1,4 Ph spacer CDCl3
20 15:02:37 250313-sub 1 1H sub + + + + + + + SB-SFD-1 CF1 DPND-7 dimer with 1,4 Ph spacer CDCl3
19 14:46:36 250313-jsm 3 13C.day jsm - + + - - + + JM283 repeat
19 14:39:47 250313-jsm 2 11B jsm - + + - - + + JM283 repeat
19 14:32:44 250313-jsm 1 1H jsm + + + + + + + JM283 repeat
18 14:23:43 250313-z5485590 3 1H z5485590 + + + + + + + MM321-0min
17 14:13:56 250313-z5485590 2 1H z5485590 + + + + + + + MM321-180min-column
16 14:03:38 250313-z5485590 1 1H z5485590 + + + + + + + MM321-180min
15 13:46:13 250313-jlt 17 1H jlt + + + + + + + X-3106-fum-Weber250313
14 13:29:07 250313-jlt 16 1H jlt + + + + + + + X-3093-ox-Weber250313
13 13:11:12 250313-jlt 15 1H jlt + + + + + + + ExtStd-Weber250313
12 13:04:13 250313-jlt 14 1H jlt + + + + + + + JT-blank
11 12:05:19 250313-dem 2 1H dem + + + + + + + chloroform_t-24h
10 11:57:51 250313-dem 1 1H dem + x + + + + + chloroform_t0 ATM Failed
9 11:49:04 250313-amn 1 1H amn + + + + + + + AMM - H004 - ZnTMP after plug and vac down in Tol-d8
8 11:44:37 250313-z5493478 2 19F z5493478 - + + - - + + SIC048-crystals CDCl3 Weber
8 11:38:13 250313-z5493478 1 1H z5493478 + + + + + + + SIC048-crystals CDCl3 Weber
7 11:28:23 250313-jnn 3 19F{1H} jnn - + + - - + + JAN-204.1
7 11:19:09 250313-jnn 2 19F jnn - + + - - + + JAN-204.1
7 11:10:01 250313-jnn 1 1H jnn + x + + + + + JAN-204.1 ATM Failed
6 10:46:17 250313-jlt 13 19F{1H} jlt - + + - - + + X-3112-fum-19F{1H}
6 10:40:11 250313-jlt 12 1H jlt + + + + + + + X-3112-fum-19F{1H}
5 10:35:43 250313-jlt 11 19F{1H} jlt - + + - - + + X-3109-fum-19F{1H}
5 10:29:23 250313-jlt 10 1H jlt + + + + + + + X-3109-fum-19F{1H}
4 10:22:39 250313-jlt 9 19F{1H} jlt - + + - - + + X-3006-fum-19F{1H}
4 10:16:39 250313-jlt 8 1H jlt + + + + + + + X-3006-fum-19F{1H}
3 10:12:16 250313-jlt 7 19F{1H} jlt - + + - - + + JT-2501-t24-30-fum-19F{1H}
3 10:06:14 250313-jlt 6 1H jlt + + + + + + + JT-2501-t24-30-fum-19F{1H}
2 10:02:24 250313-jlt 5 19F{1H} jlt - x + - - + + JT-2501-t14-20-fum-19F{1H} ATM Failed
2 09:56:12 250313-jlt 4 1H jlt + + + + + + + JT-2501-t14-20-fum-19F{1H}
1 09:36:59 250313-jlt 3 1H13C.hsqc.aded jlt - x + - - + + JT-P5J5-06B-fb-19F{1H} ATM Failed
1 09:31:34 250313-jlt 2 19F{1H} jlt - + + - - + + JT-P5J5-06B-fb-19F{1H}
1 09:23:27 250313-jlt 1 1H jlt + + + + + + + JT-P5J5-06B-fb-19F{1H}
18 00:39:45 250312-z3543503 6 13C.night z3543503 + + + + + + + EB11r
11 00:32:55 250312-z3545554 2 1H z3545554 + x + + + + + ATM Failed
10 00:26:25 250312-z3545554 1 1H z3545554 - - - - - - -
1 00:13:29 250312-suj 4 13C.day suj - + + - - + + ss-23-13 cf2 37-45
1 00:03:53 250312-suj 3 1H suj + + + + + + + ss-23-13 cf2 37-45
60 23:50:42 250312-suj 2 13C.day suj - + + - - + + ss-25-01 crude large scale after workup
60 23:43:52 250312-suj 1 1H suj + + + + + + + ss-25-01 crude large scale after workup
59 23:36:31 250312-rdr 1 1H rdr + + + + + + + 2-018 0.9 indole eq
58 23:23:28 250312-thh 2 13C.day thh - + + - - + + TA-60
58 23:14:54 250312-thh 1 1H thh + + + + + + + TA-60
57 22:09:59 250312-jlt 6 13C.night jlt - + + - - + + JT-P5JR-04B-col
57 22:04:53 250312-jlt 5 19F{1H} jlt - + + - - + + JT-P5JR-04B-col
57 21:54:11 250312-jlt 4 1H jlt + + + + + + + JT-P5JR-04B-col
56 20:48:59 250312-jlt 3 13C.night jlt - + + - - + + JT-P5JS-02-col-t21-22
56 20:43:55 250312-jlt 2 19F{1H} jlt - + + - - + + JT-P5JS-02-col-t21-22
56 20:34:57 250312-jlt 1 1H jlt + x + + + + + JT-P5JS-02-col-t21-22 ATM Failed
55 20:25:14 250312-sub 5 1H sub + + + + + + + SB145-D aliquot 2 Protection of aldehyde indole CDCl3
54 20:15:37 250312-sub 4 1H sub + + + + + + + SB-SFD-1 aliquot 1 Dimer of DPND-7 with 1,4 phenyl spacer CDCl3
53 20:03:05 250312-z5438782 1 1H z5438782 + + + + + + + elp bisttc 565 nm t0
52 19:57:12 250312-z5550254 15 19F{1H} z5550254 - + + - - + + AY-068.2
52 19:50:54 250312-z5550254 14 19F z5550254 - + + - - + + AY-068.2
52 19:36:24 250312-z5550254 13 1H z5550254 + + + + + + + AY-068.2
51 19:30:20 250312-z5550254 12 19F{1H} z5550254 - + + - - + + AY-068.1
51 19:24:54 250312-z5550254 11 19F z5550254 - + + - - + + AY-068.1
51 19:10:16 250312-z5550254 10 1H z5550254 + + + + + + + AY-068.1
50 19:02:56 250312-jcy 6 1H jcy + + + + + + + VP-02-03-T6h
49 18:56:17 250312-jcy 5 1H jcy + x + + + + + VP-02-02-T6h ATM Failed
48 18:48:47 250312-jcy 4 1H jcy + + + + + + + VP-02-01-T6h
47 18:39:26 250312-jcy 3 1H jcy + + + + + + + VP-02-03-T0
46 18:31:19 250312-jcy 2 1H jcy + x + + + + + VP-02-02-T0 ATM Failed
45 18:23:41 250312-jcy 1 1H jcy + + + + + + + VP-02-01-T0
44 18:14:10 250312-mda 3 1H mda + x + + + + + Supernatent_BT ATM Failed
43 18:05:39 250312-mda 2 1H mda + + + + + + + Purified 3MBT-CD
42 17:57:50 250312-mda 1 1H mda + + + + + + + Purified 3MBT-DM
41 17:49:38 250312-z5485590 9 1H z5485590 + + + + + + + MM318-60min-column
40 17:39:57 250312-z5485590 8 1H z5485590 + + + + + + + MM318-60min
39 17:30:20 250312-z5485590 7 1H z5485590 + + + + + + + MKA45-ppt
38 17:25:54 250312-z5493478 2 19F z5493478 - + + - - + + SIC048-Fr.3-30 CDCl3 Weber
38 17:19:19 250312-z5493478 1 1H z5493478 + + + + + + + SIC048-Fr.3-30 CDCl3 Weber
37 17:13:00 250312-z5550254 9 19F{1H} z5550254 - + + - - + + AY-068.3
37 17:07:05 250312-z5550254 8 19F z5550254 - + + - - + + AY-068.3
37 16:53:02 250312-z5550254 7 1H z5550254 + + + + + + + AY-068.3
36 16:47:01 250312-z5550254 6 19F{1H} z5550254 - + + - - + + AY-068.2
36 16:40:53 250312-z5550254 5 19F z5550254 - + + - - + + AY-068.2
36 16:26:59 250312-z5550254 3 1H z5550254 + + + + + + + AY-068.2
35 16:20:39 250312-z5550254 4 19F{1H} z5550254 - + + - - + + AY-068.1
35 16:13:56 250312-z5550254 2 19F z5550254 - + + - - + + AY-068.1
35 16:00:15 250312-z5550254 1 1H z5550254 + + + + + + + AY-068.1
34 14:51:29 250312-ild 3 13C.night ild + + + + + + + ID12027; CDCl3
33 14:44:26 250312-yab 1 1H yab + + + + + + + TROPL_NH_CR
32 14:35:50 250312-z5426952 1 1H z5426952 + + + + + + + RI-OH-1 Pure
31 14:26:30 250312-z5485590 6 1H z5485590 + + + + + + + MM318-0min-column
30 14:17:58 250312-z5485590 5 1H z5485590 + + + + + + + MM318-0min
29 14:07:52 250312-z5485590 4 1H z5485590 + + + + + + + MM319-60min-column
28 13:59:51 250312-z5485590 3 1H z5485590 + + + + + + + MM319-60min
27 13:51:06 250312-z5485590 2 1H z5485590 + + + + + + + MM319-0min-column
26 13:43:10 250312-z5485590 1 1H z5485590 + + + + + + + MM319-0min
25 13:33:38 250312-z5628481 1 1H z5628481 + + + + + + + me-01d hcl wu ext 1H
24 13:26:23 250312-sub 3 1H sub + + + + + + + SB100-F CF2 DPND-7-Br CDCl3
23 13:18:53 250312-sub 2 1H sub + + + + + + + SB100-F CF1 DPND-7-Br CDCl3
22 13:11:13 250312-djg 2 1H djg + x + + + + + DJG-B-143 Add TMSCl Frac 2-3 ATM Failed
21 13:02:43 250312-djg 1 1H djg + + + + + + + DJG-B-143 Add TMSCl Frac 1
20 12:54:18 250312-ogc 1 1H ogc + + + + + + + OG8021, Constrained AALS transfer hydrog 23 h, CDCl3
19 12:41:28 250312-ild 2 13C.day ild - + + - - + + ID12023; ether trits; CDCl3
19 12:32:53 250312-ild 1 1H ild + + + + + + + ID12023; ether trits; CDCl3
18 12:19:32 250312-z3543503 5 13C.day z3543503 - + + - - + + EB11r
18 12:13:33 250312-z3543503 4 1H z3543503 + + + + + + + EB11r
17 12:07:14 250312-z3543503 3 bbfo.1H.qnmr z3543503 - + + - - + + EB11r 2
17 12:03:35 250312-z3543503 2 19F z3543503 - x + - - + + EB11r 2 ATM Failed
17 11:56:36 250312-z3543503 1 1H z3543503 + + + + + + + EB11r 2
16 11:48:20 250312-iconnmr 5 sst.31P.sen iconnmr + + + + + + + 31P Sensitivity 0.0485 M triphenylphosphate (TPP) in d6-acetone Specification result of sinocal: Best sino value found ( > 150:1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/5/pdata/1/250312-iconnmr_5_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/5/pdata/1/250312-iconnmr_5_1.pdf Check for printing system problems
15 11:36:49 250312-iconnmr 4 sst.19F.qnp.sen iconnmr + + + + + + + 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found ( > 250 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/4/pdata/1/250312-iconnmr_4_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/4/pdata/1/250312-iconnmr_4_1.pdf Check for printing system problems
14 11:11:49 250312-iconnmr 3 sst.13C.sen iconnmr + x + + + + + 13C Sensitivity 10% Ethylbenzene (EB) in CDCl3 Specification result of sinocal: Best sino value found ( > 200 :1) ATM Failed, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/3/pdata/1/250312-iconnmr_3_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/3/pdata/1/250312-iconnmr_3_1.pdf Check for printing system problems
13 11:00:29 250312-iconnmr 2 sst.1H.sen iconnmr + + + + + + + 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found ( > 300 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/2/pdata/1/250312-iconnmr_2_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/2/pdata/1/250312-iconnmr_2_1.pdf Check for printing system problems
12 10:50:53 250312-iconnmr 1 sst.1H.lsh iconnmr + + + + + + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/1/pdata/1/250312-iconnmr_1_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250312-iconnmr/1/pdata/1/250312-iconnmr_1_1.pdf Check for printing system problems
11 10:44:58 250312-z5489717 2 1H z5489717 + + + + + + + DSM-R209-overnight-crude-vac.-filt. CDCl3
10 10:37:43 250312-z5489717 1 1H z5489717 + + + + + + + DSM-R208-overnight-crude-vac. CDCl3
9 10:25:36 250312-sub 1 1H sub + + + + + + + SB145-D aliquot 1 protecting aldehyde group CDCl3
9 01:11:24 250311-suj 9 13C.day suj + + + + + + + ss-23-13 cf2 46+47
8 00:58:27 250311-suj 8 13C.day suj - + + - - + + ss-23-13 cf2 41-45
8 00:51:42 250311-suj 7 1H suj + + + + + + + ss-23-13 cf2 41-45
7 00:38:51 250311-suj 6 13C.day suj - + + - - + + ss-23-13 cf2 37-40
7 00:32:02 250311-suj 5 1H suj + + + + + + + ss-23-13 cf2 37-40
6 00:18:59 250311-suj 4 13C.day suj - + + - - + + ss-23-13 cf2 34-36
6 00:11:28 250311-suj 3 1H suj + + + + + + + ss-23-13 cf2 34-36
5 23:03:50 250311-rdr 4 13C.night rdr + x + + + + + 2-018 RT then 60 orange ATM Failed
4 21:51:36 250311-rdr 3 13C.night rdr + + + + + + + 2-018 RT then 60 white
3 20:59:11 250311-suj 2 1H suj + + + + + + + ss-23-13 cf2 46+47
2 20:44:58 250311-rdr 2 1H rdr + + + + + + + 2-018 RT then 60C after column orange
1 20:36:44 250311-rdr 1 1H rdr + + + + + + + 2-018 RT then 60C after column white
60 20:29:18 250311-att 8 1H att + + + + + + + SA-30-4 DMSO-d6 HNMR 11/3
59 20:21:02 250311-att 7 1H att + + + + + + + SA-30-3 HNMR DMSO-d6 11/3
58 20:12:08 250311-att 6 19F att - + + - - + + MNO2MPhOTf CDCl3 HNMR 11/3
58 19:59:01 250311-att 5 13C.day att - + + - - + + MNO2MPhOTf CDCl3 HNMR 11/3
58 19:48:25 250311-att 4 1H att + + + + + + + MNO2MPhOTf CDCl3 HNMR 11/3
57 19:40:44 250311-att 3 1H att + + + + + + + MNO2MPhVin CDCl3 HNMR 11/3
56 19:29:46 250311-att 2 1H att + + + + + + + MNO2MVinOMe CDCl3 HNMR 11/3
55 19:21:14 250311-att 1 1H att + + + + + + + MNO2MVin HNMR CDCl3 11/3
54 19:16:41 250311-z5493478 2 19F z5493478 - + + - - + + SIC048-crude CDCl3 Weber
54 19:09:40 250311-z5493478 1 1H z5493478 + + + + + + + SIC048-crude CDCl3 Weber
53 18:56:15 250311-djg 6 1H13C.hmbc djg - + + - - + + DJG-B-143 ElectraSyn PMDI TMSCl 15 eq. Frac 8-13
53 18:37:30 250311-djg 5 1H13C.hsqc.aded djg - + + - - + + DJG-B-143 ElectraSyn PMDI TMSCl 15 eq. Frac 8-13
53 18:26:15 250311-djg 4 1H.cosy djg - + + - - + + DJG-B-143 ElectraSyn PMDI TMSCl 15 eq. Frac 8-13
53 18:23:32 250311-djg 3 1H djg - + + - - + + DJG-B-143 ElectraSyn PMDI TMSCl 15 eq. Frac 8-13
53 17:14:54 250311-djg 2 13C.night djg + + + + + + + DJG-B-143 ElectraSyn PMDI TMSCl 15 eq. Frac 8-13 ADC reported overflow
52 17:05:49 250311-z5485590 9 1H z5485590 + + + + + + + MM317-180min
51 16:53:57 250311-z5485590 8 1H z5485590 + + + + + + + MM317-120min
50 16:45:52 250311-z5485590 7 1H z5485590 + + + + + + + MM317-60min
49 16:36:07 250311-z5485590 6 1H z5485590 + + + + + + + MM317-30min
48 16:26:52 250311-z5485590 5 1H z5485590 + + + + + + + MM317-15min
47 16:18:17 250311-z5485590 4 1H z5485590 + + + + + + + MM317-5min
46 16:11:08 250311-djg 1 1H djg + + + + + + + DJG-B-143 ElectraSyn PMDI TMSCl 15 eq. Frac 8-13
45 16:03:36 250311-kee 3 1H kee + + + + + + + RAFT Methylation
44 15:52:59 250311-kee 2 1H kee + + + + + + + ELP tf1
43 15:46:29 250311-kee 1 1H kee + + + + + + + 3k purified 1
42 15:36:27 250311-zhz 1 1H zhz + + + + + + + ZZ-098 worked up
41 15:29:10 250311-z5489717 1 1H z5489717 + + + + + + + DSM-R208-4h-crude-vac CDCl3
40 15:21:03 250311-z5485590 3 1H z5485590 + + + + + + + MM317-0min
39 15:12:39 250311-z5485590 2 1H z5485590 + + + + + + + MM316-60min
38 15:03:18 250311-z5485590 1 1H z5485590 + + + + + + + MM316-0min
37 14:55:07 250311-z5408582 2 1H.es z5408582 + + + + + + + 21
36 14:47:55 250311-z5408582 1 1H.es z5408582 + + + + + + + 20
35 14:40:47 250311-z5167506 7 1H z5167506 + x + + + + + JF GluTMS CDCl3 ATM Failed
34 14:34:51 250311-z5550254 4 19F{1H} z5550254 - + + - - + + AY-068.crude
34 14:28:58 250311-z5550254 3 19F z5550254 - + + - - + + AY-068.crude
34 14:15:39 250311-z5550254 2 1H z5550254 + x + + + + + AY-068.crude ATM Failed
33 13:59:57 250311-z5550254 1 1H z5550254 + + + + + + + AY-054.1
32 13:50:36 250311-ogc 1 1H ogc + + + + + + + OG8019, Thiophene KSAc sub crude, CDCl3
31 12:56:14 250311-ild 1 1H ild + + + + + + + ID12029; boc piperazine SNAr cr; CDCl3
30 12:36:42 250311-z3545554 1 1H z3545554 + + + + + + +
15 12:29:05 250311-suj 1 1H suj + + + + + + + ss-23-13 cf0-6
14 12:20:31 250311-z5167506 5 1H z5167506 + + + + + + + 84 T20 CDCl3
13 12:11:16 250311-z5167506 6 1H z5167506 + + + + + + + 84 T0 CDCl3
12 12:03:14 250311-z5167506 4 1H z5167506 + + + + + + + 66 T20 CDCl3
11 11:53:13 250311-z5167506 3 1H z5167506 + + + + + + + 66 T0 CDCl3
10 11:43:43 250311-z5167506 2 1H z5167506 + + + + + + + 14 T20 CDCl3
9 11:32:52 250311-z5167506 1 1H z5167506 + + + + + + + 14 T0 CDCl3
8 11:28:21 250311-vaf 4 19F{1H} vaf - + + - - + + 4.40-3
8 11:19:01 250311-vaf 3 19F vaf + + + + + + + 4.40-3
7 11:07:31 250311-yux 1 1H yux + x + + + + + 10032025 rithik pba133-phea66 17h cr ATM Failed
49 11:03:03 250311-z3543503 10 bbfo.1H.qnmr z3543503 - + + - - + + EB11r 2 CHCl3
49 10:58:50 250311-z3543503 9 19F z3543503 - + + - - + + EB11r 2 CHCl3
49 10:52:30 250311-z3543503 8 1H z3543503 + + + + + + + EB11r 2 CHCl3
48 10:39:14 250311-z3543503 7 bbfo.1H.qnmr z3543503 + + + + + + + EB11r 1 CHCl3 wash
47 10:34:33 250311-z3543503 6 bbfo.1H.qnmr z3543503 - + + - - + + EB11r 2 CHCl3 wash
47 10:30:42 250311-z3543503 5 19F z3543503 - + + - - + + EB11r 2 CHCl3 wash
47 10:25:17 250311-z3543503 4 1H z3543503 - + + + + + + EB11r 2 CHCl3 wash
47 10:19:44 250311-z3543503 6 bbfo.1H.qnmr z3543503 - - - - - - - EB11r 2 CHCl3 wash Automation was stopped by user
47 10:17:08 250311-z3543503 5 19F z3543503 - x + - - x - EB11r 2 CHCl3 wash
47 10:07:02 250311-z3543503 4 1H z3543503 + x + + x x - EB11r 2 CHCl3 wash
46 10:05:23 250311-z3543503 3 bbfo.1H.qnmr z3543503 - - - - - - - EB11r 1 CHCl3 wash
46 10:00:36 250311-z3543503 2 19F z3543503 - + + - - + + EB11r 1 CHCl3 wash
46 09:53:36 250311-z3543503 1 1H z3543503 + + + + + + + EB11r 1 CHCl3 wash
6 08:47:42 250310-jlt 17 13C.night jlt - + + - - + + JT-X-2501-col-t24-30 ADC reported overflow
6 08:42:52 250310-jlt 16 19F{1H} jlt - + + - - + + JT-X-2501-col-t24-30
6 08:08:06 250310-jlt 15 1H.noesy jlt - + + - - + + JT-X-2501-col-t24-30
6 07:43:56 250310-jlt 14 1H13C.hmbc jlt - + + - - + + JT-X-2501-col-t24-30
6 07:25:02 250310-jlt 13 1H13C.hsqc.aded jlt - + + - - + + JT-X-2501-col-t24-30
6 07:13:46 250310-jlt 12 1H.cosy jlt - + + - - + + JT-X-2501-col-t24-30
6 07:03:45 250310-jlt 11 1H jlt + x + + + + + JT-X-2501-col-t24-30 ATM Failed
5 05:58:40 250310-jlt 10 13C.night jlt - + + - - + + JT-X-2501-col-t14-20
5 05:53:26 250310-jlt 9 19F{1H} jlt - + + - - + + JT-X-2501-col-t14-20
5 05:18:45 250310-jlt 8 1H.noesy jlt - + + - - + + JT-X-2501-col-t14-20
5 04:54:45 250310-jlt 7 1H13C.hmbc jlt - + + - - + + JT-X-2501-col-t14-20
5 04:33:40 250310-jlt 6 1H13C.hsqc.aded jlt - + + - - + + JT-X-2501-col-t14-20
5 04:22:23 250310-jlt 5 1H.cosy jlt - + + - - + + JT-X-2501-col-t14-20
5 04:12:33 250310-jlt 4 1H jlt + + + + + + + JT-X-2501-col-t14-20
4 03:07:11 250310-jlt 3 13C.night jlt - + + - - + + JT-X-3112-fb-char
4 03:01:39 250310-jlt 2 19F{1H} jlt - + + - - + + JT-X-3112-fb-char
4 02:51:01 250310-jlt 1 1H jlt + + + + + + + JT-X-3112-fb-char
3 02:43:14 250310-z5540930 1 1H z5540930 + + + + + + + 1MBT-RR
2 02:34:14 250310-z5485590 15 1H z5485590 + + + + + + + MM315-60min
1 02:22:20 250310-z5485590 14 1H z5485590 + + + + + + + MM315-0min
60 02:14:17 250310-z5485590 13 1H z5485590 + + + + + + + MM314-60min
59 02:05:54 250310-z5485590 12 1H z5485590 + + + + + + + MM314-0min
58 01:55:39 250310-z5485590 11 1H z5485590 + + + + + + + MM313-60min
57 01:47:05 250310-z5485590 10 1H z5485590 + + + + + + + MM313-0min
56 01:37:52 250310-z5485590 9 1H z5485590 + + + + + + + MM312-60min
55 01:31:22 250310-z5408582 10 1H.es z5408582 + x + + + + + 19 ATM Failed
54 01:23:21 250310-z5408582 9 1H.es z5408582 + x + + + + + 18 ATM Failed
53 01:16:43 250310-z5408582 8 1H.es z5408582 + + + + + + + 17
52 01:09:41 250310-z5408582 7 1H.es z5408582 + + + + + + + 16
51 01:03:29 250310-z3545554 2 1H z3545554 + x + + + + + ATM Failed
50 00:56:05 250310-z3545554 1 1H z3545554 + + + + + + +
45 00:40:39 250310-thh 1 13C.day thh + x + + + + + TA-00 ATM Failed
44 00:33:53 250310-z5492625 3 1H z5492625 + + + + + + + JC-076-F08-F11
43 00:25:41 250310-z5492625 2 1H z5492625 + + + + + + + JC-076-F06
42 21:50:19 250310-ccl 3 ccl.13C.DAELIM nmrcomm + + + + + + + NMR-2025-08 25058-2, ID-25025 401.85mg in 600uLCDCl3
41 19:14:32 250310-ccl 2 ccl.13C.DAELIM nmrcomm + + + + + + + NMR-2025-08 25058-1, ID-25024 413.23mg in 600uLCDCl3
40 16:38:53 250310-ccl 1 ccl.13C.DAELIM nmrcomm + + + + + + + CDCl3 screening
39 16:31:02 250310-jsm 1 1H jsm + + + + + + + AB-2 (TMP distillation)
37 16:22:22 250310-z5289573 2 1H z5289573 + + + + + + + JL127 3h
36 16:15:53 250310-z5289573 1 1H z5289573 + + + + + + + JL127 0h
35 16:08:00 250310-zhz 1 1H zhz + + + + + + + ZZ-098 crude
34 15:51:47 250310-z5319902 1 13C.dept135 z5319902 + + + + + + + AA-020 Frac 2
33 15:45:47 250310-z5628481 2 1H z5628481 + + + + + + + me-02d cond 1 wu precip 1H
32 15:38:14 250310-z5628481 1 1H z5628481 + + + + + + + Me-02d aq layer b wu 1H
31 15:33:56 250310-z5493478 4 19F z5493478 - + + - - + + SIC047-2 Fr.31-32 CDCl3 Weber
31 15:26:56 250310-z5493478 3 1H z5493478 + + + + + + + SIC047-2 Fr.31-32 CDCl3 Weber
30 15:20:22 250310-z5493478 2 19F z5493478 - + + - - + + SIC047-2 Fr.33-2.6 CDCl3 Weber
30 15:13:02 250310-z5493478 1 1H z5493478 + + + + + + + SIC047-2 Fr.33-2.6 CDCl3 Weber
29 15:06:10 250310-z5489717 1 1H z5489717 + + + + + + + DSM-R204a-f6-8 CDCl3
28 14:57:51 250310-z5564533 3 1H z5564533 + + + + + + + CM-054-5
27 14:50:48 250310-z5564533 2 1H z5564533 + + + + + + + CM-054-2
26 14:44:12 250310-z5564533 1 1H z5564533 + + + + + + + CM-054-1
25 14:35:05 250310-z5485590 8 1H z5485590 + + + + + + + MM310-PMMA
24 14:27:01 250310-z5485590 7 1H z5485590 + x + + + + + MM292-PMMA ATM Failed
23 14:17:12 250310-z5485590 6 1H z5485590 + + + + + + + MM98-PMMA
22 14:08:40 250310-z5485590 5 1H z5485590 + + + + + + + MM312-0min
21 14:00:22 250310-z5485590 4 1H z5485590 + + + + + + + MM311-60min
20 13:52:07 250310-z5485590 3 1H z5485590 + + + + + + + MM311-0min
19 13:42:53 250310-z5485590 2 1H z5485590 + + + + + + + MM310-60min
18 13:34:29 250310-z5485590 1 1H z5485590 + + + + + + + MM310-0min
17 13:29:28 250310-vaf 2 19F{1H} vaf - + + - - + + 4.40-FMorph-Fnmr
17 13:19:00 250310-vaf 1 19F vaf + + + + + + + 4.40-FMorph-Fnmr
16 11:41:57 250310-suj 1 1H suj + + + + + + + ss-23-13
15 11:34:39 250310-ogc 1 1H ogc + x + + + + + OG7101, Dimethyl bromo diamide thiophene check, CDCl3 ATM Failed
14 11:26:24 250310-z5167506 2 1H z5167506 + + + + + + + PLACy5 DMSO
13 11:18:38 250310-z5167506 1 1H z5167506 + + + + + + + PLA DMSO
12 11:07:47 250310-z5492625 1 1H z5492625 + + + + + + + JC-076-crude
11 11:01:22 250310-z5426952 1 1H z5426952 + + + + + + + RI-D-OAc-2
10 10:54:23 250310-z5408582 6 1H.es z5408582 + + + + + + + 15
9 10:48:26 250310-z5408582 5 1H.es z5408582 + x + + + + + 14 ATM Failed
8 10:41:14 250310-z5408582 4 1H.es z5408582 + + + + + + + 13
7 10:34:12 250310-z5408582 3 1H.es z5408582 + + + + + + + 12
6 10:27:28 250310-z5408582 2 1H.es z5408582 + + + + + + + 11
5 10:20:31 250310-z5408582 1 1H.es z5408582 + + + + + + + 10
4 10:10:19 250310-z3543503 12 bbfo.1H.qnmr z3543503 - + + - - + + EB11r crude liq
4 10:05:57 250310-z3543503 11 19F z3543503 - + + - - + + EB11r crude liq
4 09:59:11 250310-z3543503 10 1H z3543503 + + + + + + + EB11r crude liq
3 09:52:57 250310-z3543503 9 bbfo.1H.qnmr z3543503 - + + - - + + EB11r sol weekend
3 09:48:47 250310-z3543503 8 19F z3543503 - + + - - + + EB11r sol weekend
3 09:42:29 250310-z3543503 7 1H z3543503 + + + + + + + EB11r sol weekend
2 09:36:52 250310-z3543503 6 bbfo.1H.qnmr z3543503 - + + - - + + EB11r sol rovap
2 09:32:24 250310-z3543503 5 19F z3543503 - + + - - + + EB11r sol rovap
2 09:25:53 250310-z3543503 4 1H z3543503 + + + + + + + EB11r sol rovap
1 09:20:25 250310-z3543503 3 bbfo.1H.qnmr z3543503 - + + - - + + EB11r sol
1 09:16:22 250310-z3543503 2 19F z3543503 - + + - - + + EB11r sol
1 09:07:03 250310-z3543503 1 1H z3543503 + + + + + + + EB11r sol
14 17:34:29 250309-jnn 9 19F{1H} jnn - + + - - + + JAN-203.3
14 17:25:41 250309-jnn 8 19F jnn - + + - - + + JAN-203.3
14 17:16:21 250309-jnn 7 1H jnn + + + + + + + JAN-203.3
13 17:07:31 250309-jnn 6 19F{1H} jnn - + + - - + + JAN-203.2
13 16:58:57 250309-jnn 5 19F jnn - + + - - + + JAN-203.2
13 16:47:42 250309-jnn 4 1H jnn + + + + + + + JAN-203.2
12 16:37:15 250309-jnn 3 19F{1H} jnn - + + - - + + JAN-203.1
12 16:27:41 250309-jnn 2 19F jnn - + + - - + + JAN-203.1
12 16:18:40 250309-jnn 1 1H jnn + + + + + + + JAN-203.1
11 15:48:06 250309-z5438782 7 1H z5438782 + + + + + + + elp bisttc 6h
10 14:19:25 250309-z5438782 6 1H z5438782 + + + + + + + elp-bisttc 4h
9 13:22:27 250309-z5537965 1 1H z5537965 + + + + + + + Block CBA-Posy deprotection_3.3.25
8 11:51:54 250309-z5438782 5 1H z5438782 + + + + + + + elp disttc 2h
7 11:44:49 250309-mda 2 1H mda + + + + + + + 1MBT_RR
6 11:37:03 250309-mda 1 1H mda + + + + + + + T12-3MBT
5 11:26:53 250309-z5438782 4 1H z5438782 + x + + + + + elp disttc 1h ATM Failed
4 11:15:43 250309-z5438782 3 1H z5438782 + + + + + + + elp disttc 30min
3 11:06:05 250309-z5438782 2 1H z5438782 + + + + + + + elp disttc 15min
2 10:54:44 250309-z5438782 1 1H z5438782 + + + + + + + elp disttc t0
1 14:14:01 250308-yab 2 13C.day yab - x + - - + + 1E3_P+_TR ATM Failed
1 14:06:47 250308-yab 1 1H yab + + + + + + + 1E3_P+_TR
50 13:56:40 250308-z3542072 6 1H z3542072 + + + + + + + MM-306-t60-filtre-cdcl3 ADC reported overflow
49 13:46:32 250308-z3542072 5 1H z3542072 + + + + + + + MM-306-t60-cdcl3
48 13:37:15 250308-z3542072 4 1H z3542072 + + + + + + + MM-306-t0-cdcl3
47 13:28:58 250308-z3542072 3 1H z3542072 + x + + + + + MM-307-t60-filtre-cdcl3 ATM Failed
46 13:17:46 250308-z3542072 2 1H z3542072 + + + + + + + MM-307-t60-cdcl3
45 13:09:15 250308-z3542072 1 1H z3542072 + + + + + + + MM-307-t0-cdcl3
44 12:22:57 250308-mda 1 1H mda + + + + + + + T0-3MBT
43 03:50:46 250308-z5408582 8 1H.es z5408582 + + + + + + + 9
42 03:43:52 250308-z5408582 7 1H.es z5408582 + + + + + + + 8
41 03:36:32 250308-z5408582 6 1H.es z5408582 + + + + + + + 7
40 03:30:03 250308-z5408582 5 1H.es z5408582 + + + + + + + 6
39 03:23:12 250308-z5408582 4 1H.es z5408582 + + + + + + + 5
38 03:14:45 250308-z5408582 3 1H.es z5408582 + + + + + + + 4
37 03:08:27 250308-z5408582 2 1H.es z5408582 + + + + + + + 3
36 03:01:13 250308-z5408582 1 1H.es z5408582 + + + + + + + 2
35 02:53:34 250307-jcy 3 1H jcy + + + + + + + SR-04-03-T45min
34 02:46:24 250307-jcy 2 1H jcy + + + + + + + SR-04-03-T30min
33 02:38:56 250307-jcy 1 1H jcy + + + + + + + SR-04-03-T15min
32 02:29:24 250307-z5485590 11 1H z5485590 + + + + + + + MM298-210min-again
31 02:21:44 250307-z5485590 10 1H z5485590 + + + + + + + MM302-180min-again
30 02:11:52 250307-z5485590 9 1H z5485590 + + + + + + + MM305-180min-again
29 02:02:37 250307-z5485590 8 1H z5485590 + + + + + + + MM305-180min
28 01:54:08 250307-z5485590 7 1H z5485590 + + + + + + + MM305-120min
27 00:49:38 250307-jlt 12 13C.night jlt - + + - - + + JT-P5JR-03-19F{1H}
27 00:37:33 250307-jlt 11 1H jlt + + + + + + + JT-P5JR-03-19F{1H}
26 23:32:37 250307-jlt 10 13C.night jlt - + + - - + + JT-P5JR-02-aliquot-char
26 23:27:30 250307-jlt 9 19F{1H} jlt - + + - - + + JT-P5JR-02-aliquot-char
26 23:08:33 250307-jlt 8 1H13C.hsqc.aded jlt - + + - - + + JT-P5JR-02-aliquot-char
26 22:56:06 250307-jlt 7 1H.cosy jlt - + + - - + + JT-P5JR-02-aliquot-char
26 22:43:30 250307-jlt 6 1H jlt + + + + + + + JT-P5JR-02-aliquot-char
25 21:38:21 250307-jlt 5 13C.night jlt - + + - - + + JT-P5JR-01-aliquot-char
25 21:33:07 250307-jlt 4 19F{1H} jlt - + + - - + + JT-P5JR-01-aliquot-char
25 21:13:56 250307-jlt 3 1H13C.hsqc.aded jlt - + + - - + x JT-P5JR-01-aliquot-char
25 21:02:52 250307-jlt 2 1H.cosy jlt - + + - - + + JT-P5JR-01-aliquot-char
25 20:49:43 250307-jlt 1 1H jlt + + + + + + + JT-P5JR-01-aliquot-char
24 20:44:32 250307-jsm 5 11B jsm - + + - - + + AB1-crude
24 20:34:18 250307-jsm 4 1H jsm + + + + + + + AB1-crude
23 18:27:38 250307-ccc 2 13C.night ccc - + + - - + + GC8059-13C; C6 6-quinoline amination; F6-27; DMSO; 400MHz ADC reported overflow
23 18:19:40 250307-ccc 1 1H ccc + + + + + + + GC8059; C6 6-quinoline amination; F6-27; DMSO; 400MHz
22 17:14:56 250307-jnn 5 13C.night jnn - + + - - + + JAN-199.4
22 17:05:15 250307-jnn 4 1H jnn + + + + + + + JAN-199.4
21 16:55:32 250307-jnn 3 1H jnn + + + + + + + JAN-201.1
20 15:49:37 250307-ild 2 13C.night ild - + + - - + + ID12025; AlMe3 coupling dried; CDCl3 ADC reported overflow
20 15:36:59 250307-ild 1 1H ild + + + + + + + ID12025; AlMe3 coupling dried; CDCl3
19 15:29:33 250307-z5537965 2 1H z5537965 + + + + + + + P2 T-24
18 15:21:38 250307-z5537965 1 1H z5537965 + + + + + + + Bock CBA-Post deprotection
17 15:13:17 250307-z5485590 6 1H z5485590 + + + + + + + MM305-60min
16 15:03:37 250307-z5485590 5 1H z5485590 + + + + + + + MM305-30min
15 14:54:36 250307-z5485590 4 1H z5485590 + + + + + + + MM305-20min
14 14:46:21 250307-z5485590 3 1H z5485590 + + + + + + + MM305-10min
13 14:34:31 250307-z5485590 2 1H z5485590 + + + + + + + MM305-5min
12 14:23:44 250307-z5485590 1 1H z5485590 + + + + + + + MM305-0min
11 14:16:36 250307-jsm 3 1H jsm + + + + + + + JM300pp
10 14:09:39 250307-jsm 2 1H jsm + + + + + + + JM300oo
9 14:01:37 250307-jsm 1 1H jsm + + + + + + + JM300nn
8 13:52:27 250307-z3541685 2 1H z3541685 + + + + + + + MWB_04_033c
7 13:45:04 250307-z3541685 1 1H z3541685 + + + + + + + MWB_04_023b
6 13:33:36 250307-amn 1 1H amn + x + + + + + AMM H004 - ZnTMP After Column in CDCl3 - Extended Range ATM Failed
5 13:24:22 250307-z3542072 10 1H z3542072 + + + + + + + MM-304-redo-t180cdcl3
4 13:15:51 250307-z3542072 9 1H z3542072 + + + + + + + MM-304-redo-t120cdcl3
3 13:07:47 250307-z3542072 8 1H z3542072 - - - - - - - MM-304-redo-t80cdcl3
2 12:58:28 250307-z3542072 7 1H z3542072 + + + + + + + MM-304-redo-t30cdcl3
1 12:49:04 250307-z3542072 6 1H z3542072 + + + + + + + MM-304-redo-t20cdcl3
60 12:42:19 250307-z5564533 2 1H z5564533 + + + + + + + CM-047-2
59 12:33:34 250307-z5564533 1 1H z5564533 + + + + + + + CM-047-1
58 11:58:47 250307-z5550254 1 1H z5550254 + + + + + + + AY-011
57 11:50:35 250307-z5167506 4 1H z5167506 + + + + + + + 11 T20 CDCl3
56 11:42:14 250307-z5167506 3 1H z5167506 + + + + + + + 11 T0 CDCl3
55 11:31:54 250307-z5167506 2 1H z5167506 + + + + + + + 5.5 T20 CDCl3
54 11:24:42 250307-z5167506 1 1H z5167506 + x + + + + + 5.5 T0 CDCl3 ATM Failed
53 11:18:51 250307-nnt 3 1H nnt + x + + + + + NT1-003 ATM Failed
52 11:15:12 250307-nnt 2 1H.es nnt - + + - - + + Onpattro + CP
52 11:08:34 250307-nnt 1 1H nnt + + + + + + + Onpattro + CP
51 11:03:35 250307-z5489717 4 19F z5489717 - x + - - + + DSM-R207-DCM ext.-TFT CDCl3 ATM Failed
51 10:57:24 250307-z5489717 3 1H z5489717 + + + + + + + DSM-R207-DCM ext.-TFT CDCl3
50 10:43:19 250307-z3542072 5 1H z3542072 + + + + x + + MM-304-t30-cdcl3 Shim failed
49 10:34:00 250307-z3542072 4 1H z3542072 + + + + x + + MM-304-t20min-cdcl3 Shim failed
48 10:24:07 250307-z3542072 3 1H z3542072 + + + + + + + MM-304-t10min-cdcl3
47 10:15:41 250307-z3542072 2 1H z3542072 + + + + + + + MM-304-t5min-cdcl3
46 10:06:45 250307-z3542072 1 1H z3542072 + x + + + + + MM-304-t0-cdcl3 ATM Failed
45 10:01:58 250307-z5489717 2 19F z5489717 - + + - - + + DSM-R207-overnight-direct-filt.-TFT CDCl3
45 09:53:20 250307-z5489717 1 1H z5489717 + + + + + + + DSM-R207-overnight-direct-filt.-TFT CDCl3
44 09:41:29 250307-jnn 2 1H jnn + + + + + + + JAN-200.2
43 09:31:29 250307-jnn 1 1H jnn + + + + + + + JAN-200.1
42 06:50:19 250306-z5408582 8 1H.es z5408582 + + + + + + + 1
41 06:43:21 250306-z5408582 7 1H.es z5408582 + + + + + + + 48
40 06:35:30 250306-z5408582 6 1H.es z5408582 + + + + + + + 47
39 06:26:29 250306-z5408582 5 1H.es z5408582 + + + + + + + 46
38 06:19:53 250306-z5408582 4 1H.es z5408582 + + + + + + + 45
37 06:12:24 250306-z5408582 3 1H.es z5408582 + x + + + + + 44 ATM Failed
36 06:05:58 250306-z3545554 2 1H z3545554 + + + + + + +
35 05:59:02 250306-z3545554 1 1H z3545554 + + + + + + +
31 04:53:47 250306-jlt 9 13C.night jlt - + + - - + + JT-4-F-MiPT-step2-col ADC reported overflow
31 04:48:06 250306-jlt 8 19F{1H} jlt - + + - - + + JT-4-F-MiPT-step2-col
31 04:35:35 250306-jlt 7 1H jlt + + + + + + + JT-4-F-MiPT-step2-col
30 03:28:32 250306-jlt 6 13C.night jlt - + + - - + + JT-4-F-Az-step2-col ADC reported overflow
30 03:23:13 250306-jlt 5 19F{1H} jlt - + + - - + + JT-4-F-Az-step2-col
30 03:10:28 250306-jlt 4 1H jlt + + + + + + + JT-4-F-Az-step2-col
29 02:05:29 250306-jlt 3 13C.night jlt - x + - - + + JT-P5JR-03-col ATM Failed
29 02:00:00 250306-jlt 2 19F{1H} jlt - + + - - + + JT-P5JR-03-col
29 01:47:18 250306-jlt 1 1H jlt + + + + + + + JT-P5JR-03-col
28 01:36:42 250306-sub 5 1H sub + + + + + + + SB147 org layer Protecting aldehyde D2O
27 01:24:13 250306-sub 4 1H sub + x + + + + + SB147 aq layer Protecting aldehyde D2O ATM Failed
26 01:14:29 250306-sub 3 1H sub + + + + + + + SB 146-C crude DIND with DMF and K2CO3 DMSO
25 01:04:26 250306-sub 2 1H sub + + + + + + + SB 146-C crude DIND with DMF and K2CO3 D2O
24 00:58:00 250306-sub 1 1H sub + + + + + + + Imidazole-CHO D2O
23 00:50:55 250306-jcy 6 1H jcy + + + + + + + SR-03-03-T1h
22 00:43:37 250306-jcy 5 1H jcy + + + + + + + SR-03-02-T1h
21 00:36:22 250306-jcy 4 1H jcy + + + + + + + SR-03-01-T1h
20 00:28:58 250306-jcy 3 1H jcy + + + + + + + SR-03-03-T0
19 00:19:53 250306-jcy 2 1H jcy + + + + + + + SR-03-02-T0
18 00:12:34 250306-jcy 1 1H jcy + + + + + + + SR-03-01-T0
17 00:03:36 250306-z3542072 28 1H z3542072 + + + + + + + MM-303-120min-cdcl3
16 21:56:48 250306-ccc 4 13C.night ccc - + + - - + + GC8059-13C; C6 6-quinoline amination; F6-27; DMSO; 400MHz
16 21:49:49 250306-ccc 3 1H ccc + + + + + + + GC8059; C6 6-quinoline amination; F6-27; DMSO; 400MHz
15 19:43:51 250306-ccc 2 13C.night ccc - x + - - + + GC8059-13C; C6 6-quinoline amination; col flush #1; DMSO; 400MHz ATM Failed, ADC reported overflow
15 19:36:46 250306-ccc 1 1H ccc + + + + + + + GC8059; C6 6-quinoline amination; col flush #1; DMSO; 400MHz
14 19:22:31 250306-pld 3 1H pld + + + + + + + PLD-3-110 mid
13 19:15:12 250306-ild 5 1H ild + + + + + + + ID12025; AlMe3 cr; CDCl3
12 19:07:15 250306-z3542072 27 1H z3542072 + + + + + + + MM-303-60min-cdcl3
11 18:58:21 250306-z3542072 26 1H z3542072 + + + + + + + MM-303-30min-cdcl3
10 18:49:04 250306-z3542072 25 1H z3542072 + + + + + + + MM-303-10min-cdcl3
9 18:40:47 250306-z3542072 24 1H z3542072 + + + + + + + MM-303-0min-cdcl3
8 18:31:49 250306-z3542072 23 1H z3542072 + + + + + + + MM-302-180min-cdcl3
7 18:23:51 250306-z3542072 22 1H z3542072 + + + + + + + MM-302-120min-cdcl3
6 18:14:21 250306-z3542072 21 1H z3542072 + + + + + + + MM-302-150min-cdcl3
5 17:57:51 250306-dem 1 1H dem + + + + + + + DM-MS-02-68E
4 17:52:58 250306-z5493478 8 19F z5493478 - + + - - + + SIC047-Fr.2.1-2.17 DMSO Weber
4 17:45:20 250306-z5493478 7 1H z5493478 + + + + + + + SIC047-Fr.2.1-2.17 DMSO Weber
3 17:38:59 250306-z5564533 5 1H z5564533 + + + + + + + catherine 1
2 17:32:12 250306-z5564533 4 1H z5564533 + + + + + + + CM-053-4
1 17:24:38 250306-z5537965 1 1H z5537965 + + + + + + + Block CBA_post A_03.03.25
60 17:16:57 250306-ild 4 1H ild + + + + + + + SRPK nanobret probe stability check t=24h; DMSO
59 17:09:29 250306-ild 3 1H ild + x + + + + + ET1133 check; DMSO ATM Failed
58 16:59:15 250306-ild 2 1H ild + + + + + + + ET1125 check; CDCl3
57 16:51:34 250306-mda 6 1H mda + + + + + + + T0-DM-HE
56 16:43:39 250306-mda 5 1H mda + + + + + + + BTPA
55 16:34:27 250306-mda 4 1H mda + + + + + + + 2.MBT Pol_CD
54 16:26:47 250306-mda 3 1H mda + + + + + + + 2.MBT Pol_DM
53 16:20:30 250306-pld 2 1H pld + + + + + + + PLD-3-54 mid
52 16:13:32 250306-pld 1 1H pld + + + + + + + PLD-3-54 ald
51 16:06:58 250306-z5371131 1 1H z5371131 + + + + + + + AM4.05 Thursday rxn check
50 15:58:33 250306-yab 1 1H yab + + + + + + + 1E3_P+_III_HEX
49 15:49:43 250306-z3542072 20 1H z3542072 + + + + + + + MM-302-60min-cdcl3
48 15:40:08 250306-z3542072 19 1H z3542072 + + + + + + + MM-302-t30min-cdcl3
47 15:30:45 250306-z3542072 18 1H z3542072 + + + + + + + MM-302-t20min-cdcl3
46 15:22:25 250306-z3542072 17 1H z3542072 + + + + + + + MM-302-t10min-cdcl3
45 15:14:15 250306-z3542072 16 1H z3542072 + + + + + + + MM-302-t5min-cdcl3
44 15:05:38 250306-z3542072 15 1H z3542072 + + + + + + + MM-302-t0min-cdcl3
43 14:57:01 250306-z5489717 2 1H z5489717 + + + + + + + DSM-R207-2h-direct-filt.-CDCl3
42 14:48:04 250306-rdr 7 1H rdr + + + + + + + 2-018 BF3
41 14:41:03 250306-rdr 6 1H rdr + + + + + + + 2-018 ZnOTf
40 14:32:58 250306-rdr 5 1H rdr + + + + + + + 2-018 FeOTf
39 14:25:37 250306-rdr 4 1H rdr + + + + + + + 2-018 pTSA
38 14:18:20 250306-rdr 3 1H rdr + + + + + + + 2-018 TfOH
37 14:10:47 250306-rdr 2 1H rdr + + + + + + + 2-018 Yb
36 14:03:40 250306-rdr 1 1H rdr + + + + + + + AlCl3 2-018
35 13:53:02 250306-djg 1 1H djg + + + + + + + DJG-S-014d Isopyrocoll malononitrile purity check + 1% py-d5
34 13:43:39 250306-z5547474 1 1H z5547474 + x + + + + + DBU in mixed solution before etching ATM Failed
32 13:29:26 250306-yac 4 13C.day yac - + + - - + + Y10043 ADC reported overflow
32 13:21:37 250306-yac 3 1H yac + + + + + + + Y10043
31 13:14:32 250306-z5564533 3 1H z5564533 + + + + + + + CM-053-3
30 13:06:14 250306-z5564533 2 1H z5564533 + + + + + + + CM-053-2
29 12:58:33 250306-z5564533 1 1H z5564533 + + + + + + + CM-053-1
28 12:49:31 250306-vkk 1 1H vkk + + + + + + + VKK-RAT test 1
27 12:41:03 250306-amn 1 1H amn + + + + + + + AMM - H001 - H2TMP After Recryst in CDCl3
26 12:34:44 250306-z5408582 2 1H.es z5408582 + x + + + + + 39-16 ATM Failed
25 12:28:20 250306-z5408582 1 1H.es z5408582 + x + + + + + 38 ATM Failed
24 12:24:13 250306-z5493478 6 19F z5493478 - + + - - + + SIC047-Fr.4-6 DMSO Weber
24 12:17:58 250306-z5493478 5 1H z5493478 + + + + + + + SIC047-Fr.4-6 DMSO Weber
23 12:13:44 250306-z5493478 4 19F z5493478 - + + - - + + SIC047-Fr.18-30 DMSO Weber
23 12:07:33 250306-z5493478 3 1H z5493478 + + + + + + + SIC047-Fr.18-30 DMSO Weber
22 12:03:03 250306-z5493478 2 19F z5493478 - + + - - + + SIC047-Fr.2.18-3.1 DMSO Weber
22 11:54:24 250306-z5493478 1 1H z5493478 + + + + + + + SIC047-Fr.2.18-3.1 DMSO Weber
21 11:43:27 250306-tat 1 1H tat + + + + + + + X2-4 ADC reported overflow
20 11:33:37 250306-z3542072 8 1H z3542072 + + + + + + + MM-301-t180min-cdcl3
19 11:25:17 250306-z3542072 7 1H z3542072 + + + + + + + MM-301-t120min-cdcl3
18 11:15:26 250306-z3542072 6 1H z3542072 + + + + + + + MM-301-t60min-cdcl3
17 11:07:28 250306-z5489717 1 1H z5489717 + + + + + + + DSM-Pyrrole-2-carboxaldehyde
16 10:59:50 250306-mda 2 1H mda + + + + + + + Purified 1MBT_CHF
15 10:51:23 250306-mda 1 1H mda + + + + + + + Purified 1MBT
14 10:15:27 250306-ild 1 1H ild + + + + + + + ET1110 (R) check; CDCl3
13 09:56:41 250306-yac 2 13C.day yac - + + - - + + Y10036 p3
13 09:46:15 250306-yac 1 1H yac + + + + + + + Y10036 p3
12 08:58:39 250306-z3542072 5 1H z3542072 + + + + + + + MM-301-t30min-cdcl3
11 08:49:52 250306-z3542072 4 1H z3542072 + + + + + + + MM-301-t20min-cdcl3
10 08:41:45 250306-z3542072 3 1H z3542072 + + + + + + + MM-301-t10min-cdcl3
9 08:32:08 250306-z3542072 2 1H z3542072 + + + + + + + MM-301-t5min-cdcl3
8 08:22:49 250306-z3542072 1 1H z3542072 + + + + + + + MM-301-t0min-cdcl3
7 02:09:44 250305-z5408582 5 1H.es z5408582 + + + + + + + 37
6 02:03:05 250305-z5408582 4 1H.es z5408582 + + + + + + + 36
5 01:54:45 250305-z5408582 3 1H.es z5408582 + + + + + + + 35
4 01:48:17 250305-z5408582 2 1H.es z5408582 + + + + + + + 34
3 01:41:07 250305-z5408582 1 1H.es z5408582 + + + + + + + 33
2 01:34:16 250305-z3545554 2 1H z3545554 + + + + + + +
1 01:27:49 250305-z3545554 1 1H z3545554 + + + + + + +
52 01:21:05 250305-ogc 6 1H ogc + + + + + + + OG8017, DNT8 Flush, CDCl3
51 01:14:12 250305-ogc 5 1H ogc + x + + + + + OG8017, DNT8 F16-20, CDCl3 ATM Failed
50 01:02:32 250305-ogc 4 1H ogc + + + + x + + OG8017, DNT8 F11-15, CDCl3 Shim failed
49 00:53:11 250305-z5485590 12 1H z5485590 + + + + + + + MM300-120min
48 00:43:31 250305-z5485590 11 1H z5485590 + + + + + + + MM300-60min
47 00:35:00 250305-z5485590 10 1H z5485590 + + + + + + + MM300-30min
46 00:26:55 250305-z5485590 9 1H z5485590 + + + + + + + MM300-0min
45 00:17:42 250305-z5485590 8 1H z5485590 + + + + + + + MM298-210min
44 00:09:27 250305-z5485590 7 1H z5485590 + + + + + + + MM298-120min
43 23:59:40 250305-z5485590 6 1H z5485590 + + + + + + + MM298-60min
42 23:49:18 250305-z5485590 5 1H z5485590 + + + + + + + MM298-30min
41 23:41:16 250305-z5485590 4 1H z5485590 + + + + + + + MM298-20min
40 23:32:22 250305-z5485590 3 1H z5485590 + + + + + + + MM298-10min
39 23:24:43 250305-z5485590 2 1H z5485590 + + + + + + + MM298-5min
38 23:13:06 250305-z5485590 1 1H z5485590 + + + + + + + MM298-0min
37 21:07:23 250305-ccc 7 13C.night ccc - x + - - + + GC8055-13C; C6 5-indole amination; F3-5; DMSO; 400MHz ATM Failed
37 21:00:58 250305-ccc 6 1H ccc + + + + + + + GC8055; C6 5-indole amination; F3-5; DMSO; 400MHz
36 18:53:57 250305-ccc 5 13C.night ccc - + + - - + + GC8055-13C; C6 5-indole amination; F8-18; DMSO; 400MHz ADC reported overflow
36 18:46:31 250305-ccc 4 1H ccc + + + + + + + GC8055; C6 5-indole amination; F8-18; DMSO; 400MHz
35 18:37:13 250305-mda 1 1H mda + + + + + + + T0-2.MBT
34 18:29:40 250305-z5426952 2 1H z5426952 + + + + + + + RI-OAc F2
33 18:22:45 250305-z5426952 1 1H z5426952 + + + + + + + RI-OAc F1
32 18:15:42 250305-z5489717 4 1H z5489717 + + + + + + + DSM-R205b-direct
31 18:09:07 250305-z5489717 3 1H z5489717 + + + + + + + DSM-R205a-direct
30 18:05:20 250305-z5489717 2 19F z5489717 - + + - - + + DSM-Rdihypyr-CF3-direct test
30 17:58:39 250305-z5489717 1 1H z5489717 + + + + + + + DSM-Rdihypyr-CF3-direct test
29 17:50:48 250305-amn 1 1H amn + + + + + + + AMM - Crude H003 - MesDPM after column - CDCl3 - Increased spectrum, range
28 17:44:05 250305-ogc 3 1H ogc + + + + + + + OG8015, Constrained AALS suzuki F13-21, CDCl3
27 17:33:46 250305-ogc 2 1H ogc + + + + + + + OG8015, Constrained AALS suzuki F6-12, CDCl3
26 17:25:03 250305-ogc 1 1H ogc + + + + + + + OG8015, Constrained AALS suzuki F5, CDCl3
25 17:15:25 250305-z3542072 16 1H z3542072 + + + + + + + MM-299-240min
24 17:05:39 250305-z3542072 15 1H z3542072 + + + + + + + MM-299-120min
23 16:56:50 250305-z3542072 14 1H z3542072 + + + + + + + MM-299-60min
22 16:46:51 250305-sub 3 1H sub + + + + + + + SB139-B(2) CF3 coupling 4-Pyr to DPND-7 CDCl3
21 16:34:32 250305-sub 2 1H sub + + + + + + + SB139-B(2) CF2 coupling 4-Pyr to DPND-7 CDCl3
20 16:24:30 250305-sub 1 1H sub + + + + + + + SB139-B(2) CF1 coupling 4-Pyr to DPND-7 CDCl3
19 16:17:35 250305-ccc 3 1H ccc + + + + + + + GC8055; C6 5-indole amination; F19-24; DMSO; 400MHz
18 16:09:41 250305-ccc 2 1H ccc + x + + + + + GC8055; C6 5-indole amination; F8-18; DMSO; 400MHz ATM Failed
17 16:02:17 250305-ccc 1 1H ccc + + + + + + + GC8055; C6 5-indole amination; F3-5; DMSO; 400MHz
16 15:52:39 250305-z5550254 7 1H z5550254 + + + + + + + AY-066.crude(cesium carbonate)
15 15:46:52 250305-z5550254 6 19F{1H} z5550254 - + + - - + + AY-065.2
15 15:41:36 250305-z5550254 5 19F z5550254 - + + - - + + AY-065.2
15 15:27:46 250305-z5550254 4 1H z5550254 + + + + + + + AY-065.2
14 15:21:12 250305-z5550254 3 19F{1H} z5550254 - + + - - + + AY-065.1
14 15:15:24 250305-z5550254 2 19F z5550254 - + + - - + + AY-065.1
14 15:01:33 250305-z5550254 1 1H z5550254 + + + + + + + AY-065.1
13 14:54:43 250305-yab 2 1H yab + + + + + + + 1EP+_III
12 14:47:10 250305-yab 1 1H yab + + + + + + + 1EP+_II_R
11 14:37:55 250305-z3542072 13 1H z3542072 + x + + + + + MM-299-cdcl3-t30min ATM Failed
10 14:26:37 250305-z3542072 12 1H z3542072 + + + + + + + MM-299-cdcl3-t20min
9 14:17:00 250305-z3542072 11 1H z3542072 + + + + + + + MM-299-cdcl3-t10min
8 14:09:02 250305-z3542072 10 1H z3542072 + + + + + + + MM-299-cdcl3-t5min
7 13:59:37 250305-z3542072 9 1H z3542072 + + + + + + + MM-299-cdcl3-t0
6 13:50:08 250305-z3542072 8 1H z3542072 + + + + + + + MM-296-t180min-cdcl3
5 13:41:55 250305-iconnmr 5 sst.31P.sen iconnmr + + + + + + + 31P Sensitivity 0.0485 M triphenylphosphate (TPP) in d6-acetone Specification result of sinocal: Best sino value found ( > 150:1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/5/pdata/1/250305-iconnmr_5_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/5/pdata/1/250305-iconnmr_5_1.pdf Check for printing system problems
4 13:28:55 250305-iconnmr 4 sst.19F.qnp.sen iconnmr + + + + + + + 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found ( > 250 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/4/pdata/1/250305-iconnmr_4_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/4/pdata/1/250305-iconnmr_4_1.pdf Check for printing system problems
3 13:06:06 250305-iconnmr 3 sst.13C.sen iconnmr + x + + + + + 13C Sensitivity 10% Ethylbenzene (EB) in CDCl3 Specification result of sinocal: Best sino value found ( > 200 :1) ATM Failed, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/3/pdata/1/250305-iconnmr_3_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/3/pdata/1/250305-iconnmr_3_1.pdf Check for printing system problems
2 12:55:00 250305-iconnmr 2 sst.1H.sen iconnmr + + + + + + + 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found ( > 300 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/2/pdata/1/250305-iconnmr_2_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/2/pdata/1/250305-iconnmr_2_1.pdf Check for printing system problems
1 12:44:40 250305-iconnmr 1 sst.1H.lsh iconnmr + + + + + + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/1/pdata/1/250305-iconnmr_1_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250305-iconnmr/1/pdata/1/250305-iconnmr_1_1.pdf Check for printing system problems
60 12:30:43 250305-dem 2 13C.day dem - + + - - + + DM-MS-03-77D-Dep ADC reported overflow
60 11:52:49 250305-dem 1 1H dem + + + + + + + DM-MS-03-77D-Dep
59 11:43:14 250305-tat 2 1H tat + + + + + + + X2-3
58 11:34:33 250305-tat 1 1H tat + + + + + + + X2-2
57 11:25:53 250305-z5167506 2 1H z5167506 + + + + + + + PAcGlu6NH CDCl3 T20
56 11:16:47 250305-z5167506 1 1H z5167506 + + + + + + + PAcGlu6NH CDCl3 T0
55 11:13:43 250305-z5532358 2 11B z5532358 - + + - - + +
55 11:06:30 250305-z5532358 1 1H z5532358 + + + + + + +
54 10:52:00 250305-z3542072 7 1H z3542072 + + + + + + + MM-296-120min-cdcl3
53 10:41:03 250305-z3542072 6 1H z3542072 + + + + + + + MM-296-60min-cdcl3
46 10:31:43 250305-yux 2 1H yux + + + + + + + pr 0403 16h cr
45 10:18:11 250305-yux 1 1H yux + + + + + + + pr 0403 0h
52 09:14:59 250305-nmrsu 1 1H nmrsu + + + + + + + SB146-B residue DMSO
51 09:03:08 250305-z3542072 5 1H z3542072 + + + + + + + MM-296-100mM-t30min-cdcl3
50 08:53:08 250305-z3542072 4 1H z3542072 + + + + + + + MM-296-100mM-t20min-cdcl3
49 08:45:22 250305-z3542072 3 1H z3542072 + + + + + + + MM-296-100mM-t10min-cdcl3
48 08:37:38 250305-z3542072 2 1H z3542072 + + + + + + + MM-296-100mM-t5min-cdcl3
47 08:28:55 250305-z3542072 1 1H z3542072 + + + + + + + MM-296-100mM-t0-cdcl3
45 04:11:00 250304-z5408582 5 1H.es z5408582 + + + + + + + 32
44 04:02:39 250304-z5408582 4 1H.es z5408582 + + + + + + + 31
43 03:56:00 250304-z5408582 3 1H.es z5408582 + + + + + + + 30
42 03:49:24 250304-z5408582 2 1H.es z5408582 + + + + + + + 29
41 03:42:32 250304-z5408582 1 1H.es z5408582 + + + + + + + 28
40 02:37:50 250304-pld 6 13C.night pld - + + - - + + PLD-4-16
40 02:31:31 250304-pld 5 1H pld + + + + + + + PLD-4-16
39 01:26:31 250304-pld 4 13C.night pld - + + - - + + PLD-4-11
39 01:19:48 250304-pld 3 1H pld + + + + + + + PLD-4-11
38 00:14:19 250304-pld 2 13C.night pld - + + - - + + PLD-2-29 ADC reported overflow
38 00:06:56 250304-pld 1 1H pld + + + + + + + PLD-2-29
37 00:02:31 250304-jlt 4 19F{1H} jlt - + + - - + + JT-P5JS-01-col-t40-45
37 23:49:27 250304-jlt 3 1H jlt + + + + + + + JT-P5JS-01-col-t40-45
36 23:44:02 250304-jlt 2 19F{1H} jlt - + + - - + + JT-P5JR-02-col-t25-29
36 23:30:36 250304-jlt 1 1H jlt + + + + + + + JT-P5JR-02-col-t25-29
35 23:15:55 250304-sub 4 1H sub + + + + + + + SB146-B residue Synthesis of D-imidazole-ND DMSO
34 23:02:58 250304-sub 3 1H sub + x + + + + + SB146-B filtrate Synthesis of D-imidazole-ND DMSO ATM Failed
33 22:54:49 250304-sub 2 1H sub + + + + + + + Imidaazole 2-CHO DMSO
32 22:44:27 250304-sub 1 1H sub + + + + + + + SB139-B CF2 Coupling 4-Pyr to DPND-7 CDCL3
31 22:36:13 250304-ogc 6 1H ogc + + + + + + + OG8017, DNT8 LiAlH4 crude, CDCl3
30 20:29:12 250304-ccc 2 13C.night ccc - + + - - + + GC8053-13C; C6 6-isoquinoline amination; F13-70; DMSO; 400MHz
30 20:21:57 250304-ccc 1 1H ccc + + + + + + + GC8053; C6 6-isoquinoline amination; F13-70; DMSO; 400MHz
29 20:16:44 250304-z5493478 6 19F z5493478 - + + - - + + SIC045-Supernatant CDCl3 Weber
29 20:09:52 250304-z5493478 5 1H z5493478 + + + + + + + SIC045-Supernatant CDCl3 Weber
28 20:05:04 250304-z5493478 4 19F z5493478 - + + - - + + SIC047-crude DMSO Weber
28 19:58:40 250304-z5493478 3 1H z5493478 + + + + + + + SIC047-crude DMSO Weber
27 19:48:51 250304-z5485590 9 1H z5485590 + + + + + + + MM294-180min-t180
26 19:22:04 250304-yac 2 13C.day yac - + + - - + + Y10036 Pre-TLC ADC reported overflow
26 19:13:30 250304-yac 1 1H yac + + + + + + + Y10036 Pre-TLC
25 19:05:15 250304-z3542072 1 1H z3542072 + + + + + + + MM-292-pmma-3-cdcl3
24 18:58:20 250304-z5537965 10 1H z5537965 + x + + + + + P1 MBT CH ATM Failed
23 18:51:02 250304-z5537965 9 1H z5537965 + + + + + + + Block CBA_A 0he_03.03.25
22 18:42:49 250304-z5371131 1 1H z5371131 + + + + + + + AM4.04 crude product
21 17:32:42 250304-z3543503 2 13C.night z3543503 + x + + + + + EB11p dry ATM Failed, ADC reported overflow
20 17:25:57 250304-djg 1 1H djg + + + + + + + DJG-S-014b Thioisopyrocoll purity check
19 17:15:28 250304-tat 5 1H tat + + + + + + + X2-1-4
18 17:05:58 250304-tat 4 1H tat + x + + + + + X2-1-3 ATM Failed
17 16:54:40 250304-tat 3 1H tat + + + + + + + X2-1-2
16 16:44:51 250304-tat 2 1H tat + + + + + + + X2-1-1
15 16:36:33 250304-z5426952 2 1H z5426952 + + + + + + + RI-D-79
14 16:27:19 250304-z5426952 1 1H z5426952 + + + + + + + RI-D-73
13 16:18:47 250304-z5628481 1 1H z5628481 + + + + + + + Me-01d crude reac nmr 1H
12 16:11:16 250304-z5167506 6 1H z5167506 + + + + + + + PDMAPAA PBA DMSO
11 16:04:09 250304-z5167506 5 1H z5167506 + + + + + + + 34 DMSO
10 15:57:14 250304-z5167506 4 1H z5167506 + + + + + + + 11.5 DMSO
9 15:49:49 250304-z5167506 3 1H z5167506 + + + + + + + 9.4 DMSO
8 15:41:22 250304-z5167506 2 1H z5167506 + + + + + + + PDMAPAA PBA T20 CDCl3
7 15:30:55 250304-z5167506 1 1H z5167506 + + + + + + + PDMAPAA PBA T0 CDCl3
6 15:23:48 250304-ogc 5 1H ogc + + + + + + + ID7059, DNT8 from ILD, CDCl3
5 15:16:56 250304-ogc 4 1H ogc + + + + + + + ID7053, DNT5 from ILD, CDCl3
4 15:09:15 250304-ogc 3 1H ogc + + + + + + + AAL(S), Iliya/Dave 50 mg sample check, CDCl3
3 15:01:23 250304-nnt 1 1H nnt + + + + + + + NT2
2 14:53:27 250304-z5537965 8 1H z5537965 + + + + + + + Block CBA_Post B_03.03.25
1 14:44:39 250304-z5485590 8 1H z5485590 + + + + + + + MM294-180min-t0
60 14:36:18 250304-z5485590 7 1H z5485590 + + + + + + + MM297-120min
59 14:26:29 250304-z5485590 6 1H z5485590 + + + + + + + MM297-60min
58 14:18:36 250304-z5485590 5 1H z5485590 + + + + + + + MM297-30min
57 14:09:49 250304-z5485590 4 1H z5485590 + + + + + + + MM297-20min
56 14:01:28 250304-z5485590 3 1H z5485590 + + + + + + + MM297-10min
55 13:48:34 250304-z5485590 2 1H z5485590 + + + + x + + MM297-5min Shim failed
54 13:39:46 250304-z5485590 1 1H z5485590 + + + + + + + MM297-0min
53 13:29:00 250304-z5547474 1 1H z5547474 + + + + + + + no.9 etching 4 days less solvent
52 13:11:02 250304-z5537965 7 1H z5537965 + + + + + + + Block ABC_Post purification_21.1.25
51 13:03:36 250304-z5537965 6 1H z5537965 + + + + + + + LH_21.1.25_Post purification
50 12:56:54 250304-z5537965 5 1H z5537965 + x + + + + + Deprotected_Anionic ATM Failed
49 12:49:25 250304-z5537965 4 1H z5537965 + + + + + + + Deprotected_Cat
48 12:42:30 250304-z5537965 3 1H z5537965 + + + + + + + Gua_Monomer
47 12:35:09 250304-z5537965 2 1H z5537965 + + + + + + + Cat_monomer
46 12:25:58 250304-z5537965 1 1H z5537965 + + + + + + + P1 Modified BTPA
45 12:00:16 250304-tat 1 1H tat + + + + + + + X2-1 4 spots
44 11:35:58 250304-ogc 2 1H ogc + + + + + + + OG8011, DNT5 scholl deprot F6-10, CDCl3
43 11:28:12 250304-ogc 1 1H ogc + + + + + + + OG8011, DNT5 scholl deprot F5, CDCl3
42 10:23:25 250304-z3542072 2 1H z3542072 + + + + + + + MM-292-t60min-cdcl3
40 09:42:14 250304-z5493478 2 19F z5493478 - x + - - + + SIC046-Fr.2.25-3.2 After heating with heatgun 5 min DMSO Weber ATM Failed
40 09:35:35 250304-z5493478 1 1H z5493478 + + + + + + + SIC046-Fr.2.25-3.2 After heating with heatgun 5 min DMSO Weber
39 09:05:33 250304-z3543503 1 13C.dept135 z3543503 + + + + + + + EB11p dry
38 05:17:19 250303-z5408582 4 1H.es z5408582 + + + + + + + 27
37 05:10:28 250303-z5408582 3 1H.es z5408582 + + + + + + + 26
36 05:02:16 250303-z5408582 2 1H.es z5408582 + + + + + + + 25
35 04:54:44 250303-z5408582 1 1H.es z5408582 + + + + + + + 24
34 03:50:13 250303-pld 12 13C.night pld - + + - - + + PLD-4-24
34 03:43:59 250303-pld 11 1H pld + + + + + + + PLD-4-24
33 02:39:27 250303-pld 10 13C.night pld - + + - - + + PLD-4-16
33 02:32:18 250303-pld 9 1H pld + + + + + + + PLD-4-16
32 01:27:36 250303-pld 8 13C.night pld - + + - - + + PLD-4-13
32 01:21:09 250303-pld 7 1H pld + + + + + + + PLD-4-13
31 00:16:42 250303-pld 6 13C.night pld - + + - - + + PLD-3-112
31 00:10:26 250303-pld 5 1H pld + + + + + + + PLD-3-112
30 23:05:45 250303-pld 4 13C.night pld - + + - - + + PLD-3-109
30 22:59:18 250303-pld 3 1H pld + + + + + + + PLD-3-109
29 21:54:07 250303-pld 2 13C.night pld - + + - - + + PLD-3-54
29 21:47:55 250303-pld 1 1H pld + + + + + + + PLD-3-54
34 21:42:37 250303-pld 11 1H pld + x + + - - - PLD-4-24 Automation was stopped by user
33 21:40:19 250303-pld 10 13C.night pld - x + - - x - PLD-4-16
33 21:30:00 250303-pld 9 1H pld + x + + x x - PLD-4-16
32 21:27:19 250303-pld 8 13C.night pld - x + - - x - PLD-4-13
32 21:17:20 250303-pld 7 1H pld + x + + x x - PLD-4-13
31 21:14:53 250303-pld 6 13C.night pld - x + - - x - PLD-3-112
31 21:04:57 250303-pld 5 1H pld + x + + x x - PLD-3-112
30 21:03:38 250303-pld 4 13C.night pld - x + - - x - PLD-3-109
30 20:53:40 250303-pld 3 1H pld + x + + x x - PLD-3-109
29 20:51:27 250303-pld 2 13C.night pld - - - - - - - PLD-3-54
29 20:45:03 250303-pld 1 1H pld + + + + + + + PLD-3-54
28 20:31:33 250303-yac 2 13C.day yac - + + - - + + Y10036
28 20:22:32 250303-yac 1 1H yac + + + + + + + Y10036
20 20:06:12 250303-ccc 1 1H ccc + + + + + + + GC8055; C6 5-indole amination; crude; DMSO; 400MHz
19 18:57:58 250303-z3543503 12 13C.night z3543503 + + + + + + + EB11p dry ADC reported overflow
27 18:54:14 250303-z5493478 6 19F z5493478 - + + - - + + SIC046-Fr.2.2-2.14 DMSO Weber
27 18:48:07 250303-z5493478 5 1H z5493478 + + + + + + + SIC046-Fr.2.2-2.14 DMSO Weber
26 18:44:20 250303-z5493478 4 19F z5493478 - + + - - + + SIC046-Fr.27-2.1 DMSO Weber
26 18:38:18 250303-z5493478 3 1H z5493478 + + + + + + + SIC046-Fr.27-2.1 DMSO Weber
25 18:34:10 250303-z5493478 2 19F z5493478 - + + - - + + SIC046-Fr.2.25-3.2 DMSO Weber
25 18:25:12 250303-z5493478 1 1H z5493478 + + + + + + + SIC046-Fr.2.25-3.2 DMSO Weber
24 18:19:11 250303-z5550254 6 19F{1H} z5550254 - + + - - + + AY-065.crude
24 18:12:42 250303-z5550254 5 19F z5550254 - + + - - + + AY-065.crude
24 17:56:01 250303-z5550254 4 1H z5550254 + + + + + + + AY-065.crude
23 17:48:10 250303-mda 5 1H mda + + + + + + + ReT0-1MBT
22 16:42:06 250303-jlt 4 13C.night jlt - + + - - + + JT-P5JR-01-col ADC reported overflow
22 16:37:28 250303-jlt 3 19F{1H} jlt - + + - - + + JT-P5JR-01-col
22 16:25:33 250303-jlt 2 1H.cosy jlt - x + - - + + JT-P5JR-01-col ATM Failed
22 16:13:55 250303-jlt 1 1H jlt + + + + + + + JT-P5JR-01-col
21 16:07:35 250303-z5550254 3 19F{1H} z5550254 - + + - - + + AY-065.crude
21 16:02:40 250303-z5550254 2 19F z5550254 - x + - - + + AY-065.crude ATM Failed
21 15:48:44 250303-z5550254 1 1H z5550254 + + + + + + + AY-065.crude
20 15:43:12 250303-z3543503 11 bbfo.1H.qnmr z3543503 - + + - - + + EB10 recryst
20 15:38:48 250303-z3543503 10 19F z3543503 - + + - - + + EB10 recryst
20 15:31:52 250303-z3543503 9 1H z3543503 + + + + + + + EB10 recryst
19 15:27:39 250303-z3543503 8 bbfo.1H.qnmr z3543503 - + + - - + + EB11p dry
19 15:19:43 250303-z3543503 7 19F z3543503 - x + - - + + EB11p dry ATM Failed
19 15:07:46 250303-z3543503 6 13C.dept135 z3543503 - + + - - + + EB11p dry
19 15:01:37 250303-z3543503 5 1H z3543503 + + + + + + + EB11p dry
18 14:53:40 250303-z5537965 1 1H z5537965 + + + + + + + Block CBA_B-0hr
17 14:46:56 250303-mda 4 1H mda + x + + + + + T0-1MBT ATM Failed
16 14:38:47 250303-z3542072 2 1H z3542072 + + + + + + + MM-294-t20min-cdcl3
15 14:29:16 250303-z3542072 1 1H z3542072 + x + + + + + MM-294-t60min-cdcl3 ATM Failed
14 14:15:28 250303-yab 2 13C.day yab - + + - - + + YA_1E3_P+_II ADC reported overflow
14 14:05:59 250303-yab 1 1H yab + + + + + + + YA_1E3_P+_II
13 13:51:17 250303-z5382436 1 1H z5382436 + + + + + + + AH02,152
12 13:07:38 250303-djg 5 1H djg + + + + + + + DJG-S-014a Isopyrocoll post MeOH trit
11 11:56:03 250303-z3543503 4 bbfo.1H.qnmr z3543503 - + + - - + + EB11p dry
11 11:51:06 250303-z3543503 3 19F z3543503 - + + - - + + EB11p dry
11 11:40:26 250303-z3543503 2 13C.dept135 z3543503 - x + - - + + EB11p dry ATM Failed
11 11:34:15 250303-z3543503 1 1H z3543503 + + + + + + + EB11p dry
10 11:26:51 250303-z5167506 2 1H z5167506 + + + + + + + PDMA PBA DMSO
9 11:19:04 250303-z5167506 1 1H z5167506 + + + + + + + 44 DMSO
8 11:12:35 250303-djg 4 1H djg + + + + + + + PTS-1-001 Crude DPM
7 11:03:38 250303-djg 3 1H djg + + + + + + + DJG-S-014c Dithio purity check
6 10:56:10 250303-djg 2 1H djg + + + + + + + DJG-B-139 Isopyrocoll purity check
5 10:48:55 250303-mda 3 1H mda + + + + + + +
4 10:40:38 250303-mda 2 1H mda + + + + + + + Nod-BT- CD
3 10:32:56 250303-mda 1 1H mda + + + + + + + Mod-BT
2 10:04:46 250303-djg 1 1H djg + + + + + + + DJG-S-014a Isopyrocoll purity check
1 09:25:59 250303-z5547474 6 1H z5547474 + x + + + + + DBU in DMSO ATM Failed
58 08:52:40 250303-z5547474 5 1H z5547474 + + + + + + + no 12. etching 4 days
57 08:46:30 250303-z5547474 4 1H z5547474 + + + + + + + no 11. etching 4 days
55 08:40:12 250303-z5547474 2 1H z5547474 + + + + + + + no 9. etching 4 days
54 08:31:33 250303-z5547474 1 1H z5547474 + + + + + + + no 7. etching 4 days
53 11:31:58 250302-z5550254 1 13C.night z5550254 + + + + + + + AY-063.4
52 23:21:20 250301-pld 3 13C.night pld + + + + + + + PLD-3-100
51 22:17:31 250301-pld 2 13C.night pld - x + - - + + PLD-3-108 ATM Failed, ADC reported overflow
51 22:08:16 250301-pld 1 1H pld + + + + + + + PLD-3-108
35 22:00:13 250301-jnn 7 19F{1H} jnn - x + - - + + JAN-199.3 ATM Failed
35 21:50:10 250301-jnn 6 19F jnn - + + - - + + JAN-199.3
35 21:36:52 250301-jnn 5 1H13C.hmbc jnn - + + - - + + JAN-199.3
35 21:18:21 250301-jnn 4 1H13C.hsqc.aded jnn - + + - - + + JAN-199.3
35 21:07:16 250301-jnn 3 1H.cosy jnn - + + - - + + JAN-199.3
35 19:00:48 250301-jnn 2 13C.night jnn - + + - - + + JAN-199.3
35 18:46:20 250301-jnn 1 1H jnn + + + + + + + JAN-199.3
34 17:45:04 250301-bgw 4 13C.dept45 bgw - + + - - + + y1-dept45
34 16:44:45 250301-bgw 3 13C.dept90 bgw - x + - - + + y1-dept90 ATM Failed
34 15:32:11 250301-bgw 2 13C.dept135 bgw - + + - - + + y1-dept135
34 14:22:38 250301-bgw 1 13C.night bgw + + + + + + + y1
50 14:16:33 250301-z5426952 1 1H z5426952 + x + + + + + RI-D-78 F1 ATM Failed
49 13:13:01 250228-pld 16 13C.night pld - x + - - + + PLD-3-115 ATM Failed
49 13:05:47 250228-pld 15 1H pld + + + + + + + PLD-3-115
48 12:01:17 250228-pld 14 13C.night pld - + + - - + + PLD-3-98
48 11:53:56 250228-pld 13 1H pld + + + + + + + PLD-3-98
47 10:49:16 250228-pld 12 13C.night pld - + + - - + + PLD-3-93
47 10:43:14 250228-pld 11 1H pld + + + + + + + PLD-3-93
46 09:38:36 250228-pld 10 13C.night pld - + + - - + + PLD-3-50
46 09:32:34 250228-pld 9 1H pld + + + + + + + PLD-3-50
45 08:28:03 250228-pld 8 13C.night pld - + + - - + + PLD-3-28
45 08:21:54 250228-pld 7 1H pld + + + + + + + PLD-3-28
44 07:17:27 250228-pld 6 13C.night pld - + + - - + + PLD-3-21
44 07:11:34 250228-pld 5 1H pld + + + + + + + PLD-3-21
43 06:06:50 250228-pld 4 13C.night pld - + + - - + + PLD-3-29
43 06:00:02 250228-pld 3 1H pld + + + + + + + PLD-3-29
42 04:55:28 250228-pld 2 13C.night pld - + + - - + + PLD-3-43
42 04:48:15 250228-pld 1 1H pld + + + + + + + PLD-3-43
41 03:44:11 250228-jlt 9 13C.night jlt - x + - - + + JT-4F-DET-step2-col-fb ATM Failed, ADC reported overflow
41 03:38:47 250228-jlt 8 19F{1H} jlt - + + - - + + JT-4F-DET-step2-col-fb
41 03:30:04 250228-jlt 7 1H jlt + + + + + + + JT-4F-DET-step2-col-fb
40 02:24:22 250228-jlt 6 13C.night jlt - + + - - + + JT-4F-DMT-step2-col-fb ADC reported overflow
40 02:15:32 250228-jlt 5 19F{1H} jlt - + + - - + + JT-4F-DMT-step2-col-fb
40 02:06:06 250228-jlt 4 1H jlt + + + + + + + JT-4F-DMT-step2-col-fb
39 01:01:35 250228-jlt 3 13C.night jlt - x + - - + + JT-4F-Pyr-step2-col-fb ATM Failed
39 00:56:17 250228-jlt 2 19F{1H} jlt - + + - - + + JT-4F-Pyr-step2-col-fb
39 00:48:00 250228-jlt 1 1H jlt + x + + + + + JT-4F-Pyr-step2-col-fb ATM Failed
38 23:43:51 250228-bgw 7 13C.night bgw - + + - - + + 2-c13-d2o
38 23:24:33 250228-bgw 6 1H.es bgw + + + + + + + 2-proton-d2o
37 22:20:04 250228-bgw 5 13C.night bgw - + + - - + + 1-c13-d2o
37 21:59:25 250228-bgw 4 1H.es bgw + + + + + + + 1-proton-d2o
36 21:46:39 250228-bgw 3 1H bgw + + + + + + + 3-standard-proton
35 21:34:01 250228-bgw 2 1H bgw + + + + + + + 2-proton
34 21:20:51 250228-bgw 1 1H bgw + + + + + + + 1-proton
33 21:09:55 250228-z5485590 1 1H z5485590 + x + + + + + MKA45-13h-crude ATM Failed
32 20:57:20 250228-z5550254 8 1H.cosy z5550254 - + + - - + + AY-062.2
32 19:29:43 250228-z5550254 7 13C.night z5550254 - + + - - + + AY-062.2
32 19:15:46 250228-z5550254 3 1H z5550254 + x + + + + + AY-062.2 ATM Failed
31 18:10:59 250228-z5550254 4 13C.night z5550254 - + + - - + + AY-063.4
31 17:57:13 250228-z5550254 3 1H z5550254 + + + + + + + AY-063.4
30 16:51:51 250228-z5550254 2 13C.night z5550254 - + + - - + + AY-064.2
30 16:37:07 250228-z5550254 1 1H z5550254 + + + + + + + AY-064.2
29 16:03:24 250228-z5426952 5 19F{1H} z5426952 + + + + + + + RI-118+IS
28 15:48:26 250228-z5537965 5 1H z5537965 + + + + + + + Samuel Polymer
27 15:41:13 250228-z5537965 4 1H z5537965 + + + + + + + T16 Anionic Poly
26 15:34:00 250228-z5537965 3 1H z5537965 + + + + + + + T16 Cationic poly
25 15:26:42 250228-z5537965 2 1H z5537965 + + + + + + + Random_ex_Post deprotection_24.25.25
24 15:16:17 250228-amn 1 1H amn + + + + + + + AMM H2 - Crude DPM after column - Fractions 24-55 - Supervisor Peeks
23 15:09:51 250228-z5426952 4 1H z5426952 + + + + + + + RI-118
22 14:51:07 250228-z5426952 3 19F{1H} z5426952 + x + + + + + RI-117+ IS ATM Failed
21 14:46:45 250228-z5426952 2 19F z5426952 - + + - - + + RI-117
21 14:38:25 250228-z5426952 1 1H z5426952 + + + + + + + RI-117
20 14:25:09 250228-djg 2 1H djg + + + + + + + DJG-B-143 Frac 5
19 14:17:06 250228-djg 1 1H djg + + + + + + + DJG-B-143 Frac 2
18 13:23:03 250228-z5537965 1 1H z5537965 + + + + + + + Block CBA_Post C_27.2.25
17 13:00:13 250228-ccc 1 1H ccc + + + + + + + GC8053; C6 6-isoquinoline amination; col flush BW; DMSO; 400MHz
16 12:05:30 250228-z5438782 1 1H z5438782 + x + + + + + elp mma 24h ATM Failed
15 11:57:53 250228-z5167506 2 1H z5167506 + + + + + + + PDMAPAA PBA T20 CDCl3
14 11:49:05 250228-z5167506 1 1H z5167506 + + + + + + + PDMAPAA PBA T0 CDCl3
13 11:41:24 250228-z5547474 5 1H z5547474 + + + + + + + no 12. etching 1 day
12 11:32:23 250228-z5547474 4 1H z5547474 + + + + + + + no 11. etching 1 day
11 11:25:17 250228-z5547474 3 1H z5547474 + + + + + + + no 10. etching 1 day
10 11:17:57 250228-z5547474 2 1H z5547474 + + + + + + + no 9. etching 1 day
9 11:10:00 250228-z5547474 1 1H z5547474 + + + + + + + no.7 etching 2 days
8 11:01:41 250228-z3542072 3 1H z3542072 + + + + + + + MM-292-t2-cdcl3
7 10:53:53 250228-z3542072 2 1H z3542072 + + + + + + + MM-292-t1-cdcl3
6 10:45:49 250228-z3542072 1 1H z3542072 + + + + + + + MM-292-t0-cdcl3
5 10:41:28 250228-z5493478 2 19F z5493478 - + + - - + + SIC046-crude DMSO Weber
5 10:33:07 250228-z5493478 1 1H z5493478 + + + + + + + SIC046-crude DMSO Weber
4 10:24:57 250228-jnn 4 19F{1H} jnn - x + - - + + JAN-199.3 ATM Failed
4 10:15:46 250228-jnn 3 19F jnn - + + - - + + JAN-199.3
4 10:02:01 250228-jnn 2 13C.day jnn - + + - - + + JAN-199.3
4 09:51:42 250228-jnn 1 1H jnn + x + + + + + JAN-199.3 ATM Failed
3 09:45:48 250228-z3543503 3 1H z3543503 + + + + + + + EB11n poly s1
2 09:39:31 250228-z3543503 2 1H z3543503 + + + + + + + EB11n poly s2
1 09:31:45 250228-z3543503 1 1H z3543503 + + + + + + + EB11n poly s2 t=0
53 03:30:39 250227-jnn 4 19F{1H} jnn - x + - - x - JAN-199.3
53 03:28:03 250227-jnn 3 19F jnn - x + - - x - JAN-199.3
53 03:25:34 250227-jnn 2 13C.night jnn - - - - - - - JAN-199.3
53 03:14:22 250227-jnn 1 1H jnn + + + + + + + JAN-199.3
52 03:06:27 250227-zhz 3 1H zhz + + + + + + + ZZ-097 purer NaH
51 02:56:33 250227-zhz 2 1H zhz + + + + + + + ZZ-097 purer NaH
50 02:49:30 250227-mda 3 1H mda + + + + + + + T0-DMHE
49 02:42:31 250227-mda 2 1H mda + + + + + + + HAEM Mono
48 02:35:32 250227-mda 1 1H mda + x + + + + + DMAE Mono ATM Failed
47 01:30:43 250227-z5550254 4 13C.night z5550254 - + + - - + + AY-065 ADC reported overflow
47 01:14:24 250227-z5550254 3 1H z5550254 + + + + + + + AY-065
46 01:05:47 250227-ogc 4 1H ogc + + + + + + + OG8013, Oxo-Pro scale up triflation crude, CDCl3
45 00:56:59 250227-ogc 3 1H ogc + + + + + + + OG8011, DNT5 Scholl deprot TFA crude, CDCl3
44 00:51:06 250227-ccc 1 1H ccc + x + + + + + GC8053; C6 6-isoquinoline amination; Flush; DMSO; 400MHz ATM Failed
43 00:46:10 250227-jlt 11 19F{1H} jlt - + + - - + + JT-4-F-MET-step1-19F{1H}
43 00:39:10 250227-jlt 10 1H jlt + x + + + + + JT-4-F-MET-step1-19F{1H} ATM Failed
42 23:33:39 250227-jlt 9 13C.night jlt - + + - - + + JT-4-F-pyr-step1 ADC reported overflow
42 23:28:47 250227-jlt 8 19F{1H} jlt - + + - - + + JT-4-F-pyr-step1
42 23:20:01 250227-jlt 7 1H jlt + x + + + + + JT-4-F-pyr-step1 ATM Failed
41 22:15:44 250227-jlt 6 13C.night jlt - x + - - + + JT-4-F-az-step1 ATM Failed, ADC reported overflow
41 22:07:02 250227-jlt 5 19F{1H} jlt - + + - - + + JT-4-F-az-step1
41 21:58:11 250227-jlt 4 1H jlt + + + + + + + JT-4-F-az-step1
40 20:54:22 250227-jlt 3 13C.night jlt - x + - - + + JT-4-F-DIPT-step1-THFrxn-DCMsolubleppt ATM Failed, ADC reported overflow
40 20:48:55 250227-jlt 2 19F{1H} jlt - + + - - + + JT-4-F-DIPT-step1-THFrxn-DCMsolubleppt
40 20:39:43 250227-jlt 1 1H jlt + + + + + + + JT-4-F-DIPT-step1-THFrxn-DCMsolubleppt
39 20:36:10 250227-z5493478 6 19F z5493478 - x + - - + + SIC046-crude DMSO Weber ATM Failed
39 20:29:46 250227-z5493478 5 1H z5493478 + + + + + + + SIC046-crude DMSO Weber
38 20:23:44 250227-z5426952 5 1H z5426952 + x + + + + + RI-117 Crude ATM Failed
37 20:11:01 250227-z5426952 4 13C.day z5426952 - + + - - + + RI-D-78 F2
37 20:03:43 250227-z5426952 3 1H z5426952 + + + + + + + RI-D-78 F2
36 18:55:44 250227-z5426952 2 13C.night z5426952 - + + - - + + RI-D-78 F3
36 18:45:35 250227-z5426952 1 1H z5426952 + + + + + + + RI-D-78 F3
35 18:39:42 250227-ild 3 1H ild + x + + + + + ID12021; nitro reduction cr; CDCl3 ATM Failed
34 18:33:01 250227-ild 2 1H ild + + + + + + + ID12019; indoline RedAm workup; CDCl3
33 17:28:44 250227-pld 2 13C.night pld - + + - - + + PLD-2-38
33 17:22:27 250227-pld 1 1H pld + x + + + + + PLD-2-38 ATM Failed
32 17:08:41 250227-z3541685 1 1H z3541685 + + + + + + + MWB_04_030a_fr30
31 16:59:23 250227-zhz 1 1H zhz + + + + + + + ZZ-097 DCM wash
30 16:49:24 250227-z5438782 2 1H z5438782 + + + + + + + elp mma 4h
29 16:38:07 250227-z3542072 4 1H z3542072 + + + + + + + MM-291-t5min-cdcl3
28 16:29:27 250227-z3542072 3 1H z3542072 + + + + + + + MM-291-t0-cdcl3
27 16:10:44 250227-z5371131 6 1H13C.hsqc.aded z5371131 - + + - - + + AM4.02 crude product
27 16:07:20 250227-z5371131 5 1H z5371131 - x + - - + + AM4.02 crude product ATM Failed
27 15:57:17 250227-z5371131 4 13C.dept90 z5371131 - + + - - + + AM4.02 crude product
27 15:43:33 250227-z5371131 3 13C.dept135 z5371131 - + + - - + + AM4.02 crude product ADC reported overflow
27 15:28:25 250227-z5371131 2 13C.day z5371131 + x + + + + + AM4.02 crude product ATM Failed, ADC reported overflow
26 15:18:09 250227-z5485590 2 1H z5485590 + + + + + + + MKA45-0min
25 15:09:03 250227-z5485590 1 1H z5485590 + x + + + + + MKA43-ppt ATM Failed
24 14:49:18 250227-nnt 1 1H nnt + x + + + + + ATM Failed
23 14:41:02 250227-djg 1 1H djg + + + + + + + DJG-B-142 ElectraSyn PMDI TBABr TMSCl 24h worked up
22 14:30:00 250227-z5438782 1 1H z5438782 + x + + + + + mma elp t0 ATM Failed
21 14:21:30 250227-yab 3 1H yab + + + + + + + 1E_3_P+
20 14:15:18 250227-yab 4 19F yab - + + - - + + TROPL_N+_BF4-
20 14:01:39 250227-yab 2 13C.day yab - + + - - + + TROPL_N+_BF4-
20 13:53:56 250227-yab 1 1H yab + x + + + + + TROPL_N+_BF4- ATM Failed
2 13:46:54 250227-ild 1 1H ild + + + + + + + ID12019; indoline RedAm A1; CDCl3; 400 MHz
1 13:40:04 250227-z5371131 1 1H z5371131 + + + + + + + 4.02 retry crude prod using NaCNBH3
60 13:30:46 250227-ogc 2 1H ogc + + + + + + + OG8009, Oxo-Pro trif 2 eq F8-11, CDCl3
59 13:24:31 250227-ogc 1 1H ogc + + + + + + + OG8009, Oxo-Pro trif 2 eq F7, CDCl3
58 13:17:55 250227-z5489717 1 1H z5489717 + + + + + + + DSM-R204a-ext.-CDCl3
57 13:10:39 250227-sub 3 1H sub + + + + + + + Matt's DP-Br2 CDCl3
56 13:01:53 250227-jcy 6 1H jcy + + + + + + + VP-01-03-T6h
55 12:54:04 250227-jcy 5 1H jcy + + + + + + + VP-01-02-T6h
54 12:46:49 250227-jcy 4 1H jcy + x + + + + + VP-01-01-T6h ATM Failed
53 12:39:14 250227-jcy 3 1H jcy + + + + + + + VP-01-03-T0 ADC reported overflow
52 12:30:34 250227-jcy 2 1H jcy + + + + + + + VP-01-02-T0
51 12:21:34 250227-jcy 1 1H jcy + + + + + + + VP-01-01-T0
50 12:13:33 250227-z3542072 2 1H z3542072 + + + + + + + MM-290-t10min-cdcl3
49 12:05:52 250227-z3542072 1 1H z3542072 + + + + + + + MM-290-t0-cdcl3
46 11:42:32 250227-sub 2 1H sub + + + + + + + SB83-K CF2 DPND-7 Br2 CDCl3
45 11:31:16 250227-sub 1 1H sub + + + + + + + SB83-K CF1 DPND-7 Br2 CDCl3
44 10:40:14 250227-z5106225 5 1H z5106225 - + + - - + + PET 2h
44 10:32:33 250227-z5106225 4 1H.es z5106225 + + + + + + + PET 2h
43 10:29:11 250227-z5106225 3 1H z5106225 - + + - - + + Piezophoto D2O 9:1
43 10:21:17 250227-z5106225 2 1H.es z5106225 + x + + + + + Piezophoto D2O 9:1 ATM Failed
42 10:15:20 250227-z5106225 1 1H z5106225 + x + + + + + Water D2O 1:1 ATM Failed
41 10:10:52 250227-z5493478 4 19F z5493478 - + + - - + + SIC045-waste CDCl3 Weber
41 10:04:31 250227-z5493478 3 1H z5493478 + + + + + + + SIC045-waste CDCl3 Weber
40 09:59:59 250227-z5493478 2 19F z5493478 - + + - - + + SIC045-crystals CDCl3 Weber
40 09:53:03 250227-z5493478 1 1H z5493478 + + + + + + + SIC045-crystals CDCl3 Weber
39 09:37:25 250227-z5550254 2 1H z5550254 + x + + + + + AY-064.2 ATM Failed
38 09:26:48 250227-z5550254 1 1H z5550254 + + + + + + + AY-065-chlorination of triazole
37 09:15:23 250227-z5537965 1 1H z5537965 + + + + + + + Block CBA_Ohr_27.2.25
36 07:59:13 250226-pld 8 13C.night pld - + + - - + + PLD-2-36
36 07:51:55 250226-pld 7 1H pld + + + + + + + PLD-2-36
35 06:46:49 250226-pld 6 13C.night pld - + + - - + + PLD-2-31
35 06:40:51 250226-pld 5 1H pld + + + + + + + PLD-2-31
34 05:36:21 250226-pld 4 13C.night pld - + + - - + + PLD-2-30
34 05:29:56 250226-pld 3 1H pld + x + + + + + PLD-2-30 ATM Failed
33 04:24:53 250226-pld 2 13C.night pld - + + - - + + PLD-1-95 ADC reported overflow
33 04:17:34 250226-pld 1 1H pld + + + + + + + PLD-1-95
32 04:08:48 250226-jnn 6 19F{1H} jnn - x + - - + + JAN-199.2 ATM Failed
32 03:59:25 250226-jnn 5 19F jnn - + + - - + + JAN-199.2
32 03:44:43 250226-jnn 4 1H jnn + + + + + + + JAN-199.2
31 02:38:53 250226-jlt 18 13C.night jlt - + + - - + + JT-4F-DET-step1
31 02:33:27 250226-jlt 17 19F{1H} jlt - + + - - + + JT-4F-DET-step1
31 02:20:47 250226-jlt 16 1H jlt + x + + + + + JT-4F-DET-step1 ATM Failed
30 01:15:39 250226-jlt 15 13C.night jlt - + + - - + + JT-4F-MIPT-step1 ADC reported overflow
30 01:10:06 250226-jlt 14 19F{1H} jlt - + + - - + + JT-4F-MIPT-step1
30 00:55:07 250226-jlt 13 1H jlt + + + + + + + JT-4F-MIPT-step1
29 23:50:18 250226-jlt 12 13C.night jlt - + + - - + + JT-4F-DMT-step1
29 23:44:52 250226-jlt 11 19F{1H} jlt - x + - - + + JT-4F-DMT-step1 ATM Failed
29 23:32:41 250226-jlt 10 1H jlt + x + + + + + JT-4F-DMT-step1 ATM Failed
28 22:27:05 250226-jlt 9 13C.night jlt - + + - - + + JT-4F-MET-step1 ADC reported overflow
28 22:22:42 250226-jlt 8 19F{1H} jlt - x + - - + + JT-4F-MET-step1 ATM Failed
28 22:09:14 250226-jlt 7 1H jlt + + + + + + + JT-4F-MET-step1
27 22:04:26 250226-jlt 6 19F{1H} jlt - + + - - + + JT-6F-DMT-step2-fb-19F{1H}
27 21:56:48 250226-jlt 5 1H jlt + + + + + + + JT-6F-DMT-step2-fb-19F{1H}
26 21:49:36 250226-jcy 13 1H jcy + + + + + + + SR-02-03-T1.5h
25 21:42:10 250226-jcy 12 1H jcy + + + + + + + SR-02-02-T1.5h
24 21:35:01 250226-jcy 11 1H jcy + + + + + + + SR-02-01-T1.5h
23 21:25:38 250226-jcy 10 1H jcy + + + + + + + SR-02-03-T0
22 21:18:01 250226-jcy 9 1H jcy + + + + + + + SR-02-02-T0
21 21:11:29 250226-jcy 8 1H jcy + x + + + + + SR-02-01-T0 ATM Failed
20 21:04:17 250226-jcy 7 1H jcy + + + + + + + SR-01-03-T1h
19 20:56:30 250226-jcy 6 1H jcy + + + + + + + SR-01-02-T1h
18 20:49:10 250226-jcy 5 1H jcy + + + + + + + SR-01-01-T1h
17 20:43:19 250226-jcy 4 1H jcy - - - - - - - SR-01-03-T0
15 20:35:55 250226-jcy 3 1H jcy + + + + + + + SR-01-02-T0
14 20:27:22 250226-jcy 2 1H jcy + + + + + + + SR-01-01-T0
13 20:19:28 250226-jcy 1 1H jcy + + + + + + + VP-01-DMAPAm.HCl
12 20:11:06 250226-jnn 3 19F{1H} jnn - x + - - + + JAN-199.1 ATM Failed
12 20:02:46 250226-jnn 2 19F jnn - x + - - + + JAN-199.1 ATM Failed
12 19:48:37 250226-jnn 1 1H jnn + + + + + + + JAN-199.1
11 18:43:38 250226-z5426952 6 13C.night z5426952 - x + - - + + RI-D-78 L ATM Failed
11 18:37:44 250226-z5426952 5 1H z5426952 + x + + + + + RI-D-78 L ATM Failed
10 17:32:02 250226-z5426952 4 13C.night z5426952 - + + - - + + RI-D-78 2L ADC reported overflow
10 17:21:38 250226-z5426952 3 1H z5426952 + + + + + + + RI-D-78 2L
9 17:13:16 250226-z3542072 4 1H z3542072 + x + + + + + MM-289-t30min-cdcl3 ATM Failed
8 17:04:39 250226-z3542072 3 1H z3542072 + + + + + + + MM-289-t0-cdcl3
7 16:58:23 250226-z5371131 1 1H z5371131 + x + + + + + AM1.04-3 mannich rxn crude prec ATM Failed
6 16:49:15 250226-z5438782 2 1H z5438782 + x + + + + + c3n4 pmma crude ATM Failed
5 16:39:52 250226-z5438782 1 1H z5438782 + x + + + + + elp 75wt% 24h ATM Failed
4 16:27:45 250226-z3543503 16 19F.polymer z3543503 - + + - - + + EB11n poly s1 t=0
4 16:16:47 250226-z3543503 15 1H z3543503 + + + + + + + EB11n poly s1 t=0
3 16:04:38 250226-z3543503 14 19F.polymer z3543503 - + + - - + + EB11n poly s2
3 15:57:27 250226-z3543503 13 1H z3543503 + + + + + + + EB11n poly s2
2 15:46:10 250226-z3543503 12 19F.polymer z3543503 - x + - - + + EB11n poly s2 t=0 ATM Failed
2 15:39:36 250226-z3543503 11 1H z3543503 + + + + + + + EB11n poly s2 t=0
1 15:33:47 250226-z3543503 10 bbfo.1H.qnmr z3543503 - x + - - + + EB11q purified ATM Failed
1 15:29:18 250226-z3543503 9 19F z3543503 - + + - - + + EB11q purified
1 15:19:46 250226-z3543503 8 1H z3543503 + + + + + + + EB11q purified
26 14:32:16 250226-jlt 4 1H.cosy jlt - + + - - + + JT-6F-DIPT-alt-step2-t24-26
26 14:23:16 250226-jlt 3 1H jlt + x + + + + + JT-6F-DIPT-alt-step2-t24-26 ATM Failed
25 14:14:16 250226-jlt 2 1H jlt + + + + + + + JT-6F-DIPT-alt-step2-t10
24 14:00:51 250226-jlt 1 1H jlt + + + + + + + X-2499-011-check
23 13:45:48 250226-iconnmr 5 sst.31P.sen iconnmr + + + + + + + 31P Sensitivity 0.0485 M triphenylphosphate (TPP) in d6-acetone Specification result of sinocal: Best sino value found ( > 150:1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/5/pdata/1/250226-iconnmr_5_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/5/pdata/1/250226-iconnmr_5_1.pdf Check for printing system problems
22 13:35:00 250226-iconnmr 4 sst.19F.qnp.sen iconnmr + + + + + + + 19F Sensitivity 0.05 Trifluourotoluene in CDCl3 Specification result of sinocal: Best sino value found ( > 250 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/4/pdata/1/250226-iconnmr_4_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/4/pdata/1/250226-iconnmr_4_1.pdf Check for printing system problems
21 13:11:17 250226-iconnmr 3 sst.13C.sen iconnmr + + + + + + + 13C Sensitivity 10% Ethylbenzene (EB) in CDCl3 Specification result of sinocal: Best sino value found ( > 200 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/3/pdata/1/250226-iconnmr_3_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/3/pdata/1/250226-iconnmr_3_1.pdf Check for printing system problems
20 13:00:45 250226-iconnmr 2 sst.1H.sen iconnmr + + + + + + + 1H Sensitivity 0.1% Ethyl Benzene in CDCl3 Specification result of sinocal: Best sino value found ( > 300 :1) No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/2/pdata/1/250226-iconnmr_2_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/2/pdata/1/250226-iconnmr_2_1.pdf Check for printing system problems
19 12:51:38 250226-iconnmr 1 sst.1H.lsh iconnmr + x + + + + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) ATM Failed, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/1/pdata/1/250226-iconnmr_1_1.pdf Check for printing system problems, No Pdf file found in dataset: F:/Weber/data/iconnmr/nmr/250226-iconnmr/1/pdata/1/250226-iconnmr_1_1.pdf Check for printing system problems
18 12:44:27 250226-z5537965 2 1H z5537965 + + + + + + + Random_post poly_24.2.25
17 12:37:14 250226-z5537965 1 1H z5537965 + + + + + + + Block CBA- post C_ 24.2.25_300mg
16 12:33:22 250226-z5532358 5 19F z5532358 - - - - - - - 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) sst.1H.lsh Acetone {F:\Weber} iconnmr 33
15 12:25:47 250226-mda 1 1H mda + + + + + + + T16-Mod BT
14 12:19:56 250226-z3543503 6 1H z3543503 + + + + + + + EB11n poly repeat
13 12:16:20 250226-z3543503 7 19F z3543503 - x + - - + + EB11n poly t=0 ATM Failed
13 12:06:02 250226-z3543503 5 1H z3543503 + + + + + + + EB11n poly t=0
12 12:02:34 250226-z5532358 4 19F z5532358 - + + - - + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) sst.1H.lsh Acetone {F:\Weber} iconnmr 33 complex
12 11:54:28 250226-z5532358 3 19F z5532358 + x + + + + + 1H Lineshape: CHCl3 in d6-Acetone Specification result of humpcal: Linewidth at 0.55% of signal height = ( < 6 Hz) Linewidth at 0.11% of signal height = ( < 12 Hz) Halfwidth = ( < 0.6 Hz) sst.1H.lsh Acetone {F:\Weber} iconnmr 33 complex ATM Failed
11 11:50:59 250226-z5532358 2 1H z5532358 - + + - - + + rtg44 insoluble in acetone white powqder
11 11:43:01 250226-z5532358 1 11B z5532358 + + + + + + + rtg44 insoluble in acetone white powqder
10 11:32:31 250226-z5582032 4 1H z5582032 + + + + + + + 8k POEGMEA Tf
9 11:22:14 250226-z5582032 3 1H z5582032 + x + + + + + 8k POEGMEA T0 ATM Failed
8 11:12:07 250226-z5582032 2 1H z5582032 + + + + + + + 5k POEGMEA Tf
7 11:02:20 250226-z5582032 1 1H z5582032 + x + + + + + 5k POEGMEA T0 ATM Failed
6 10:55:14 250226-z3542072 2 1H z3542072 + + + + + + + MM-PMMA-257-cdcl3
5 10:47:31 250226-z3542072 1 1H z3542072 + + + + + + + MM-PMMA-batcha-cdcl3
4 10:41:19 250226-amn 1 1H amn + + + + + + + AMM - Crude TMPH2 in CDCl3 + pyr-5d - supervisor Peeks
3 10:27:49 250226-z5426952 2 13C.day z5426952 - + + - - + + RI-D-77 Pure ADC reported overflow
3 10:17:42 250226-z5426952 1 1H z5426952 + + + + + + + RI-D-77 Pure
2 10:12:42 250226-z3543503 4 bbfo.1H.qnmr z3543503 - + + - - + + EB11n poly
2 10:04:09 250226-z3543503 2 1H z3543503 + x + + + + + EB11n poly ATM Failed
1 09:12:47 250226-z3543503 3 bbfo.1H.qnmr z3543503 - + + - - + + EB11n poly t=0
1 09:03:40 250226-z3543503 1 1H z3543503 + + + + + + + EB11n poly t=0
28 20:46:28 250225-z5532358 5 19F z5532358 + x + + x + + rtg45 ATM Failed, Shim failed
3 20:40:11 250225-ccc 2 1H ccc + x + + + + + GC8051; C6 phenylmethylsulfonamide amination; crude; DMSO; 400MHz ATM Failed
2 20:28:40 250225-z5438782 7 1H z5438782 + + + + + + + elp 75wt% 6h
1 20:24:03 250225-jlt 4 19F{1H} jlt - + + - - + + 4F-Cl-19F{H}
1 20:17:02 250225-jlt 3 1H jlt + + + + + + + 4F-Cl-19F{H}
60 20:13:36 250225-jlt 2 19F{1H} jlt - x + - - + + 6-F-az-fum-check ATM Failed
60 19:57:47 250225-jlt 1 1H jlt + + + + + + + 6-F-az-fum-check
59 19:53:41 250225-tat 5 31P tat - x + - - + + (15)-F18-20 ATM Failed
59 19:43:22 250225-tat 4 1H tat + + + + + + + (15)-F18-20
58 19:39:06 250225-tat 3 31P tat - x + - - + + (15)-F21-24 ATM Failed
58 19:30:32 250225-tat 2 1H tat + x + + + + + (15)-F21-24 ATM Failed
57 19:23:34 250225-tat 1 1H tat + + + + + + + RA-CN
56 19:19:00 250225-z5493478 2 19F z5493478 - + + - - + + SIC045-Fr.5-15 CDCl3 Weber
56 19:11:33 250225-z5493478 1 1H z5493478 + x + + + + + SIC045-Fr.5-15 CDCl3 Weber ATM Failed
55 19:04:55 250225-mda 1 1H mda + x + + + + + T0-Mod-BT ATM Failed
54 18:55:31 250225-z3543503 16 bbfo.1H.qnmr z3543503 - + + - - + + EB11q liquid
54 18:51:10 250225-z3543503 15 19F z3543503 - + + - - + + EB11q liquid
54 18:45:01 250225-z3543503 14 1H z3543503 + + + + + + + EB11q liquid
53 18:40:55 250225-z3543503 13 bbfo.1H.qnmr z3543503 - + + - - + + EB11q solid DCM filter
53 18:36:42 250225-z3543503 12 19F z3543503 - + + - - + + EB11q solid DCM filter
53 18:30:35 250225-z3543503 11 1H z3543503 + + + + + + + EB11q solid DCM filter
52 18:24:17 250225-z3543503 10 bbfo.1H.qnmr z3543503 - + + - - + + EB11q solid after rovap
52 18:20:32 250225-z3543503 9 19F z3543503 - + + - - + + EB11q solid after rovap
52 18:13:34 250225-z3543503 8 1H z3543503 + + + + + + + EB11q solid after rovap
51 18:07:33 250225-z3543503 7 bbfo.1H.qnmr z3543503 - + + - - + + EB11q solid
51 18:03:38 250225-z3543503 6 19F z3543503 - + + - - + + EB11q solid
51 17:55:50 250225-z3543503 5 1H z3543503 + + + + + + + EB11q solid
50 17:44:19 250225-z3543503 4 19F.polymer z3543503 - + + - - + + EB11n poly
50 17:38:18 250225-z3543503 3 1H z3543503 + x + + + + + EB11n poly ATM Failed
49 17:26:13 250225-z3543503 2 19F.polymer z3543503 - + + - - + + EB11n poly t=0
49 17:20:03 250225-z3543503 1 1H z3543503 + x + + + + + EB11n poly t=0 ATM Failed
48 17:13:16 250225-z5371131 2 1H z5371131 + + + + + + + AM4.01 using NaCNBH3 prod check
47 17:01:06 250225-z5485590 2 1H z5485590 + + + + + + + MKA43-0min-crude
46 16:50:01 250225-z5485590 1 1H z5485590 + + + + + + + MKA43-2h-crude
45 16:42:36 250225-jsm 4 1H jsm + + + + + + + JM300ff (stopped after S1 to see yield of first step and how location in light reactor is affecting yield)
44 16:35:28 250225-jsm 3 1H jsm + + + + + + + JM300ee (stopped after S1 to see yield of first step and how location in light reactor is affecting yield)
43 16:28:01 250225-jsm 2 1H jsm + + + + + + + JM300dd (stopped after S1 to see yield of first step and how location in light reactor is affecting yield)
42 16:19:28 250225-jsm 1 1H jsm + + + + + + + JM300cc (stopped after S1 to see yield of first step and how location in light reactor is affecting yield)
41 16:10:11 250225-z3542072 2 1H z3542072 + + + + + + + MM-282-T3h-cdcl3
40 16:01:17 250225-z3542072 1 1H z3542072 + + + + + + + MM-282-T0-cdcl3
39 15:54:44 250225-z5543281 2 1H z5543281 + + + + + + + Gua di-Boc after column
38 15:43:14 250225-z5438782 6 1H z5438782 + + + + + + + elp 75wt% 2h
37 15:32:59 250225-z5438782 5 1H z5438782 + + + + + + + elp 75 wt% 1h
36 15:18:50 250225-zhz 1 1H.es zhz + + + + x + + Forced fluorescent MeOH soluble Shim failed
35 15:04:12 250225-z5550254 3 1H z5550254 + + + + + + + AY-064
34 14:49:17 250225-z5550254 2 1H z5550254 + + + + + + + AY-062.2
33 14:35:24 250225-z5550254 1 1H z5550254 + + + + + + + AY-062.1
32 14:29:22 250225-z5543281 1 1H z5543281 + x + + + + + HETS10 ATM Failed
31 14:14:34 250225-z5426952 3 1H z5426952 + + + + + + + RI-D-77 F2
30 14:06:25 250225-z5426952 2 1H z5426952 + + + + + + + RI-D-77 F1
29 14:00:12 250225-z5426952 1 1H z5426952 + x + + + + + RI-D-75 pure ATM Failed
28 13:54:43 250225-z5532358 4 19F z5532358 - + + - - + + rtg45
28 13:46:37 250225-z5532358 3 11B z5532358 + + + + x + + rtg45 Shim failed
28 13:35:21 250225-z5532358 2 19F z5532358 - + + - - + + rtg45
28 13:27:12 250225-z5532358 1 11B z5532358 + x + + x + + rtg45 ATM Failed, Shim failed
27 13:19:06 250225-isj 1 19F{1H} isj + x + + + + + IJ-025-2 ATM Failed
26 13:08:39 250225-yab 3 19F yab + + + + + + + TROPL_N+_RECRY
25 12:55:32 250225-yab 2 13C.day yab - + + - - + + 1EM_+RECRY
25 12:47:41 250225-yab 1 1H yab + + + + + + + 1EM_+RECRY
24 12:00:24 250225-z5371131 1 1H z5371131 + + + + + + + AM1.04-2 check 25.02.25
23 11:40:25 250225-z5438782 4 1H z5438782 + + + + + + + elp bulk 2h
22 11:25:47 250225-z5438782 3 1H z5438782 + + + + + + + elp bulk 1h
21 11:06:48 250225-law 1 1H law + + + + + + + LW-166-A2
20 10:57:19 250225-ccc 1 1H ccc + x + + + + + GC6105; C6 phenylmethylsulfonamide suzuki; F5-10 freezer RBF; CDCl3; 400MHz ATM Failed
19 10:49:55 250225-z5407480 1 1H z5407480 + + + + + + + hl017
18 10:36:33 250225-z5438782 2 1H z5438782 + + + + + + + elp bulk 6h
17 10:23:01 250225-z5438782 1 1H z5438782 + + + + + + + elp bulk 4h
16 10:10:18 250225-yac 2 13C.day yac - + + - - + + Y100028 main peak
16 09:58:56 250225-yac 1 1H yac + + + + + + + Y100028 main peak
15 09:48:05 250225-att 1 1H att + + + + + + + SA-26-6 Post Heck reaction (maybe SA-26-7?) Yellow solid HNMR DMSO-d6
14 09:37:41 250225-z5601781 1 1H z5601781 + + + + + + + YZ-AM-014-17h
13 09:31:49 250225-z5451239 2 1H z5451239 + x + + + + + tp1-p40 ATM Failed
12 09:25:17 250225-z5451239 1 1H z5451239 + + + + + + + tpi- oh
11 09:17:44 250225-z5537965 2 1H z5537965 + + + + + + + Block C-B-A_ 0hr_24.2.25_300mg
10 09:10:05 250225-z5537965 1 1H z5537965 + + + + + + + Random_24.2.25_ex
9 09:01:18 250225-z5492625 1 1H z5492625 + + + + + + + JC-073-2 (5d)
8 02:27:04 250224-z5408582 4 1H.es z5408582 + + + + + + + 23
7 02:19:43 250224-z5408582 3 1H.es z5408582 + + + + + + + 22
6 02:13:23 250224-z5408582 2 1H.es z5408582 + x + + + + + 21 ATM Failed
5 02:06:01 250224-z5408582 1 1H.es z5408582 + + + + + + + 20
4 00:57:54 250224-pld 1 13C.night pld + + + + + + + PLD-4-7
3 00:51:01 250224-z5543281 3 1H z5543281 + x + + + + + Guanidine monomer 4th spot ATM Failed
2 00:44:10 250224-z5543281 2 1H z5543281 + + + + + + + Guanidine monomer 2nd+3rd spots
1 00:36:31 250224-z5543281 1 1H z5543281 + + + + + + + Guanidine monomer 1st spot
60 00:31:07 250224-z5493478 4 19F z5493478 - + + - - + + CHL336 Bromo o-FAB CDCl3 Weber
60 00:22:18 250224-z5493478 3 1H z5493478 + + + + + + + CHL336 Bromo o-FAB CDCl3 Weber
59 00:18:52 250224-z5493478 2 19F z5493478 - x + - - + + SIC045-crude CDCl3 Weber ATM Failed
59 00:12:56 250224-z5493478 1 1H z5493478 + x + + + + + SIC045-crude CDCl3 Weber ATM Failed
58 00:07:04 250224-ogc 4 1H ogc + x + + + + + OG8005, Methyl Scholl purif F19, CDCl3 ATM Failed
57 23:59:33 250224-ogc 3 1H ogc + + + + + + + OG8005, Methyl Scholl purif F18, CDCl3
56 23:52:29 250224-ogc 2 1H ogc + + + + + + + OG8005, Methyl Scholl purif F17, CDCl3
55 23:45:28 250224-ogc 1 1H ogc + + + + + + + OG8005, Methyl Scholl purif F16, CDCl3
54 23:38:22 250224-law 6 1H law + + + + + + + LW-165-P2-F1-2
53 23:30:58 250224-law 5 1H law + + + + + + + LW-162-A2-P1-F12-14
52 23:22:54 250224-law 4 1H law + x + + + + + LW-158-A2-P1-F1 ATM Failed
51 23:18:35 250224-law 3 19F law - + + - - + + JT-4-F-Cl
51 22:13:55 250224-law 2 13C.night law - + + - - + + JT-4-F-Cl
51 22:07:48 250224-law 1 1H law + x + + + + + JT-4-F-Cl ATM Failed
50 21:52:35 250224-z5550254 4 1H z5550254 + + + + + + + AY-063.4
49 21:39:37 250224-z5550254 3 1H z5550254 + x + + + + + AY-063.3 ATM Failed
48 21:23:14 250224-z5550254 2 1H z5550254 + + + + + + + AY-063.2
47 21:08:47 250224-z5550254 1 1H z5550254 + + + + + + + AY-063.1
46 20:47:47 250224-zhz 2 1H.cosy zhz - + + - - + +
46 20:38:03 250224-zhz 1 1H zhz + + + + + + +
45 20:22:58 250224-ccc 10 1H13C.hmbc ccc - + + - - + + GC8045; C6 benzonitrile amination; C2F6-10; DMSO; 400MHz
45 20:02:07 250224-ccc 9 1H13C.hsqc.aded ccc - + + - - + x GC8045; C6 benzonitrile amination; C2F6-10; DMSO; 400MHz
45 19:26:58 250224-ccc 8 1H.noesy ccc - + + - - + + GC8045; C6 benzonitrile amination; C2F6-10; DMSO; 400MHz
45 19:15:59 250224-ccc 7 1H.cosy ccc - + + - - + + GC8045; C6 benzonitrile amination; C2F6-10; DMSO; 400MHz
45 19:08:41 250224-ccc 6 1H ccc + + + + + + + GC8045; C6 benzonitrile amination; C2F6-10; DMSO; 400MHz
44 18:55:08 250224-ccc 5 1H13C.hmbc ccc - + + - - + + GC8045; C6 benzonitrile amination; C3F11-18; DMSO; 400MHz
44 18:36:31 250224-ccc 4 1H13C.hsqc.aded ccc - + + - - + x GC8045; C6 benzonitrile amination; C3F11-18; DMSO; 400MHz
44 18:01:16 250224-ccc 3 1H.noesy ccc - + + - - + + GC8045; C6 benzonitrile amination; C3F11-18; DMSO; 400MHz
44 17:49:56 250224-ccc 2 1H.cosy ccc - + + - - + + GC8045; C6 benzonitrile amination; C3F11-18; DMSO; 400MHz
44 17:43:11 250224-ccc 1 1H ccc + x + + + + + GC8045; C6 benzonitrile amination; C3F11-18; DMSO; 400MHz ATM Failed
43 17:36:38 250224-z5489717 1 1H z5489717 + + + + + + + DSM-5-bromopent-1-ene CDCl3
42 17:02:31 250224-jlt 3 13C.night jlt - + + - - + + JT-6-F-pyr-step2-fb ADC reported overflow
42 16:57:48 250224-jlt 2 19F{1H} jlt - + + - - + + JT-6-F-pyr-step2-fb
42 16:47:54 250224-jlt 1 1H jlt + + + + + + + JT-6-F-pyr-step2-fb
41 16:41:11 250224-mda 8 1H mda + x + + + + + T60min FDB ATM Failed
40 16:33:36 250224-mda 7 1H mda + + + + + + + T40min FDB
39 16:26:30 250224-mda 6 1H mda + + + + + + + T30min FDB
38 16:19:03 250224-mda 5 1H mda + + + + + + + T20min FDB
37 16:10:37 250224-mda 4 1H mda + + + + + + + T15min FDB
36 16:04:06 250224-mda 3 1H mda + x + + + + + T10min FDB ATM Failed
35 15:56:42 250224-mda 2 1H mda + + + + + + + T5min FDB
34 15:47:11 250224-z5485590 1 1H z5485590 + + + + + + + toluene-raft-point-6
33 15:37:03 250224-z5382436 6 1H z5382436 + + + + + + + AH01-73 final
32 15:27:20 250224-z5382436 5 1H z5382436 + + + + + + + pure BA chloroform
31 15:17:33 250224-z5382436 4 1H z5382436 + + + + + + + pure BA acetone
30 15:07:17 250224-z5382436 3 1H z5382436 + x + + + + + AH(35-2) ATM Failed
29 14:57:50 250224-z5382436 2 1H z5382436 + x + + + + + AH(35-1) ATM Failed
28 14:47:33 250224-z5382436 1 1H z5382436 + + + + + + + AH(35)
27 14:28:10 250224-bgw 8 1H.es bgw + + + + + + + b4c10a
26 14:08:16 250224-bgw 7 1H.es bgw + x + + + + + b4c08a ATM Failed
25 13:48:27 250224-bgw 6 1H.es bgw + + + + + + + b4c06a
24 13:29:35 250224-bgw 5 1H.es bgw + + + + + + + b4c04a
23 13:08:27 250224-bgw 4 1H.es bgw + + + + + + + b4c10
22 12:49:06 250224-bgw 3 1H.es bgw + + + + + + + b4c08
21 12:29:56 250224-bgw 2 1H.es bgw + x + + + + + b4c06 ATM Failed
20 12:05:07 250224-bgw 1 1H.es bgw + + + + x + + b4c04 Shim failed
8 11:37:50 250224-mda 1 1H mda + x + + + + + T0-FastDB ATM Failed
7 11:27:26 250224-z5371131 1 1H z5371131 + x + + + + + AM1.01-2 ATM Failed
6 11:17:23 250224-z5438782 2 1H z5438782 + x + + + + + elp bulk 30 min ATM Failed
5 11:05:46 250224-z5438782 1 1H z5438782 + + + + + + + elp bulk 15min
4 10:46:46 250224-z3543503 9 bbfo.1H.qnmr z3543503 - + + - - + + EB11p CHCl3 wash
4 10:42:57 250224-z3543503 8 19F z3543503 - + + - - + + EB11p CHCl3 wash
4 10:36:21 250224-z3543503 7 1H z3543503 + x + + + + + EB11p CHCl3 wash ATM Failed
3 10:32:08 250224-z3543503 6 bbfo.1H.qnmr z3543503 - + + - - + + EB11o CHCl3 wash
3 10:27:58 250224-z3543503 5 19F z3543503 - + + - - + + EB11o CHCl3 wash
3 10:21:51 250224-z3543503 4 1H z3543503 + + + + + + + EB11o CHCl3 wash
2 10:17:02 250224-z3543503 3 bbfo.1H.qnmr z3543503 - + + - - + + EB11n CHCl3 wash
2 10:12:46 250224-z3543503 2 19F z3543503 - + + - - + + EB11n CHCl3 wash
2 10:04:51 250224-z3543503 1 1H z3543503 + + + + + + + EB11n CHCl3 wash
1 08:38:59 250224-aes 1 1H aes + + + + + + +